IP Library Granted Patent US 12,365,027
Granted Patent B2
US 12,365,027 · App. 17/473,178 · Granted Jul 22, 2025

High speed shear-assisted extrusion

Inventors: Scott A. Whalen (West Richland, WA); Jens T. Darsell (West Richland, WA); Md. Reza-E-Rabby (Richland, WA); Brandon Scott Taysom (West Richland, WA); Tianhao Wang (Richland, WA); Darrell R. Herling (Kennewick, WA); Xiao Li (Richland, WA)
Assignee: Battelle Memorial Institute
B22F3/20B21C23/001B22F3/24B22F2003/248B22F2301/052B22F2302/25
View Patent ↗
Loading inventors, assignments & file history…
Monitor This Case
Get email alerts when status or documents change.
Order Certified Copies
Most orders are placed with the USPTO same day — all within 24 business hours.
Order via The Patent Place →
Pre-filled with this patent's details
Quick Facts
Patent No.
US 12,365,027
App. No.
17/473,178
Granted
Jul 22, 2025
Kind
B2
Abstract

A method for preparing a shear-assisted extruded material from a powder billet is provided, the method comprising providing a billet of material in substantially powder form; applying both axial and rotational pressure to the material to deform at least some of the contacted material; and extruding the material to form an extruded material. A method for preparing shear-assisted extruded material is provided, the method comprising applying both axial and rotational pressure to stock material to form an extruded material at a rate between 2 and 13 m/min. A method for preparing shear-assisted extruded material is provided. The method comprises applying both axial and rotational pressure to stock material to form an extruded material; and aging the extruded material for less than 3 hours. A method for preparing shear-assisted extruded material is provided. The method comprises providing a stock material for shear-assisted extrusion; and applying both axial and rotational force to the stock material to form an extruded material, wherein the axial force does not decrease during the extrusion.

Claims (36)

1. A method for preparing extruded material by shear assisted processing and extrusion, the method comprising:

applying axial extrusion force and rotational force at an interface of a face of a die tool and a face of a metallic stock material provided in a rotating feedstock container to form an extruded material at a rate between 2 and 13 m/min, wherein:

the face of the die tool comprises at least a portion that is generally perpendicular to the axial extrusion force; and

the portion that is generally perpendicular to the axial extrusion force comprise at least one spiral groove that directs plasticized material of the stock material toward aperture ports of the face of the die tool; and

wherein the metallic stock material is not pre-heated before applying the axial extrusion force and the rotational shearing force.

2. The method of claim 1 wherein the metallic stock material is defined by castings.

3. The method of claim 1 wherein the metallic stock material comprises Al.

4. The method of claim 1 wherein the extruded material comprises Al.

5. The method of claim 1 wherein the method further comprises maintaining a temperature of the die face below 420° C.

6. The method of claim 1 wherein the extruded material has a tensile strength between 500 and 580 MPa.

7. The method of claim 1 wherein the extruded material has a yield strength between 420 and 500 MPa.

8. The method of claim 1 wherein the extruded material has an elongation % between 12 and 18.

9. The method of claim 1 wherein the rate is between 3 and 13 m/min.

10. The method of claim 1 wherein the rate is between 7 and 13 m/min.

11. The method of claim 1 , wherein the metallic stock material is a non-homogenized metallic billet.

12. The method of claim 11 , wherein at least a portion of the extruded material is homogenized due to the applying of the axial extrusion force and the rotational shearing force.

13. A method for shear-assisted extrusion, the method comprising:

establishing an axial extrusion force and a rotational shearing force at an interface of a face of a die tool and a face of a non-homogenized metallic billet provided in a rotating feedstock container, wherein:

the face of the die tool comprises at least a portion that is generally perpendicular to the axial extrusion force; and

the portion that is generally perpendicular to the axial extrusion force comprises a spiral groove;

directing plasticized material of the non-homogenized metallic billet toward aperture ports of the face of the die tool using the spiral groove; and

extruding an extruded material from the non-homogenized metallic billet at a rate between 2 and 13 m/min.

14. The method of claim 13 , wherein the non-homogenized metallic billet is not pre-heated before applying the axial extrusion force and the rotational shearing force.

15. The method of claim 13 , wherein the non-homogenized metallic billet is not pre-heated or homogenized to remove microfissures before establishing the axial extrusion force and the rotational shearing force.

16. The method of claim 13 , wherein the extruded material is extruded at a rate between 3 and 13 m/min.

17. The method of claim 13 , wherein a linear speed of the non-homogenized metallic billet or the die tool is 0.36 m/min.

