IP Library Granted Patent US 12,341,227
Granted Patent B2
US 12,341,227 · App. 17/739,227 · Granted Jun 24, 2025

Perfluorosulfonyl monomers suitable for fluoropolymers and fuel cell membrane articles

Inventors: Michael A. Yandrasits (Hastings, MN); Miguel A. Guerra (Woodbury, MN); Carl A. Laskowski (Minneapolis, MN); Matthew J. Lindell (Woodbury, MN)
Assignee: 3M Innovative Properties Company
H01M8/1032C07C309/82C08F214/262C08F216/1475H01M8/1004H01M8/1039H01M2008/1095H01M2300/0082
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Quick Facts
Patent No.
US 12,341,227
App. No.
17/739,227
Granted
Jun 24, 2025
Kind
B2
Abstract

Presently described is a monomer having the formula: wherein n ranges from 2 to 8; Y is F or C m F 2m+1 ; a is 0, or averages 1 to 2; m is independently 1, 2, 3, or 4; and X is F or OH. Also described is a method of making such monomer, various compounds prepared during while making the monomer, fluoropolymers comprising polymerized units of such monomer, fuel cell membranes, membrane electrode assemblies, and methods of making fluoropolymers.

Claims (24)

1. A monomer of the formula:

wherein

n ranges from 2 to 8;

Y is F or C m F 2m+1 ;

a is 0, or averages 1 to 2;

m is independently 1, 2, 3, or 4; and

X is F or OH.

2. The monomer of claim 1 wherein m is 1.

3. The monomer of claim 1 wherein a is 0.

4. The monomer of claim 1 wherein n is 2, 3, or 4.

5. The monomer of claim 1 wherein the energy barrier to abstract a fluorine atom by a hydrogen atom (H·) from C m F 2m+1 of the ethylenically unsaturated group is greater than the energy barrier to abstract a fluorine atom from C m F 2m+1 , wherein m is 0.

6. A fluoropolymer comprising polymerized units of the monomer according to claim 1 .

7. The fluoropolymer of claim 6 , wherein the polymer comprises polymerized units of at least one other ethylenically unsaturated comonomer.

8. The fluoropolymer of claim 7 wherein the polymer comprises polymerized units of at least one other fluorinated ethylenically unsaturated comonomer.

9. The fluoropolymer of claim 8 wherein the other fluorinated ethylenically unsaturated comonomer comprises TFE.

10. A fuel cell membrane comprising a support and a fluoropolymer according to claim 6 .

11. The fuel cell membrane of claim 10 wherein the support comprises a nanofiber or expanded PTFE reinforcing material.

12. A membrane electrode assembly comprising the fuel cell membrane of claim 10 .

13. A method of making a fluoropolymer comprising:

emulsifying the monomer according to claim 1 in an aqueous liquid;

optionally emulsifying at least one additional ethylenically unsaturated comonomer in the aqueous liquid;

charging a polymerization kettle with the aqueous liquid of emulsified monomer(s); and

heating the aqueous liquid of emulsified monomer under pressure such that the monomers polymerize forming a fluoropolymer.

14. The method of claim 13 further comprises hydrolyzing, ion exchanging with an acid, drying, and dispersing the fluoropolymer in a mixture of alcohol and water.

Assignments (3)
CONFIRMATORY LICENSE Recorded Jun 24, 2024
From: 3M COMPANY
To: UNITED STATES DEPARTMENT OF ENERGY
Reel/Frame 067822/0692 →
CONFIRMATORY LICENSE Recorded May 15, 2024
From: 3M COMPANY
To: UNITED STATES DEPARTMENT OF ENERGY
Reel/Frame 067910/0038 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded May 9, 2022
From: YANDRASITS, MICHAEL A.; GUERRA, MIGUEL A.; LASKOWSKI, CARL A.; LINDELL, MATTHEW J.
To: 3M INNOVATIVE PROPERTIES COMPANY
Reel/Frame 059866/0610 →
Continuity (2)
Provisional Application 63196729 · Jun 4, 2021
Related Publication 20230006230A1 · Jan 5, 2023
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