IP Library › Granted Patent US 12,352,676
Granted Patent B2
US 12,352,676 · App. 17/754,831 · Granted Jul 8, 2025

Particle group characteristic measurement device, particle group characteristic measurement method, storage medium recording program for particle group characteristic measurement device, particle diameter distribution measurement device, and particle diameter distribution measurement method

Inventors: Yasuhiro Tatewaki (Kyoto, JP); Shingo Fujiwara (Kyoto, JP)
Assignee: HORIBA, LTD.
G01N15/0227G01N15/0211G01N2015/0053
View Patent ↗
Loading inventors, assignments & file history…
Monitor This Case
Get email alerts when status or documents change.
Order Certified Copies
Most orders are placed with the USPTO same day — all within 24 business hours.
Order via The Patent Place →
Pre-filled with this patent's details
Quick Facts
Patent No.
US 12,352,676
App. No.
17/754,831
Granted
Jul 8, 2025
Kind
B2
Abstract

A particle group characteristic measurement device includes an image acquisition portion that acquires images of a particle group, a particle information extraction portion that processes acquisition images acquired by the image acquisition portion, and then extracts particle information which is information about particles appearing in the acquisition images, and a particle group characteristic calculation portion that calculates a particle group characteristic at a plurality of time points in a time series based on the particle information extracted from a plurality of the acquisition images acquired prior to respective time points. The particle group characteristic calculation portion calculates the particle group characteristic at each time point based on the plurality of acquisition images used to calculate the particle group characteristic at time points previous to that time point, and on the particle information extracted from the plurality of acquisition images whose image acquisition time periods partially overlap each other.

Claims (40)

1. A particle group characteristic measurement device that measures changes over time in a particle group characteristic which is a characteristic of a particle group that is formed by a plurality of particles dispersed in a dispersion medium, comprising:

an image acquisition portion that includes image acquisition elements and acquires consecutive acquisition images of the particle group, each of the consecutive acquisition images being acquired using the image acquisition elements;

a particle information extraction portion that processes the consecutive acquisition images acquired by the image acquisition portion, and then extracts particle information which is information about the particles appearing in the consecutive acquisition images;

a particle group characteristic calculation portion that calculates the particle group characteristic at a plurality of time points in a time series based on the particle information extracted from a plurality of the consecutive acquisition images acquired prior to the respective time points, the particle group characteristic being a representative particle diameter of a plurality of particles forming the particle group; and

a display control portion that displays a graph showing changes over time in the representative particle diameter calculated by the particle group characteristic calculation portion at each of the plurality of time points, wherein

a portion of the plurality of the consecutive acquisition images used to calculate the particle group characteristic at one time point of the plurality of time points overlaps in image acquisition time period with a portion of the plurality of the consecutive acquisition images used to calculate the particle group characteristic at an earlier time point of the plurality of time points.

2. The particle group characteristic measurement device according to claim 1 , wherein the plurality of the consecutive acquisition images used to calculate the particle group characteristics at the one time point partially overlaps with the plurality of the consecutive acquisition images used to calculate the particle group characteristic at the earlier time point immediately previous to the one time point.

3. The particle group characteristic measurement device according to claim 1 , wherein the particle group characteristic calculation portion calculates the particle group characteristic at the one time point based on a plurality of the particle information items that include the particle information extracted from the acquisition image immediately previous to the one time point.

4. The particle group characteristic measurement device according to claim 1 , wherein the particle group characteristic calculation portion calculates the particle group characteristic at each time point based on the particle information extracted from a fixed number of the consecutive acquisition images that were acquired in a continuous acquisition sequence.

5. The particle group characteristic measurement device according to claim 1 , further comprising a calculation command portion that outputs a calculation command signal commanding that the particle group characteristic be calculated to the particle group characteristic calculation portion, wherein

the calculation command portion outputs the calculation command signal at predetermined time intervals.

6. The particle group characteristic measurement device according to claim 1 , further comprising a calculation command portion that outputs a calculation command signal commanding that the particle group characteristic be calculated to the particle group characteristic calculation portion, wherein

the calculation command portion outputs the calculation command signal each time the particle information extraction portion extracts the particle information from a predetermined number of the consecutive acquisition images.

7. The particle group characteristic measurement device according to claim 1 , wherein the display control portion displays in real time results of the calculation made by the particle group characteristic calculation portion at each of the time points.

8. The particle group characteristic measurement device according to claim 7 , wherein the particle group characteristic calculation portion calculates a mutually different plurality of the particle group characteristics, and

the display control portion displays this plurality of particle group characteristics on the same screen.

9. A particle diameter distribution measurement device that measures a particle diameter distribution of a particle group that is formed by a plurality of particles dispersed in a dispersion medium, comprising:

a circulation system that causes a suspension to circulate between a measurement cell and a mixture tank that creates the suspension by mixing the dispersion medium with the particles;

an optical measurement system that measures the particle diameter distribution of the particle group based on scattered light that is generated as a result of laser light being irradiated onto the suspension that is flowing through an interior of the measurement cell; and

the particle group characteristic measurement device according to claim 1 that measures changes over time in a characteristic of the particle group in the suspension that is flowing through the circulation system.

10. The particle group characteristic measurement device according to claim 1 , further comprising a storage, wherein

the particle information extracted from the plurality of the consecutive acquisition images is stored in the storage as particle data groups corresponding respectively to the plurality of the consecutive acquisition images,

the particle group characteristic calculation portion uses a fixed number of the particle data groups stored in the storage that were extracted in a continuous sequence for calculating the particle group characteristic for each of the time points, and

a portion of the particle data groups used for calculating the particle group characteristic at the one time point were used to calculate a previous particle group characteristic at the earlier time point.

