Solidifying liquid anionic surfactants
The invention relates to solidification of liquid anionic surfactants with a binder, carrier, or both binder and carrier to form a solidified surfactant composition. In particular, the invention relates to solidification of liquid surfactants utilizing drying device(s), wherein the feed composition contains at least one liquid surfactant and the binder, carrier, or binder and carrier to form a solidified surfactant composition. The solidified surfactant compositions can be useful in various cleaning compositions.
1. A method of preparing a solidified surfactant composition comprising:
adding to a drying device:
a liquid anionic surfactant comprising a sodium lauryl ether sulfate surfactant;
a solid binder comprising a polyethylene glycol (PEG); wherein the solid binder is dissolved with the liquid surfactant in a ratio of between about 4:1 to about 1:60 by actives, and
a solid carrier comprising an alpha olefin sulfonate, wherein the carrier and the liquid surfactant are in a ratio of between about 5:1 to about 1:30 by actives;
drying the liquid surfactant and binder and solid carrier to form a solidified surfactant composition;
wherein the drying device comprises a fluidized bed; and
wherein the liquid surfactant is solidified in the solidified surfactant composition, and wherein the solidified surfactant composition has less than about 5 wt-% water.
2. The method of claim 1 , wherein the binder is a PEG having a melting point of at least about 40° C.
3. The method of claim 1 , wherein the binder is PEG 1450, PEG 3350, PEG 4000, PEG 4600, PEG 8000, or combination thereof.
4. The method of claim 1 , wherein the carrier and the liquid surfactant are in a ratio of between about 2:1 and about 1:20 actives.
5. The method of claim 1 , wherein the method employs an agglomerating process.
6. The method of claim 1 , wherein the method employs a granulating process.
7. The method of claim 1 , wherein the solidified surfactant composition contains at least about 10 wt. % active surfactants.
8. The method of claim 1 , wherein the drying process is performed in a batch system.
9. The method of claim 1 , wherein the drying process is performed in a continuous system.
10. The method of claim 1 , wherein there are at least two drying devices placed in series or in parallel.
11. The method of claim 1 , wherein the fluidized bed has an air velocity between about 1 and about 100 feet per second.
12. The method of claim 1 , wherein the fluidized bed has a liquid flow rate between about 0.001 and about 0.15 lb/min of pounds of bed material.
13. The method of claim 1 , wherein the fluidized bed has an atomizing air pressure between about from 0 psig and about 100 psig per nozzle.
14. The method of claim 1 , wherein the carrier has a water solubility of about 0.2 g/L or more at 20° C.
15. The method of claim 1 , wherein the solidified surfactant composition has less than about 2 wt-% water.