18. The method of claim 17 , wherein the linear speed of 0.36 m/min causes a rate of extrusion of between 7 and 8 m/min.

19. A method for shear-assisted extrusion, the method comprising:

establishing an axial extrusion force and a rotational shearing force at an interface of a face of a die tool and a face of a non-homogenized metallic billet provided in a rotating feedstock container; and

extruding an extruded material from the non-homogenized metallic billet at a rate between 2 and 13 m/min;

wherein:

the face of the die tool comprises at least a portion that is generally perpendicular to the axial extrusion force;

the portion that is generally perpendicular to the axial extrusion force comprises a spiral groove that directs plasticized material of the non-homogenous metallic billet toward aperture ports of the face of the die tool;

the non-homogenized metallic billet is not pre-heated before establishing the axial extrusion force and the rotational shearing force; and

the non-homogenized metallic billet is not homogenized to remove microfissures before establishing the axial extrusion force and the rotational shearing force.

20. The method of claim 19 , wherein the non-homogenized metallic billet is not pre-heated or homogenized to cause phase conversion and has less uniform consistency before extrusion than the extruded material.

Assignments (2)
CONFIRMATORY LICENSE Recorded Dec 14, 2021
From: BATTELLE MEMORIAL INSTITUTE, PNWD
To: U. S. DEPARTMENT OF ENERGY
Reel/Frame 058584/0268 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Dec 9, 2021
From: WHALEN, SCOTT A.; DARSELL, JENS T.; REZA-E-RABBY, MD.; TAYSOM, BRANDON SCOTT; WANG, TIANHAO; HERLING, DARRELL R.; LI, XIAO
To: BATTELLE MEMORIAL INSTITUTE
Reel/Frame 058346/0736 →
Continuity (13)
Continuation In Part 17242166 · Apr 27, 2021
Continuation In Part 17033854 · Sep 27, 2020
Continuation In Part 16562314 · Sep 5, 2019
Continuation In Part 16028173 · Jul 5, 2018
Continuation In Part 15898515 · Feb 17, 2018
Continuation In Part 15351201 · Nov 14, 2016
Continuation In Part 14222468 · Mar 21, 2014
Provisional Application 63077191 · Sep 11, 2020
Provisional Application 63015913 · Apr 27, 2021
Provisional Application 62460227 · Feb 17, 2017
Provisional Application 62313500 · Mar 25, 2016
Provisional Application 61084560 · Mar 22, 2013
Related Publication 20210402471A1 · Dec 30, 2021
References Cited (261)
US 3432369A · Naastepad · 1969 [cited by applicant]
US 3640657A · Rowe et al. · 1972 [cited by applicant]
US 3661726A · Denes · 1972 [cited by applicant]
US 3684593A · Benz et al. · 1972 [cited by applicant]
US 3884062A · Green · 1975 [cited by applicant]
US 3892603A · Reid · 1975 [cited by applicant]
US 3933536A · Doser et al. · 1976 [cited by applicant]
US 3977918A · Paladino et al. · 1976 [cited by applicant]
US 3989548A · Morris · 1976 [cited by applicant]
US 4287749A · Bachrach et al. · 1981 [cited by applicant]
US 4300378A · Thiruvarudchelvan · 1981 [cited by applicant]
US 4431467A · Staley et al. · 1984 [cited by applicant]
US 4585473A · Narasimhan et al. · 1986 [cited by applicant]
US 4778542A · Clemens · 1988 [cited by applicant]
US 4801340A · Inoue et al. · 1989 [cited by applicant]
US 4808224A · Anderson et al. · 1989 [cited by applicant]
US 4892596A · Chatterjee · 1990 [cited by applicant]
US 4985085A · Chatterjee · 1991 [cited by applicant]
US 5026438A · Young et al. · 1991 [cited by applicant]
US 5089060A · Bradley et al. · 1992 [cited by applicant]
US 5226989A · Sukonnik · 1993 [cited by applicant]
US 5242508A · McCallum et al. · 1993 [cited by applicant]
US 5262123A · Thomas et al. · 1993 [cited by applicant]
US 5283130A · Bradley et al. · 1994 [cited by applicant]
