IP Library › Granted Patent US 12,011,440
Granted Patent B2
US 12,011,440 · App. 17/656,149 · Granted Jun 18, 2024

Ready-to-administer hydromorphone formulations

Inventors: Andrew Conrad (Bedford, OH); Bernadette Colvard (Bedford, OH)
Assignee: Hikma Pharmaceuticals USA Inc.
A61K31/485A61K9/0019A61K47/02
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Quick Facts
Patent No.
US 12,011,440
App. No.
17/656,149
Granted
Jun 18, 2024
Kind
B2
Abstract

The present disclosure relates to a ready-to-administer (RTA), intravenous (IV) bag presentation for hydromorphone. In particular, the present disclosure relates to terminally sterilized liquid formulations comprising hydromorphone hydrochloride in sodium chloride packaged in an RTA IV bag. The present disclosure also relates to methods of treating patients by administration of such formulations and RTA IV bags containing such formulations.

Claims (33)

1. A ready-to-administer parenteral liquid formulation comprising:

(a) 0.2 mg/mL of hydromorphone hydrochloride;

(b) 9 mg/mL of sodium chloride;

(c) 0.23 mg/mL of sodium citrate dihydrate; and

(d) 0.22 mg/mL of citric acid monohydrate;

wherein the liquid formulation has a pH of 3.5 to 4.2,

wherein the liquid formulation has been terminally sterilized in a polymeric infusion container, wherein terminal sterilization is characterized by an F 0 value from 5 to 15, and

wherein the liquid formulation is stable for at least 6 months when stored in the polymeric infusion container at 25° C.±2° C. and not more than 40% RH.

2. The liquid formulation of claim 1 , wherein the liquid formulation has a pH of 3.6 to 3.8.

3. The liquid formulation of claim 1 , further comprising a pH adjusting agent.

4. The liquid formulation of claim 1 , wherein the liquid formulation retains at least 95% w/w of the hydromorphone hydrocholoride and has not more than 5% w/w of hydromorphone degradation products after storage at 25° C.±2° C. and not more than 40% RH for at least 6 months.

5. The liquid formulation of claim 1 , wherein the liquid formulation retains at least 98% w/w of the hydromorphone hydrocholoride and has not more than 2% w/w of hydromorphone degradation products after storage at 25° C.±2° C. and not more than 40% RH for at least 6 months.

6. A method of treating a patient in need of management of pain comprising parenterally administering to the patient the liquid formulation of claim 1 .

7. A polymeric infusion container filled with the liquid formulation of claim 1 .

8. The liquid formulation of claim 1 , wherein the liquid formulation has been terminally sterilized by autoclave.

9. The liquid formulation of claim 1 , wherein the polymeric infusion container is an intravenous infusion bag.

10. The liquid formulation of claim 9 , wherein the intravenous infusion bag comprises one or more ports.

11. An intravenous infusion bag filled with at least 50 mL of the liquid formulation of claim 1 .

12. An intravenous infusion bag filled with at least 50 mL of a ready-to-administer, sterile, parenteral liquid formulation, the ready-to-administer, sterile, parenteral liquid formulation comprising:

(a) 0.2 mg/mL of hydromorphone hydrochloride;

(b) 9 mg/mL of sodium chloride;

(c) 0.23 mg/mL of sodium citrate dihydrate; and

(d) 0.22 mg/mL of citric acid monohydrate;

wherein the liquid formulation has a pH of 3.5 to 4.2,

wherein the liquid formulation has an osmolality of from about 285 mOsmol/kg to about 310 mOsmol/kg,

wherein the liquid formulation has been terminally sterilized in the intravenous infusion bag, wherein terminal sterilization is characterized by an F 0 value from 5 to 15, and

wherein the liquid formulation is stable for at least 6 months when stored at 25° C.±2° C. and not more than 40% RH.

13. The liquid formulation of claim 1 , wherein terminal sterilization is carried out at a temperature ranging from 115° C. to 130° C.

14. The intravenous infusion bag of claim 12 , wherein the liquid formulation has a pH of 3.6 to 3.8.

15. The intravenous infusion bag of claim 12 , wherein the liquid formulation has been terminally sterilized by autoclave.

16. The intravenous infusion bag of claim 12 , wherein the intravenous infusion bag comprises one or more ports.

17. The intravenous infusion bag of claim 12 , wherein terminal sterilization is carried out at a temperature ranging from 115° C. to 130° C.

18. The method of claim 6 , wherein the pain is moderate to severe pain due to surgery, cancer, trauma (soft tissue and bone), biliary colic, myocardial infarction, burns, or renal colic.

Assignments (1)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Mar 30, 2022
From: CONRAD, ANDREW; COLVARD, BERNADETTE
To: HIKMA PHARMACEUTICALS USA INC.
Reel/Frame 059448/0549 →
Continuity (1)
Related Publication 20230301986A1 · Sep 28, 2023
Cited By (1)
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