IP Library › Granted Patent US 11,532,478
Granted Patent B2
US 11,532,478 · App. 17/520,830 · Granted Dec 20, 2022

GaN devices with ion implanted ohmic contacts and method of fabricating devices incorporating the same

Inventors: Travis J. Anderson (Alexandria, VA); James C. Gallagher (Alexandria, VA); Marko J. Tadjer (Vienna, VA); Alan G. Jacobs (Arlington, VA); Boris N. Feigelson (Springfield, VA)
Assignee: The Government of the United States of America, as represented by the Secretary of the Navy
H01L21/26546H01L21/266H01L21/28575H01L21/3245H01L29/2003H01L29/207H01L29/36H01L29/452
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Quick Facts
Patent No.
US 11,532,478
App. No.
17/520,830
Granted
Dec 20, 2022
Kind
B2
Abstract

A method for activating implanted dopants and repairing damage to dopant-implanted GaN to form n-type or p-type GaN. A GaN substrate is implanted with n- or p-type ions and is subjected to a high-temperature anneal to activate the implanted dopants and to produce planar n- or p-type doped areas within the GaN having an activated dopant concentration of about 10 18 -10 22 cm −3 . An initial annealing at a temperature at which the GaN is stable at a predetermined process temperature for a predetermined time can be conducted before the high-temperature anneal. A thermally stable cap can be applied to the GaN substrate to suppress nitrogen evolution from the GaN surface during the high-temperature annealing step. The high-temperature annealing can be conducted under N 2 pressure to increase the stability of the GaN. The annealing can be conducted using laser annealing or rapid thermal annealing (RTA).

Claims (30)

1. A method for selectively forming at least one p-doped region in an epitaxial GaN substrate, the method including the steps of:

selectively applying a mask to a predetermined region of the GaN substrate;

implanting p-type dopant ions into at least one predetermined unmasked region of the GaN substrate to form an p-implanted GaN substrate;

removing the mask from the p-implanted GaN substrate;

subjecting the p-implanted GaN substrate to an initial annealing at a predetermined temperature at which the GaN is stable at a predetermined process temperature for a predetermined time of a few seconds to several hours;

subjecting the p-implanted GaN substrate to a high-temperature annealing at a predetermined temperature between 1200 and 1600° C. for a predetermined time between a few seconds and a few hours and at a predetermined pressure between about 1 atm and about 100 bar to activate the implanted p-dopant ions and to produce at least one electrically activated doped region within the GaN;

wherein the electrically activated p-doped region is planar to an upper surface of the epitaxial GaN substrate and has a concentration of activated implanted p-type dopant ions of about 10 18 cm −3 to about 10 22 cm −3 .

2. The method according to claim 1 , wherein the initial annealing is conducted at a temperature of about 850° C. for several hours at atmospheric pressure.

3. The method according to claim 1 , wherein the first annealing is conducted at a temperature between about 850° C. and about 1050° C. for a few minutes at atmospheric pressure.

4. The method according to claim 1 , further including applying a thermally protective cap to an upper surface of the p-implanted GaN before annealing, the cap being configured to suppress evolution of nitrogen from the GaN during annealing.

5. The method according to claim 1 , further including applying a nitrogen overpressure of up to about 100 bar during the high-temperature annealing to further stabilize the GaN.

6. The method according to claim 1 , wherein the high-temperature annealing is conducted by means of laser annealing or rapid thermal annealing (RTA).

7. The method according to claim 1 , wherein the p-dopant ions comprise Mg or Be.

8. A method for selectively forming at least one p-doped region in an epitaxial GaN material layer, the method including the steps of:

selectively applying a mask to a predetermined region of the GaN material layer;

implanting p-type dopant ions into at least one predetermined unmasked region of the GaN material layer to form an p-implanted GaN material layer;

removing the mask from the p-implanted GaN material layer;

subjecting the p-implanted GaN material layer to an initial annealing at a predetermined temperature at which the GaN is stable at a predetermined process temperature for a predetermined time of a few seconds to several hours;

subjecting the p-implanted GaN material layer to a high-temperature annealing at a predetermined temperature between 1200 and 1600° C. for a predetermined time between a few seconds and a few hours and at a predetermined pressure between about 1 atm and about 100 bar to activate the implanted p-dopant ions and to produce at least one electrically activated doped region within the GaN;

wherein the electrically activated p-doped region is planar to an upper surface of the epitaxial GaN material layer and has a concentration of activated implanted p-type dopant ions of about 10 18 cm −3 to about 10 22 cm −3 .

9. The method according to claim 8 , wherein the GaN material layer comprises unintentionally doped GaN, semi-insulating GaN, carbon-doped GaN, or a GaN-containing heterostructure.

10. The method according to claim 8 , wherein the GaN material layer comprises an AlGaN/GaN heterostructure.

11. The method according to claim 8 , wherein the GaN material layer comprises a GaN substrate.

12. The method according to claim 8 , wherein the GaN material layer is situated on a substrate comprising GaN, SiC, Si, sapphire, or an engineered composite.

13. The method according to claim 8 , wherein the initial annealing is conducted at a temperature of about 850° C. for several hours at atmospheric pressure.

14. The method according to claim 8 , wherein the first annealing is conducted at a temperature between about 850° C. and about 1050° C. for a few minutes at atmospheric pressure.

15. The method according to claim 8 , further including applying a thermally protective cap to an upper surface of the p-implanted GaN material layer before annealing, the cap being configured to suppress evolution of nitrogen from the GaN material layer during annealing.

16. The method according to claim 8 , further including applying a nitrogen overpressure of up to about 100 bar during the high-temperature annealing to further stabilize the GaN material layer.

17. The method according to claim 8 , wherein the high-temperature annealing is conducted by means of laser annealing or rapid thermal annealing (RTA).

18. The method according to claim 8 , wherein the p-dopant ions comprise Mg or Be.

Assignments (1)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Nov 8, 2021
From: ANDERSON, TRAVIS J.; FEIGELSON, BORIS N.; GALLAGHER, JAMES C.; TADJER, MARKO J.; JACOBS, ALAN G.
To: THE GOVERNMENT OF THE UNITED STATES OF AMERICA, AS REPRESENTED BY THE SECRETARY OF THE NAVY
Reel/Frame 058042/0507 →
Continuity (3)
Division 16927061 · Jul 13, 2020
Provisional Application 62878766 · Jul 26, 2019
Related Publication 20220059353A1 · Feb 24, 2022
Cited By (1)
US 12,598,927