US 5437545A · Hirai · 1995 [cited by applicant]
US 5461898A · Lessen · 1995 [cited by applicant]
US 5470401A · McCallum et al. · 1995 [cited by applicant]
US 5492264A · Wadleigh · 1996 [cited by applicant]
US 5737959A · Korbel et al. · 1998 [cited by applicant]
US 5739498A · Sunamoto et al. · 1998 [cited by applicant]
US 5964117A · Holroyd et al. · 1999 [cited by applicant]
US 5988484A · Osborn et al. · 1999 [cited by applicant]
US 6022424A · Sellers et al. · 2000 [cited by applicant]
US 6036467A · Jameson · 2000 [cited by applicant]
US 6638462B2 · Davidson et al. · 2003 [cited by applicant]
US 6843405B2 · Okamoto et al. · 2005 [cited by applicant]
US 6940379B2 · Creighton · 2005 [cited by applicant]
US 7096705B2 · Segal · 2006 [cited by applicant]
US 7314670B2 · Bartsch et al. · 2008 [cited by applicant]
US 7322508B2 · Chang · 2008 [cited by applicant]
US 7954692B2 · Fukuda · 2011 [cited by applicant]
US 8016179B2 · Burford · 2011 [cited by applicant]
US 8240540B2 · Tanaka et al. · 2012 [cited by applicant]
US 8313692B2 · Somekawa et al. · 2012 [cited by applicant]
US 8695868B2 · Messer et al. · 2014 [cited by applicant]
US 10189063B2 · Lavender et al. · 2019 [cited by applicant]
US 10369748B2 · Whalen et al. · 2019 [cited by applicant]
US 10695811B2 · Joshi et al. · 2020 [cited by applicant]
US 10987754B1 · Eller et al. · 2021 [cited by applicant]
US 11045851B2 · Joshi et al. · 2021 [cited by applicant]
US 20020029601A1 · Kwok · 2002 [cited by applicant]
US 20040057782A1 · Okamoto et al. · 2004 [cited by applicant]
US 20040238501A1 · Kawazoe et al. · 2004 [cited by applicant]
US 20040265503A1 · Clayton et al. · 2004 [cited by applicant]
US 20050081594A1 · Segal · 2005 [cited by applicant]
US 20060005898A1 · Lui et al. · 2006 [cited by applicant]
US 20060027628A1 · Sutherlin et al. · 2006 [cited by applicant]
US 20080029581A1 · Kumagai et al. · 2008 [cited by applicant]
US 20080048005A1 · Forrest et al. · 2008 [cited by applicant]
US 20080202653A1 · Ignberg · 2008 [cited by applicant]
US 20080251571A1 · Burford · 2008 [cited by applicant]
US 20090072007A1 · Nagano · 2009 [cited by applicant]
US 20090269605A1 · Warke et al. · 2009 [cited by applicant]
US 20090291322A1 · Watanabe et al. · 2009 [cited by applicant]
US 20100059151A1 · Iwamura et al. · 2010 [cited by applicant]
US 20100089976A1 · Szymanski et al. · 2010 [cited by applicant]
US 20100132430A1 · Tsai et al. · 2010 [cited by applicant]
US 20110104515A1 · Kou et al. · 2011 [cited by applicant]
US 20110132970A1 · Nakagawa et al. · 2011 [cited by applicant]
US 20110309131A1 · Hovanski et al. · 2011 [cited by applicant]
US 20120006086A1 · Manchiraju et al. · 2012 [cited by applicant]
US 20120052322A1 · Hatakeyama et al. · 2012 [cited by applicant]
US 20120168045A1 · Ihara et al. · 2012 [cited by applicant]
US 20120223451A1 · Hulseman et al. · 2012 [cited by applicant]
US 20120258332A1 · Hatakeyama et al. · 2012 [cited by applicant]
US 20130075452A1 · Burford · 2013 [cited by applicant]
US 20130266467A1 · Manchiraju et al. · 2013 [cited by applicant]
US 20140000332A1 · Wilson et al. · 2014 [cited by applicant]
US 20140002220A1 · Johnson et al. · 2014 [cited by applicant]
US 20140076957A1 · Sayama et al. · 2014 [cited by applicant]
US 20140102159A1 · Denison · 2014 [cited by applicant]
US 20140102161A1 · Stewart · 2014 [cited by applicant]
US 20140248508A1 · Ohhama et al. · 2014 [cited by applicant]
US 20140260489A1 · Funk · 2014 [cited by examiner]
US 20140283574A1 · Lavender et al. · 2014 [cited by applicant]
US 20140291886A1 · Mark et al. · 2014 [cited by applicant]
US 20140328710A1 · Cui et al. · 2014 [cited by applicant]
US 20150075242A1 · Eller et al. · 2015 [cited by applicant]
