IP Library › Granted Patent US 12,618,844
Granted Patent B2
US 12,618,844 · App. 17/793,374 · Granted May 5, 2026

Cancer

Inventors: George Hanna (London, GB); Sophie Doran (London, GB)
Assignee: Imperial College Innovations Limited
G01N33/57585G01N33/497G01N33/5753G01N33/4975
View Patent ↗
Loading inventors, assignments & file history…
Monitor This Case
Get email alerts when status or documents change.
Order Certified Copies
Most orders are placed with the USPTO same day — all within 24 business hours.
Order via The Patent Place →
Pre-filled with this patent's details
Quick Facts
Patent No.
US 12,618,844
App. No.
17/793,374
Granted
May 5, 2026
Kind
B2
Abstract

The invention relates to biomarkers, and to novel biological markers for diagnosing cancer. In particular, the invention relates to the use of these compounds as diagnostic and prognostic markers in assays for detecting cancer, such as oesophagogastric cancer, and corresponding methods of detection. The invention also relates to methods of determining the efficacy of treating these diseases with a therapeutic agent. The assays are qualitative and/or quantitative, and are adaptable to large-scale screening and clinical trials.

Claims (12)

1 . A method of treating an individual suffering from oesophagogastric cancer, said method comprising the steps of:

a) detecting the level of at least one signature compound in a bodily sample from a test subject using gas chromatography, mass spectrometry, and/or GCMS, wherein the bodily sample is a breath sample from the test subject, wherein the at least one signature compound is elected from group (i) consisting of methyl 2,3,5,6-tetra-O-methyl-α-D-galactofuranoside; 1-tetradecanol; N-butyl-benzenesulfonamide; hexadecanoic acid; tetradec-5-yl ester 3,5,5-trimethyl-hexanoic acid; tetradecyl ester undec-10-ynoic acid; 1-dotriacontanol; 1-chloro-tetradecane; 4-methyloctan-1-ol; carbon monoxide; nickel; 2-ethyl-cyclohexylamine; 3-ethyl-1-octene; ethyl lactate; tetramethyl succinimide; 6-methyl-2-heptanone; (E)-ethen-2-d-ol; 4-anilino-4-keto-2-phenyl-butyric acid; diisobutyl (oxybis(ethane-2,1-diyl)) dicarbonate; nickel tetracarbonyl; (E)-2-ethylene-4-methylene-5-hexenal; 3-methyl-1-butyne; (R)-5-methyl-2-(1-methylethylidene)-cyclohexanone; α-propyl-benzeneethanol; 4-methyl-1-pentene; 1,3,3-trimethyl-2-oxabicyclo[2.2.2]oct-5-ene; 2,2′-(ethene-1,2-diylbis(sulfanediyl))diethanol; 3-methyl-thiophene; tert-butyl alcohol; and 2-methoxysuccinonitrile, compared to the reference, in the bodily sample from the test subject, or group (ii) consisting of 4-hydroximino-2,2,6,6-tetramethyl-1-piperidinyl ester 4-amino-benzoic acid; 4,4-dimethyl-octane; benzyl 3-deuterio-α-diazopropionate; and 1-methylethyl ester formic acid; and

b) treating the test subject with a therapeutic agent and/or radiotherapy, if there is an increase in the level of the at least one signature compound selected from group (i) or a decrease in the level of the at least one signature compound selected from group (ii) in the bodily sample from the test subject, compared to a reference, wherein the reference level is the level of the at least one signature compound in an individual, or the average level for a group of individuals, wherein the individual or group of individuals do not suffer from oesophagogastric cancer, wherein the treatment reduces or delays progression of cancer and/or treats cancer.

2 . A method according to claim 1 , wherein the at least one signature compound is selected from the group consisting of methyl 2,3,5,6-tetra-O-methyl-α-D-galactofuranoside; 4-hydroximino-2,2,6,6-tetramethyl-1-piperidinyl ester 4-amino-benzoic acid; 1-tetradecanol; N-butyl-benzenesulfonamide; hexadecanoic acid; tetradec-5-yl ester 3,5,5-trimethyl-hexanoic acid; 4,4-dimethyl-octane; tetradecyl ester undec-10-ynoic acid; 1-dotriacontanol; benzyl 3-deuterio-α-diazopropionate; 1-methylethyl ester formic acid; 1-chloro-tetradecane; 4-methyloctan-1-ol; carbon monoxide; nickel; and 2-ethyl-cyclohexylamine.

