IP Library Granted Patent US 11,850,546
Granted Patent B2
US 11,850,546 · App. 17/591,991 · Granted Dec 26, 2023

Process for separation of hydrogen and oxygen

Inventors: Abdulaziz M. Al-Jodai (Riyadh, SA); Nasser Ali Aldalaan (Riyadh, SA); Mubarik Ali Bashir (Riyadh, SA)
Assignee: SABIC GLOBAL TECHNOLOGIES B.V.
B01D53/0476C01B3/042C01B3/508C01B13/027C01B13/0266B01D2253/102B01D2253/108B01D2253/112B01D2256/12B01D2256/16C01B2203/042C01B2203/1288C01B2210/0017C01B2210/0018C01B2210/0042C01B2210/0062
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Quick Facts
Patent No.
US 11,850,546
App. No.
17/591,991
Granted
Dec 26, 2023
Kind
B2
Abstract

Embodiments of the invention are directed to methods, processes, and systems for safely and reliably purifying hydrogen from a gas mixture containing hydrogen and oxygen.

Claims (26)

1. A process for separating hydrogen and oxygen from a gas mixture comprising:

separating the hydrogen and the oxygen at about atmospheric pressure by passing the feed source through an adsorption medium comprising a carbon molecular sieve that selectively adsorbs hydrogen from the feed source producing an enriched oxygen product gas and an adsorption medium enriched in hydrogen; and

desorbing the adsorbed hydrogen by exposing the hydrogen enriched adsorption medium to a vacuum forming a hydrogen enriched purge gas and a regenerated adsorption medium.

2. A process for separating hydrogen and oxygen comprising:

providing a gas mixture feed comprising oxygen and hydrogen;

passing the gas mixture feed through an adsorption medium that selectively adsorbs hydrogen from the gas mixture feed producing a hydrogen enriched adsorption medium;

desorbing the adsorbed hydrogen by exposing the hydrogen enriched adsorption medium to a vacuum forming a hydrogen enriched purge gas and a regenerated adsorption medium, and

injecting a hydrogen product gas to the gas mixture feed.

3. The process of claim 1 , wherein the adsorption medium further comprises a zeolite.

4. The process of claim 1 , wherein the adsorption process is performed at 15 to 60° C.

5. The process of claim 1 , wherein the desorption process is performed at about 15 to 60° C.

6. The process of claim 1 , wherein the adsorption process is performed at a pressure of about 0.8 to 1.2 bar.

7. The process of claim 1 , wherein the adsorption selectively adsorbs hydrogen at about atmospheric pressure and desorbs hydrogen at a pressure below 0.5 bar.

8. The process of claim 1 , wherein the adsorption medium further comprises a zeolite.

9. The process of claim 8 , wherein the zeolite is a 5 angstrom zeolite.

10. The process of claim 1 , wherein the adsorption medium further comprises a binder.

11. The process of claim 8 , wherein the adsorption medium further comprises a binder.

12. The process of claim 2 , wherein the adsorption medium comprises a zeolite.

13. The process of claim 2 , wherein the adsorption process is performed at 15 to 60° C.

14. The process of claim 2 , wherein the desorption process is performed at about 15 to 60° C.

15. The process of claim 2 , wherein the adsorption process is performed at a pressure of about 0.8 to 1.2 bar.

16. The process of claim 2 , wherein the adsorption selectively adsorbs hydrogen at about atmospheric pressure and desorbs hydrogen at a pressure below 0.5 bar.

17. The process of claim 14 , wherein the adsorption medium comprises a zeolite.

18. The process of claim 17 , wherein the zeolite is a 5 angstrom zeolite.

19. The process of claim 2 , wherein the adsorption medium further comprises a binder.

20. The process of claim 2 , wherein the desorption process is performed at about 60° C.

Assignments (3)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Apr 16, 2024
From: SAUDI BASIC INDUSTRIES CORPORATION
To: SABIC AGRI-NUTRIENTS COMPANY
Reel/Frame 067128/0216 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Apr 2, 2024
From: SABIC GLOBAL TECHNOLOGIES B.V.
To: SAUDI BASIC INDUSTRIES CORPORATION
Reel/Frame 066986/0030 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Feb 3, 2022
From: AL-JODAI, ABDULAZIZ M.; ALDALAAN, NASSER ALI; BASHIR, MUBARIK ALI
To: SABIC GLOBAL TECHNOLOGIES B.V.
Reel/Frame 058878/0771 →
Continuity (3)
Continuation 16073139
Provisional Application 62290136 · Feb 2, 2016
Related Publication 20220152548A1 · May 19, 2022