US 20150115019A1 · Pascal et al. · 2015 [cited by applicant]
US 20150360317A1 · Kalvala et al. · 2015 [cited by applicant]
US 20160008918A1 · Burford · 2016 [cited by applicant]
US 20160151817A1 · Nayfeh et al. · 2016 [cited by applicant]
US 20160151818A1 · Shao · 2016 [cited by applicant]
US 20160167353A1 · Fan et al. · 2016 [cited by applicant]
US 20160175981A1 · Kandasamy · 2016 [cited by applicant]
US 20160175982A1 · Kandasamy et al. · 2016 [cited by applicant]
US 20160184922A1 · Kikyo · 2016 [cited by applicant]
US 20160228932A1 · Hayashi et al. · 2016 [cited by applicant]
US 20160354860A1 · Boettcher et al. · 2016 [cited by applicant]
US 20170008121A1 · Li · 2017 [cited by applicant]
US 20170056947A1 · Lavender et al. · 2017 [cited by applicant]
US 20170136686A1 · Ueno et al. · 2017 [cited by applicant]
US 20170163135A1 · Emberton et al. · 2017 [cited by applicant]
US 20170182587A1 · Tokoro et al. · 2017 [cited by applicant]
US 20170216961A1 · Utter et al. · 2017 [cited by applicant]
US 20170225265A1 · Ito et al. · 2017 [cited by applicant]
US 20170304933A1 · Miles et al. · 2017 [cited by applicant]
US 20170355003A1 · TenHouten et al. · 2017 [cited by applicant]
US 20180036840A1 · Hu et al. · 2018 [cited by applicant]
US 20180043467A1 · Huysmans · 2018 [cited by applicant]
US 20180050419A1 · Das et al. · 2018 [cited by applicant]
US 20180311713A1 · Joshi et al. · 2018 [cited by applicant]
US 20180354231A1 · Iwase · 2018 [cited by applicant]
US 20180369889A1 · Zhang et al. · 2018 [cited by applicant]
US 20190267153A1 · Kappagantula et al. · 2019 [cited by applicant]
US 20190275608A1 · Das et al. · 2019 [cited by applicant]
US 20210053100A1 · Whalen et al. · 2021 [cited by applicant]
US 20210086291A1 · Okada et al. · 2021 [cited by applicant]
US 20210205918A1 · Fujii et al. · 2021 [cited by applicant]
US 20210252632A1 · Eller et al. · 2021 [cited by applicant]
US 20230081786A1 · Joshi et al. · 2023 [cited by applicant]
US 20230088412A1 · Joshi et al. · 2023 [cited by applicant]
US 20230150022A1 · Whalen et al. · 2023 [cited by applicant]
US 20230234115A1 · Kappagantula et al. · 2023 [cited by applicant]
CN 106140847A · 2016 [cited by applicant]
CN 107282671A · 2017 [cited by applicant]
CN 105925846B · 2018 [cited by applicant]
CN 109295332B · 2020 [cited by applicant]
CN 112512710B · 2023 [cited by applicant]
EP 2990178 · 2014 [cited by applicant]
EP 2777837A1 · 2014 [cited by applicant]
GB 1258141 · 1971 [cited by applicant]
JP 2002361320A · 2002 [cited by applicant]
JP 2003275876 · 2003 [cited by applicant]
JP 2004174563A · 2004 [cited by applicant]
JP 2007222925 · 2007 [cited by applicant]
JP 2009090359A · 2009 [cited by applicant]
JP 2019115909A · 2019 [cited by applicant]
KR 101316989B1 · 2013 [cited by applicant]
WO PCTUS2019040730 · 2019 [cited by applicant]
WO 2020010331 · 2020 [cited by applicant]
WO 2020053168 · 2020 [cited by applicant]
WO WO2021062415A1 · 2021 [cited by applicant]
WO 2022056358 · 2022 [cited by applicant]
WO PCTUS2020053168 · 2022 [cited by applicant]
WO PCTUS2021050022 · 2022 [cited by applicant]
WO PCTUS2243532 · 2023 [cited by applicant]
WO PCTUS2023015228 · 2023 [cited by applicant]
WO WO2023177693A1 · 2023 [cited by applicant]
Abu-Farha, “A Preliminary Study on the Feasibility of Friction Stir Back Extrusion”, Scripta Materials, 66, 2012, United States, 615-618. [cited by applicant]
Amancio-Filho et al., “Joining of Polymers and Polymer-Metal Hybrid Structures: Recent Developments and Trends”, Polymer Engineering & Science, 2009, United States, pp. 1461-1476. [cited by applicant]
Bozzi et al., “Intermetallic Compounds in Al 6016/IF-Steel Friction Stir Spot Welds”, Materials Science and Engineering, 2010, Netherlands, pp. 4505-4509. [cited by applicant]