11. A particle group characteristic measurement method which is a method of measuring changes over time in a particle group characteristic which is a characteristic of a particle group that is formed by a plurality of particles dispersed in a dispersion medium, comprising:

acquiring consecutive acquisition images of the particle group using image acquisition elements of an image acquisition portion;

processing the acquired consecutive acquisition images of the particle group, and extracting particle information which is information about the particles appearing in the consecutive acquisition images;

calculating the particle group characteristic at a plurality of time points in a time series based on the particle information extracted from the plurality of the consecutive acquisition images acquired prior to the respective time points, the particle group characteristic being a representative particle diameter of a plurality of particles forming the particle group; and

displaying a graph showing changes over time in the representative particle diameter calculated in the step of calculating at each of the plurality of time points, wherein,

in the calculation of the particle group characteristic, a portion of the plurality of the consecutive acquisition images used to calculate the particle group characteristic at one time point of the plurality of time points overlaps in image acquisition time period with a portion of the plurality of the consecutive acquisition images used to calculate the particle group characteristic at an earlier time point of the plurality of time points.

12. A particle diameter distribution measurement method which is a method of measuring a particle diameter distribution of a particle group that is formed by a plurality of particles dispersed in a dispersion medium, comprising:

causing a suspension to circulate between a measurement cell and a mixture tank that creates the suspension by mixing the dispersion medium with the particles;

measuring changes over time in a characteristic of the particle group in the suspension being circulated using the method according to claim 11 ; and

measuring the particle diameter distribution of the particle group based on scattered light that is generated as a result of laser light being irradiated onto the suspension that is flowing through an interior of the measurement cell.

13. A storage medium that stores program for a particle group characteristic measurement device that measures changes over time in a particle group characteristic which is a characteristic of a particle group that is formed by a plurality of particles dispersed in a dispersion medium, the program being characterized by causing a computer to perform functions of:

an image acquisition portion with image acquisition elements that acquires consecutive acquisition images of the particle group, each of the consecutive acquisition images being acquired using the image acquisition elements;

a particle information extraction portion that processes the consecutive acquisition images acquired by the image acquisition portion, and then extracts particle information which is information about the particles appearing in the consecutive acquisition images;

a particle group characteristic calculation portion that calculates the particle group characteristic at a plurality of time points in a time series based on the particle information extracted from a plurality of the consecutive acquisition images acquired prior to the respective time points, the particle group characteristic being a representative particle diameter of a plurality of particles forming the particle group; and

a display control portion that displays a graph showing changes over time in the representative particle diameter calculated by the particle group characteristic calculation portion at each of the plurality of time points, wherein

a portion of the plurality of the consecutive acquisition images used to calculate the particle group characteristic at one time point of the plurality of time points overlaps in image acquisition time period with a portion of the plurality of the consecutive acquisition images used to calculate the particle group characteristic at an earlier time point of the plurality of time points.

Assignments (1)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Apr 13, 2022
From: TATEWAKI, YASUHIRO; FUJIWARA, SHINGO
To: HORIBA, LTD.
Reel/Frame 059591/0355 →
Priority Claims (1)
JP 2019-188443 · Oct 15, 2019 · national
Continuity (1)
Related Publication 20240102907A1 · Mar 28, 2024
References Cited (32)
US 10943692B1 · Lynn · 2021 [cited by examiner]
US 20040184649A1 · Canty · 2004 [cited by examiner]
US 20120135535A1 · Grier · 2012 [cited by examiner]
US 20130330666A1 · Fukuri · 2013 [cited by examiner]
US 20140368378A1 · Crain · 2014 [cited by examiner]
US 20180056689A1 · Makuta · 2018 [cited by examiner]
US 20180257104A1 · Che · 2018 [cited by examiner]
US 20210190660A1 · Stahl · 2021 [cited by examiner]
US 20240102907A1 · Tatewaki · 2024 [cited by examiner]
CN 105571998A · 2016 [cited by applicant]
CN 103575734B · 2016 [cited by examiner]
CN 107316301A · 2017 [cited by applicant]
JP H0436637A · 1992 [cited by applicant]
JP H06277687A · 1994 [cited by applicant]
JP 2000146817A · 2000 [cited by applicant]
JP 2001056282A · 2001 [cited by applicant]
JP 2001074637A · 2001 [cited by examiner]
JP 2002207001A · 2002 [cited by applicant]
JP 3411112B2 · 2003 [cited by examiner]
JP 2008249724A · 2008 [cited by applicant]
JP 2013015357A · 2013 [cited by applicant]
JP 2015105898A · 2015 [cited by applicant]
JP 2015520397A · 2015 [cited by applicant]
JP 2017116260A · 2017 [cited by applicant]
JP 2020504296A · 2020 [cited by examiner]
JP 7172212B2 · 2022 [cited by examiner]
WO WO2008131409A1 · 2008 [cited by examiner]
WO 2013190327A2 · 2013 [cited by applicant]
WO WO2022247945A1 · 2022 [cited by examiner]
PCT, International Search Report for the corresponding application No. PCT/JP2020/037815, dated Dec. 22, 2020, with English translation. [cited by applicant]
Decision to Grant a Patent, dated Nov. 14, 2024, which was issued for the corresponding Japanese Patent Application No. 2021-552335, 5 pages, with English Translation. [cited by applicant]
Office Action dated Sep. 13, 2024, issued in related Chinese patent application No. 202080071290.2, with English translation, 28 pages. [cited by applicant]