IP Library › Granted Patent US 12,630,460
Granted Patent B2
US 12,630,460 · App. 17/683,792 · Granted May 19, 2026

High alumina low soda glass compositions

Inventors: John Rich (Allison Park, PA); Alan Miller (Gibsonia, PA); José Guadalupe Cid-Aguilar (Monterrey, MX)
Assignee: Vitro Flat Glass LLC
C03C3/087C03C3/078C03C4/085C03C2203/10
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Quick Facts
Patent No.
US 12,630,460
App. No.
17/683,792
Granted
May 19, 2026
Kind
B2
Abstract

A glass composition includes a base glass portion comprising: 65-75 wt % SiO 2 ; 5-15 wt % CaO; 0-5 wt % MgO; 0-5 wt % K 2 O; 10-14 wt % Na 2 O; and 1-5 wt % Al 2 O 3 ; wherein the glass composition has a ratio of Na 2 O to Al 2 O 3 is in the range of 9.5-12.5 wt %/wt %.

Claims (46)

1 . A glass composition comprising:

a base glass portion comprising:

65-75 wt % SiO 2 ;

5-9.5 wt % CaO;

2.6-5 wt % MgO;

0-5 wt % K 2 O;

10-14 wt % Na 2 O; and

0.8-1.47 wt % Al 2 O 3 ; and

a colorant portion comprising:

30 to 120 ppm of CoO; and

no more than 7.5 ppm selenium,

wherein the glass composition has a ratio of Na 2 O to Al 2 O 3 in the range of 10.0-11.5 wt. %/wt.%, wherein the glass composition has a ratio of CaO to MgO in the range of 1.7 to 1.9 wt. %/wt.%, wherein the glass composition has an iron redox ratio in the range of 0.221-0.311, wherein the total iron in the glass composition is in the range of 0.01 to 0.30 wt. %, and wherein a glass sheet formed from the glass composition has an a* in the range of −3 to +1 and a b* in the range of −2 to −12.

2 . The glass composition of claim 1 , wherein the base glass portion comprises 0.1-0.5 wt % K 2 O.

3 . The glass composition of claim 1 , wherein the base glass portion comprises:

68-74 wt % SiO 2 ;

13-13.5 wt % Na 2 O;

1-1.4 wt % Al 2 O 3 ;

8.1-8.6 wt % CaO; and

4.5-5 wt % MgO.

4 . The glass composition of claim 1 , wherein the glass sheet has an a* in the range of −2.5 to 0 and a b* in the range of −4 to −9.

5 . The glass composition of claim 1 , wherein the glass sheet has a visible light transmittance of no greater than 80%.

6 . The glass composition of claim 1 , wherein the colorant portion comprises selenium in an amount from greater than 0 ppm to 3 ppm.

7 . The glass composition of claim 1 , wherein a colorant portion comprises at least one of the following oxides of manganese, tin, cerium, molybdenum, vanadium, copper, zinc, tungsten, and lanthanum, or any combination thereof.

8 . The glass composition of claim 1 , wherein the glass composition comprises 0.16-0.18 wt. % Fe 2 O 3 .

9 . A glass composition comprising:

a base glass portion comprising:

71.2-71.6 wt. % SiO 2 ;

8.3-8.6 wt. % CaO;

5.0-5.2 wt. % MgO;

0.24-0.25 wt. % K 2 O;

13.4-13.5 wt. % Na 2 O; and

1.1-1.2 wt. % Al 2 O 3 ; and

a colorant portion comprising:

30 to 120 ppm of CoO; and

no more than 7.5 ppm selenium,

wherein the glass composition has a ratio of Na 2 O to Al 2 O 3 in the range of 11.17-12.27 wt. %/wt.%, wherein the glass composition has an iron redox ratio in the range of 0.221-0.311, wherein the total iron in the glass composition is in the range of 0.01 to 0.30 wt. %, and wherein a glass sheet formed from the glass composition has an a* in the range of −2.5 to 0 and a b* in the range of −5 to −9.

10 . The glass composition of claim 9 , wherein the glass composition comprises 0.20-0.21 wt. % Fe 2 O 3 .

11 . The glass composition of claim 9 , wherein the ratio of CaO to MgO is 1.7 to 1.9 wt. %/wt.%.

12 . A method of producing a glass sheet comprising:

feeding raw batch materials into a container;

melting the raw batch materials in the container to form a molten glass composition;

passing the molten glass composition from the container into a pool of a molten metal such that the molten glass composition floats in the pool of molten metal;

forming the molten glass composition into a shape of a flat glass sheet on the pool of molten metal; and

cooling the molten glass composition to form the flat glass sheet, wherein the flat glass sheet comprises the glass composition of claim 1 .

13 . The glass composition of claim 1 , wherein the glass composition has a ratio of Na 2 O to Al 2 O 3 in the range of 10.5-11.0 wt. %/wt.%, and wherein the glass sheet formed from the glass composition has an a* in the range of −2.5 to 0 and a b* in the range of −4 to −9.

14 . The glass composition of claim 1 , wherein the glass composition has a ratio of Na 2 O to Al 2 O 3 in the range of 10.55-10.90 wt. %/wt.%, and wherein the glass sheet formed from the glass composition has an a* in the range of −1.8 to −0.5 and a b* in the range of −5 to −8.

Assignments (2)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Aug 4, 2022
From: CID-AGUILAR, JOSÉ GUADALUPE
To: VITRO FLAT GLASS LLC
Reel/Frame 060722/0936 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Mar 1, 2022
From: RICH, JOHN; MILLER, ALAN
To: VITRO FLAT GLASS LLC
Reel/Frame 059134/0918 →
Continuity (3)
Division 16452835 · Jun 26, 2019
Provisional Application 62690663 · Jun 27, 2018
Related Publication 20220298056A1 · Sep 22, 2022
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