Cole et al., “Lightweight materials for Automotive Applications”, Materials Characterization, 35, 1995, United States, pp. 3-9. [cited by applicant]
Evans et al., “Friction Stir Extrusion: A new process for joining dissimilar materials”, Manufacturing Letters, 5, 2015, United States, pp. 25-28. [cited by applicant]
Gann, J.A., “Magnesium Industry's Lightest Structural Metal”, SAE Transactions, vol. 25-26, 1930-1931, United States, pp. 620-634, 641. [cited by applicant]
Hammond et al., “Equal-Channel Angular Extrusion of a Low-Density High-Entropy Alloy Produced by High-Energy Cryogenic Mechanical Alloying”, JOM. Vol. 66, No. 10, United States, 2014, pp. 2021-2029. [cited by applicant]
Kaiser et al., “Anisotropic Properties of Magnesium Sheet AZ31”, Materials Science Forum, vols. 419-422, Switzerland, 2003, pp. 315-320. [cited by applicant]
Kuo et al., “Fabrication of High Performance Magnesium/Carbon-Fiber/PEEK/Laminated Composites”, Materials Transactions, vol. 44, No. 8 (2003), Japan, pp. 1613-1619. [cited by applicant]
Leitao et al., “Aluminum-steel lap joining by multipass friction stir welding”, Materials and Design, 106, 2016, United States, pp. 153-160. [cited by applicant]
Liu et al., “A Review of Dissimilar Welding Techniques for Magnesium Alloys to Aluminum Alloys”, Materials, 7, 2014, United States, pp. 3735-3757. [cited by applicant]
Liu et al., “Microstructure and mechanical properties of equimolar FeCoCrNi high entropy alloy prepared via powder extrusion”, Intermetallics 75 (2016) , United States, pp. 25-30. [cited by applicant]
Luo, Alan, “Magnesium: Current and Potential Automotive Applications”, JOM, 54(2), 2002, United States, pp. 42-48. [cited by applicant]
Martinsen et al., “Joining of Dissimilar Materials”, CIRP Annals—Manufactring Technology, 2015, United States, 21 pages. [cited by applicant]
Nakamura et al., “Tool Temperature and Process Modeling of Friction Stir Welding”, (2018) Modern Mechanical Engineering, 8, 78-94. [cited by applicant]
Office Action for U.S. Appl. No. 14/222,468, filing date Mar. 21, 2014, First named inventor Curtis A. Lavender, Notification date Nov. 6, 2015, 10 pages. [cited by applicant]
Office Action for U.S. Appl. No. 14/222,468, filing date Mar. 21, 2014, First named inventor Curtis A. Lavender, Notification date Apr. 1, 2016, 10 pages. [cited by applicant]
Office Action for U.S. Appl. No. 14/222,468, filing date Mar. 21, 2014, First named inventor Curtis A. Lavender, Notification date May 20, 2016, 3 pages. [cited by applicant]
Office Action for U.S. Appl. No. 14/222,468, filing date Mar. 21, 2014, First named inventor Curtis A. Lavender, Notification date Jan. 26, 2017, 9 pages. [cited by applicant]
Office Action for U.S. Appl. No. 14/268,220, Filing date May 2, 2014, First Named Inventor Jun Cui, Notification date Dec. 1, 2015, 7 pages. [cited by applicant]
Pickens, “Aluminum Powder Metallurgy Technology for High-Strength Applications”, Journal of Materials Science 16 (1981) 1437-1457, United Kingdom, 21 pages. [cited by applicant]
Rodewald et al. “Top Nd—Fe—B Magnets with Greater Than 56 MGOe Energy Density and 9.8 kOe Coercivity”, IEEE Transactions on Magnetics, vol. 38, No. 5, 2002, United States, pp. 2955-2957. [cited by applicant]
Saha, “Aluminum Extrusion Technology, Chapter 1, Fundamentals of Extrusion”, The Materials Information Society, ASM International, 2000, United States, pp. 1-29. [cited by applicant]
ThomasNet.com, https:/www.thomasnet.com/articles/custom-manufacturing-fabricating/friction-stir-welding/ Feb. 10, 2011 (Year: 2011). [cited by applicant]
Trang et al., “Designing a Magnesium Alloy with High Strength and High Formability”, Nature Communications, 2018, United Kingdom, 6 pages. [cited by applicant]
