IP Library Granted Patent US 11,667,062
Granted Patent B2
US 11,667,062 · App. 17/492,862 · Granted Jun 6, 2023

Nanostructures from laser-ablated nanohole templates

Inventors: William Hudson Hofmeister (Nashville, TN); Alexander Yuryevich Terekhov (Murfreesboro, TN); Jose Lino Vasconcelos da Costa (Tullahoma, TN); Kathleen Stacia Lansford (Manchester, TN); Deepak Rajput (Tullahoma, TN); Lloyd M. Davis (Tullahoma, TN)
Assignee: ULTRA SMALL FIBERS, LLC
B29C41/003B29C33/3842B29C41/02B29C41/38B29C41/42B82Y10/00B82Y40/00C08B3/06C08B5/02C08F110/02C08F120/18C08F120/40C08G63/08C08G63/664C08G77/04G03F7/0002B29K2001/12B29K2001/18B29K2023/06B29K2031/04B29K2033/12B29K2067/04B29K2071/00B29K2083/00B29K2901/10B29K2901/12B29K2907/045B29K2909/00B29K2909/08B29K2909/14B29K2995/0026B29K2995/0094B29L2031/7562Y02P20/582Y10T428/24355Y10T428/24802
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Quick Facts
Patent No.
US 11,667,062
App. No.
17/492,862
Granted
Jun 6, 2023
Kind
B2
Abstract

Solution casting a nanostructure. Preparing a template by ablating nanoholes in a substrate using single-femtosecond laser machining. Replicating the nanoholes by applying a solution of a polymer and a solvent into the template. After the solvent has substantially dissipated, removing the replica from the substrate.

Claims (29)

1. A method for fabricating a nanofiber array, comprising:

providing a template comprising a transparent substrate having a surface, the surface comprising a plurality of nanoholes, each nanohole of the plurality being ablated in the surface using a laser;

applying a flowable polymer into the plurality of nanoholes; and

extracting an array of polymer nanofibers from the template;

wherein the nanofibers have an aspect ratio of at least ten-to-one and a diameter of less than 1000 nanometers.

2. The method of claim 1 , wherein the flowable polymer includes a polymer capable of forming a continuous film.

3. The method of claim 1 , wherein the flowable polymer does not contain a solvent.

4. The method of claim 1 , wherein the flowable polymer is a polymer resin.

5. The method of claim 1 , wherein the flowable polymer overflows the plurality of nanoholes and covers at least a portion of the surface of the template such that the flowable polymer connects at least some of the plurality of nanoholes.

6. The method of claim 1 , wherein said extracting is lifting or peeling the array of polymer nanofibers away from the surface of the template.

7. The method of claim 1 , wherein the nanofibers are not hollow or porous.

8. The method of claim 1 , wherein the array comprises a plurality of freestanding polymer nanofibers extending from a surface of a polymer substrate.

9. The method of claim 8 , wherein the polymer nanofibers are positioned on the polymer substrate in a non-random, user-defined pattern.

10. The method of claim 1 , further comprising treating the surface of the template with a material to modify the surface and bonding characteristics associated with the template and the array.

11. The method of claim 1 , further comprising applying a fluorocarbon-based antistick coating to the template prior to applying the flowable polymer into the plurality of nanoholes.

12. A method for fabricating a nanofiber array, comprising:

providing a template comprising a transparent substrate having a surface, the surface comprising a plurality of nanoholes, each nanohole of the plurality being ablated in the surface using a laser;

filling the plurality of nanoholes with a polymer resin; and

lifting or peeling an array of polymer nanofibers away from the surface of the template;

wherein the nanofibers have an aspect ratio of at least ten-to-one and a diameter of less than 1000 nanometers.

13. The method of claim 12 , wherein the nanofibers have an average length greater than ten micrometers.

14. The method of claim 12 , wherein the nanofibers have an aspect ratio of greater than twenty-five-to-one.

15. The method of claim 12 , wherein the nanofibers have an average length greater than 25 micrometers.

16. A method for fabricating an array of nanofibers, comprising:

providing a template having a surface comprising a plurality of nanoholes, each nanohole of the plurality being ablated in the surface using a laser;

applying a flowable polymer capable of forming a continuous film into the nanoholes until the flowable polymer covers at least a portion of the surface of the template and connects at least some of the plurality of nanoholes;

allowing the flowable polymer to form the continuous film on the portion of the surface of the template; and

removing the continuous film from the surface of the template;

wherein the continuous film comprises an array of nanofibers having an aspect ratio of at least ten-to-one and a diameter of less than 1000 nanometers.

Assignments (2)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Oct 4, 2021
From: HOFMEISTER, WILLIAM HUDSON; TEREKHOV, ALEXANDER YURYEVICH; DA COSTA, JOSE LINO VASCONCELOS; LANSFORD, KATHLEEN STACIA; RAJPUT, DEEPAK; DAVIS, LLOYD M.
To: UNIVERSITY OF TENNESSEE RESEARCH FOUNDATION
Reel/Frame 057687/0272 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Oct 4, 2021
From: UNIVERSITY OF TENNESSEE RESEARCH FOUNDATION
To: ULTRA SMALL FIBERS, LLC
Reel/Frame 057687/0352 →
Continuity (4)
Continuation 14560833 · Dec 4, 2014
Continuation 13769575 · Feb 18, 2013
Provisional Application 61599926 · Feb 16, 2012
Related Publication 20220024084A1 · Jan 27, 2022