IP Library Granted Patent US 11,932,820
Granted Patent B2
US 11,932,820 · App. 17/605,320 · Granted Mar 19, 2024

Lubricating oil composition and method for producing lubricating oil composition

Inventors: Ryuji Monden (Tokyo, JP); Kunio Kondo (Tokyo, JP)
Assignees: Resonac Corporation; MITSUBISHI CORPORATION
C10M125/02C10M101/02C10M177/00C10M2201/041C10M2203/1006C10N2070/00
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Quick Facts
Patent No.
US 11,932,820
App. No.
17/605,320
Granted
Mar 19, 2024
Kind
B2
Abstract

A method for producing a lubricating oil composition of the present embodiment includes an irradiation step of irradiating a fullerene solution in which fullerenes are dissolved in a base oil with radiation, in which the above-described radiation is ultraviolet light or ionizing radiation.

Claims (37)

1. A method for producing a lubricating oil composition, comprising:

an irradiation step of irradiating a fullerene solution in which fullerenes are dissolved in a base oil with radiation to produce fullerene adducts,

wherein the radiation is ultraviolet light.

2. The method for producing a lubricating oil composition according to claim 1 , further comprising:

a removal step of removing an insoluble component from the fullerene solution.

3. The method for producing a lubricating oil composition according to claim 1 ,

wherein, in the irradiation step, the radiation is emitted in a non-oxidizing atmosphere.

4. The method for producing a lubricating oil composition according to claim 3 ,

wherein the radiation is emitted while setting an oxygen gas concentration in the fullerene solution to 10 mass ppm or less.

5. The method for producing a lubricating oil composition according to claim 1 ,

wherein the ultraviolet light has a wavelength of 190 nm to 365 nm.

6. The method for producing a lubricating oil composition according to claim 1 ,

wherein the radiation is emitted until a ratio of a concentration of the fullerenes in the fullerene solution after the irradiation step to a concentration of the fullerenes in the fullerene solution before the irradiation step is 0.1 to 0.7.

7. The method for producing a lubricating oil composition according to claim 1 ,

wherein the fullerenes include C 60 or C 70 or a mixture thereof.

8. The method for producing a lubricating oil composition according to claim 1 ,

wherein, in the irradiation step, the radiation is emitted while controlling a temperature of the fullerene solution such that it is 40° C. to 200° C.

9. The method for producing a lubricating oil composition according to claim 1 ,

wherein, in the irradiation step, the radiation is emitted 2 to 9 times.

10. The method for producing a lubricating oil composition according to claim 1 ,

wherein, in the irradiation step, the fullerene solution is accommodated in a container, and

wherein, in the irradiation step, the radiation is emitted from outside of the container.

11. The method for producing a lubricating oil composition according to claim 1 ,

wherein, in the irradiation step, 1 g of the fullerene solution is irradiated with the radiation at an irradiation energy of 1 J to 100 J.

12. A lubricating oil composition comprising:

a base oil; and

fullerene adducts,

wherein added groups of the fullerene adducts have a part of a molecular structure constituting the base oil, and

wherein the base oil is selected from a mineral oil, diesters, polyalkylene glycols, polyalkyl vinyl ether, polybutene, isoparaffin, olefin copolymers, alkylbenzene, alkylnaphthalene, diisodecyl adipate, monoesters, dibasic acid esters, tribasic acid esters, polyol esters, dialkyl diphenyl ethers, alkyl diphenyl sulfide, polyphenyl ethers, silicone lubricating oils, and perfluoropolyether.

13. The method for producing a lubricating oil composition according to claim 1 ,

wherein the radiation is emitted until a ratio of a concentration of the fullerenes in the fullerene solution after the irradiation step to a concentration of the fullerenes in the fullerene solution before the irradiation step is 0.03 to 0.88.

14. The lubricating oil according to claim 12 ,

wherein the base oil is a mineral oil.

15. The lubricating oil according to claim 12 ,

wherein the base oil is a mineral oil selected from a paraffinic base oil and a naphthenic base oil.

16. The lubricating oil according to claim 12 ,

wherein the base oil is selected from diesters, polyol esters, polyalkylene glycols, and polyalkyl vinyl ethers.

Assignments (5)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded May 16, 2024
From: RESONAC CORPORATION
To: MITSUBISHI CORPORATION
Reel/Frame 067434/0947 →
CHANGE OF ADDRESS Recorded Nov 7, 2023
From: RESONAC CORPORATION
To: RESONAC CORPORATION
Reel/Frame 065488/0797 →
PARTIAL ASSIGNMENT Recorded Nov 7, 2023
From: RESONAC CORPORATION
To: MITSUBISHI CORPORATION
Reel/Frame 065488/0893 →
CHANGE OF NAME Recorded Jun 23, 2023
From: SHOWA DENKO K.K.
To: RESONAC CORPORATION
Reel/Frame 064082/0513 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Oct 21, 2021
From: MONDEN, RYUJI; KONDO, KUNIO
To: SHOWA DENKO K.K.
Reel/Frame 057886/0310 →
Priority Claims (1)
JP 2019-083393 · Apr 24, 2019 · national
Continuity (1)
Related Publication 20220186136A1 · Jun 16, 2022