Whalen et al., “High Ductility Aluminum Alloy Made from Powder by Friction Extrusion”, Materalia 6 (2019) 100260, Netherlands, 6 pages. [cited by applicant]
Whalen et al., U.S. Appl. No. 15/694,565, filed Sep. 1, 2017, titled “System and Process for Joining Dissimilar Materials and Solid-State Interocking Joint with Intermetallic Interface Formed Thereby”, 69 pages. [cited by applicant]
Zhang et al., “Numerical Studies on Effect of Axial Pressure in Friction Stir Welding”, (2007) Science and Technology of Welding and Joining, vol. 12, No. 3, United Kingdom, pp. 226-248. [cited by applicant]
Martinsen et al., “Joining of Dissimilar Materials”, CIRP Annals—Manufactring Technology, 2015, United States, 21 pages. Manufacturing. [cited by applicant]
“U.S. Appl. No. 17/033,854, Final Office Action mailed Jun. 7, 2023”, 11 pgs. [cited by applicant]
“U.S. Appl. No. 17/035,597, Final Office Action mailed May 10, 2023”, 13 pgs. [cited by applicant]
“U.S. Appl. No. 17/826,054, Preliminary Amendment filed Jul. 13, 2023”, 9 pgs. [cited by applicant]
“U.S. Appl. No. 17/033,854, Response filed Aug. 7, 2023 to Final Office Action mailed Jun. 7, 2023”, 9 pgs. [cited by applicant]
“U.S. Appl. No. 17/033,854, Advisory Action mailed Aug. 16, 2023”, 4 pgs. [cited by applicant]
“U.S. Appl. No. 17/035,597, Non Final Office Action mailed Aug. 28, 2023”, 10 pgs. [cited by applicant]
“U.S. Appl. No. 17/242,166, Final Office Action mailed Aug. 30, 2023”, 7 pgs. [cited by applicant]
U.S. Appl. No. 18/426,042, filed Jan. 29, 2024, Devices and Methods for Performing Shear-Assisted Extrusion and Extrusion Processes. [cited by applicant]
“European Application Serial No. 19745460.6, Response filed Sep. 18, 2023 to Communication Pursuant to Article 94(3) EPC mailed May 10, 2023”, 9 pages. [cited by applicant]
“European Application Serial No. 19745460.6, Communication Pursuant to Article 94(3) EPC mailed May 10, 2023”, 6 pages. [cited by applicant]
“CN 201980045070X Office Action mailed Sep. 6, 2022”, with English translation, 13 pages. [cited by applicant]
“CN 201980045070X Response mailed Apr. 11, 2023 to Office Action Sep. 6, 2022”, with English claims, 8 pages. [cited by applicant]
“European Application Serial No. 21867741.7, Response to Communication Pursuant to Rules 161 and 162 EPC filed Oct. 16, 2023”, 15 pages. [cited by applicant]
“U.S. Appl. No. 18/093,636, Restriction Requirement mailed Dec. 20, 2023”, 6 pages. [cited by applicant]
“U.S. Appl. No. 17/473,178, Non Final Office Action mailed Jan. 3, 2024”, 10 pages. [cited by applicant]
“U.S. Appl. No. 17/033,854, Final Office Action mailed Mar. 28, 2024”, 12 pgs. [cited by applicant]
“U.S. Appl. No. 17/033,854, Non Final Office Action mailed Oct. 4, 2023”, 11 pgs. [cited by applicant]
“U.S. Appl. No. 17/033,854, Response filed Mar. 7, 2024 to Non Final Office Action mailed Oct. 4, 2023”, 10 pgs. [cited by applicant]
“U.S. Appl. No. 17/035,597, Final Office Action mailed Apr. 17, 2024”, 23 pgs. [cited by applicant]
“U.S. Appl. No. 17/035,597, Response filed Feb. 28, 2024 to Non Final Office Action mailed Aug. 28, 2023”, 10 pgs. [cited by applicant]
“U.S. Appl. No. 17/473,178, Response filed Apr. 11, 2024 to Non Final Office Action mailed Jan. 3, 2024”, 8 pgs. [cited by applicant]
“U.S. Appl. No. 17/826,054, Non Final Office Action mailed Mar. 8, 2024”, 13 pgs. [cited by applicant]
“U.S. Appl. No. 17/874,140, Non Final Office Action mailed Mar. 20, 2024”, 10 pgs. [cited by applicant]
“U.S. Appl. No. 17/984,144, Non Final Office Action mailed Mar. 29, 2024”, 14 pgs. [cited by applicant]
“U.S. Appl. No. 17/985,611, Non Final Office Action mailed Mar. 27, 2024”, 10 pgs. [cited by applicant]
“U.S. Appl. No. 18/093,636, Response filed Apr. 5, 2024 to Restriction Requirement mailed Dec. 20, 2023”, 6 pgs. [cited by applicant]
“Canadian Application Serial No. 3,105,375 Examiners Rule 86 2 Requisition mailed Dec. 28, 2023”, 7 pgs. [cited by applicant]
“Canadian Application Serial No. 3,105,375, Response filed Apr. 26, 2024 to Examiners Rule 86 2 Requisition mailed Dec. 28, 2023”, 27 pgs. [cited by applicant]
“Canadian Application Serial No. 3,192,375, Voluntary Amendment filed Dec. 28, 2023”, 59 pgs. [cited by applicant]
“Chinese Application Serial No. 202180062766.0, Voluntary Amendment filed Nov. 13, 2023”, with English claims, 91 pages. [cited by applicant]
“Chinese Application Serial No. 202311192831.9, Response filed Dec. 28, 2023 to Notification to Make Rectification issued Nov. 1, 2023”, with English claims, 21 pages. [cited by applicant]
“European Application Serial No. 19745460.6, Summons to attend oral proceedings pursuant to Rule 115(1) EPC mailed Jan. 4, 2024”, 6 pgs. [cited by applicant]
“U.S. Appl. No. 17/033,854, Response filed May 28, 2024 to Final Office Action mailed Mar. 28, 2024”, 13 pages. [cited by applicant]
“U.S. Appl. No. 17/033,854, Advisory Action mailed Jun. 5, 2024”, 4 pages. [cited by applicant]
“U.S. Appl. No. 14/268,220, Non-Final Office Action mailed Dec. 1, 2015”, 7 pgs. [cited by applicant]
“U.S. Appl. No. 17/033,854, Examiner Interview Summary mailed Jul. 30, 2024”, 3 pgs. [cited by applicant]
“U.S. Appl. No. 17/033,854, Notice of Allowance mailed Sep. 20, 2024”, 16 pgs. [cited by applicant]
“U.S. Appl. No. 17/033,854, Response filed Aug. 23, 2024 to Advisory Action mailed Jun. 5, 2024”, 17 pgs. [cited by applicant]
“U.S. Appl. No. 17/035,597, Examiner Interview Summary mailed Aug. 22, 2024”, 3 pgs. [cited by applicant]
“U.S. Appl. No. 17/035,597, Non Final Office Action mailed Sep. 6, 2024”, 19 pgs. [cited by applicant]
“U.S. Appl. No. 17/035,597, Response filed Aug. 19, 2024 to Final Office Action mailed Apr. 17, 2024”, 17 pgs. [cited by applicant]
“U.S. Appl. No. 17/035,597, Response filed Sep. 11, 2023 to Non Final Office Action mailed Aug. 28, 2023”, 61 pgs. [cited by applicant]
“U.S. Appl. No. 17/826,054, Examiner Interview Summary mailed Jul. 30, 2024”, 3 pgs. [cited by applicant]
“U.S. Appl. No. 17/826,054, Final Office Action mailed Oct. 18, 2024”, 14 pgs. [cited by applicant]
“U.S. Appl. No. 17/826,054, Response filed Aug. 8, 2024 to Non Final Office Action mailed Mar. 8, 2024”, 13 pgs. [cited by applicant]
“U.S. Appl. No. 17/874,140, Response filed Sep. 16, 2024 to Non Final Office Action mailed Mar. 20, 2024”, 15 pgs. [cited by applicant]
“U.S. Appl. No. 17/957,207, Final Office Action mailed Jun. 12, 2024”, 13 pgs. [cited by applicant]
“U.S. Appl. No. 17/957,207, Response filed Oct. 14, 2024 to Final Office Action mailed Jun. 12, 2024”, 14 pgs. [cited by applicant]
“U.S. Appl. No. 17/984,144, Response filed Sep. 17, 2024 to Non Final Office Action mailed Mar. 29, 2024”, 8 pgs. [cited by applicant]
“U.S. Appl. No. 17/985,611, Response filed Sep. 17, 2024 to Non Final Office Action mailed Mar. 27, 2024”, 12 pgs. [cited by applicant]
“U.S. Appl. No. 18/093,636, Non Final Office Action mailed Jun. 14, 2024”, 14 pgs. [cited by applicant]
“U.S. Appl. No. 18/093,636, Response filed Oct. 14, 2024 to Non Final Office Action mailed Jun. 14, 2024”, 14 pgs. [cited by applicant]
“Application Serial No. PCT/US2023/015228, IPRP mailed Sep. 26, 2024”, 11 pgs. [cited by applicant]
“Application Serial No. PCT/US2023/015228, Written Opinion mailed Jun. 15, 2023”, 6 pgs. [cited by applicant]
“Canadian Application No. 3155420, Examiners Rule 862 Requisition Report Consolidated Correspondence Jul. 20, 2023”, 5 pgs. [cited by applicant]
“Canadian Application No. 3155420, Examiners Rule mailed May 11, 2023”, 4 pgs. [cited by applicant]
“Canadian Application Serial No. 3,155,420, Examiners Rule 862 Requisition Report Apr. 18, 2024”, 3 pgs. [cited by applicant]
“Canadian Application Serial No. 3,155,420, Response filed Aug. 13, 2024 to Examiners Rule 862 Requisition Report Apr. 18, 2024”, 10 pgs. [cited by applicant]
“European Application Serial No. 19745460.6, Response filed Jun. 20, 2024 to Summons to attend oral proceedings pursuant to Rule 115(1) EPC mailed Jan. 4, 2024”, 12 pgs. [cited by applicant]
“European Application Serial No. 20869757, Extended European Search Report mailed Sep. 19, 2023”, 10 pgs. [cited by applicant]
“European Application Serial No. 20869757, Response filed Apr. 12, 2024 to Extended European Search Report mailed Sep. 19, 2023”, 13 pgs. [cited by applicant]
“European Application Serial No. 20869757.3, Communication Pursuant to Article 94(3) EPC mailed Sep. 4, 2024”, 6 pgs. [cited by applicant]
“European Application Serial No. 21867741.7, Extended European Search Report mailed Aug. 12, 2024”, 8 pgs. [cited by applicant]
“International Application Serial No. PCT/US2020/05168 International Search Report mailed Feb. 8, 2021”, 5 pgs. [cited by applicant]
“International Application Serial No. PCT/US2020/05168 Written Opinion mailed Feb. 8, 2021”, 6 pgs. [cited by applicant]
“International Application Serial No. PCT/US2020/053168, International Preliminary Report on Patentability mailed Apr. 7, 2022”, 8 pgs. [cited by applicant]
“International Application Serial No. PCT/US2021/050022, International Preliminary Report on Patentability mailed Dec. 1, 2022”, 17 pgs. [cited by applicant]
“International Application Serial No. PCT/US2021/050022, International Search Report mailed Feb. 3, 2022”, 5 pgs. [cited by applicant]
“International Application Serial No. PCT/US2021/050022, Written Opinion mailed Feb. 3, 2022”, 6 pgs. [cited by applicant]
“International Application Serial No. PCT/US2023/015228, International Search Report mailed Jun. 15, 2023”, 5 pgs. [cited by applicant]
“JP 2004-174563 Translation from FIT database”, (Year: 2024), 22 pgs. [cited by applicant]
“U.S. Appl. No. 17/957,207, Response filed Nov. 8, 2024 to Advisory Action mailed Oct. 31, 2024 and Final Office Action mailed Jun. 12, 2024”, 16 pgs. [cited by applicant]
“U.S. Appl. No. 17/957,207, Advisory Action mailed Oct. 31, 2024”, 3 pgs. [cited by applicant]
“Canadian Application Serial No. 3,105,375, Examiners Rule 86(2) Report mailed Nov. 6, 2024”, 9 pgs. [cited by applicant]
“U.S. Appl. No. 17/874,140, Final Office Action mailed Nov. 15, 2024”, 11 pgs. [cited by applicant]
“U.S. Appl. No. 17/035,597, Response filed Feb. 6, 2025 to Non Final Office Action mailed Sep. 6, 2024”, 8 pgs. [cited by applicant]
“U.S. Appl. No. 17/826,054, Response filed Jan. 6, 2025 to Final Office Action mailed Oct. 18, 2024”, 9 pgs. [cited by applicant]
“U.S. Appl. No. 17/984,144, Notice of Allowance mailed Nov. 26, 2024”, 11 pgs. [cited by applicant]
“U.S. Appl. No. 17/985,611, Final Office Action mailed Dec. 5, 2024”, 15 pgs. [cited by applicant]
“U.S. Appl. No. 18/093,636, Final Office Action mailed Jan. 13, 2025”, 12 pgs. [cited by applicant]
“European Application Serial No. 20869757.3, Response filed Jan. 3, 2025 to Communication Pursuant to Article 94(3) EPC mailed Sep. 4, 2024”, 10 pgs. [cited by applicant]
“JP-2002361320-A Translation provided by FIT database”, Retrieved from Patent Center, (Year: 2025), 8 pages. [cited by applicant]
X, Li, et al., “CN-105925846-B translation provided by FIT database (Year: 2024)”, (Feb. 23, 2018), 12 pgs. [cited by applicant]