3 . A method according to claim 2 , wherein the at least one signature compound is selected from the group consisting of methyl 2,3,5,6-tetra-O-methyl-α-D-galactofuranoside; 4-hydroximino-2,2,6,6-tetramethyl-1-piperidinyl ester 4-amino-benzoic acid; 1-tetradecanol; N-butyl-benzenesulfonamide; hexadecanoic acid; tetradec-5-yl ester 3,5,5-trimethyl-hexanoic acid; 4,4-dimethyl-octane; tetradecyl ester undec-10-ynoic acid; 1-dotriacontanol; and benzyl 3-deuterio-α-diazopropionate.

4 . A method according to claim 3 , wherein the at least one signature compound is selected from the group consisting of methyl 2,3,5,6-tetra-O-methyl-α-D-galactofuranoside; 4-hydroximino-2,2,6,6-tetramethyl-1-piperidinyl ester 4-amino-benzoic acid; 1-tetradecanol; N-butyl-benzenesulfonamide; and hexadecanoic acid.

5 . A method according to claim 1 , wherein the at least one signature compound is selected from the group consisting of 3-ethyl-1-octene; ethyl lactate; tetramethyl succinimide; 6-methyl-2-heptanone; (E)-ethen-2-d-ol; 4-anilino-4-keto-2-phenyl-butyric acid; diisobutyl (oxybis(ethane-2,1-diyl)) dicarbonate; nickel tetracarbonyl; (E)-2-ethylene-4-methylene-5-hexenal; 3-methyl-1-butyne; (R)-5-methyl-2-(1-methylethylidene)-cyclohexanone; α-propyl-benzeneethanol; 4-methyl-1-pentene; 1,3,3-trimethyl-2-oxabicyclo[2.2.2]oct-5-ene; 2,2′-(ethene-1,2-diylbis(sulfanediyl))diethanol; 3-methyl-thiophene; tert-butyl alcohol; and 2-methoxysuccinonitrile.

6 . A method according to claim 5 , wherein the at least one signature compound is selected from the group consisting of 3-ethyl-1-octene; ethyl lactate; tetramethyl succinimide; 6-methyl-2-heptanone; (E)-ethen-2-d-ol; 4-anilino-4-keto-2-phenyl-butyric acid; diisobutyl (oxybis(ethane-2,1-diyl)) dicarbonate; nickel tetracarbonyl; (E)-2-ethylene-4-methylene-5-hexenal; 3-methyl-1-butyne; (R)-5-methyl-2-(1-methylethylidene)-cyclohexanone; α-propyl-benzeneethanol; 4-methyl-1-pentene; and 1,3,3-trimethyl-2-oxabicyclo[2.2.2]oct-5-ene.

7 . A method according to claim 6 , wherein the at least one signature compound is selected from the group consisting of 3-ethyl-1-octene; ethyl lactate; tetramethyl succinimide; 6-methyl-2-heptanone; (E)-ethen-2-d-ol; 4-anilino-4-keto-2-phenyl-butyric acid; diisobutyl (oxybis(ethane-2,1-diyl)) dicarbonate; and nickel tetracarbonyl.

8 . A method according to claim 7 , wherein the at least one signature compound is selected from the group consisting of 3-ethyl-1-octene; and ethyl lactate.

9 . A method according to claim 1 , wherein the mass spectrometry comprises TOF.

10 . A method according to claim 1 , wherein the at least one signature compound is selected from the group consisting of 1-tetradecanol; 4-methyloctan-1-ol; 3-ethyl-1-octene; ethyl lactate; 6-methyl-2-heptanone; (E)-ethen-2-d-ol; (E)-2-ethylene-4-methylene-5-hexenal; 3-methyl-1-butyne; 4-methyl-1-pentene; 3-methyl-thiophene; tert-butyl alcohol; and 4,4-dimethyl-octane.

Assignments (1)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jul 20, 2023
From: HANNA, GEORGE; DORAN, SOPHIE
To: IMPERIAL COLLEGE INNOVATIONS LIMITED
Reel/Frame 064330/0220 →
Priority Claims (1)
GB 2000739 · Jan 17, 2020 · national
Continuity (1)
Related Publication 20230068371A1 · Mar 2, 2023
References Cited (19)
US 6027550A · Vickery · 2000 [cited by examiner]
US 20130150261A1 · Haick · 2013 [cited by examiner]
US 20180156775A1 · Chou · 2018 [cited by examiner]
US 20180209978A1 · Postrel · 2018 [cited by examiner]
US 20190317073A1 · Horvath · 2019 [cited by applicant]
US 20200029858A1 · Reddy · 2020 [cited by examiner]
US 20210341461A1 · Allsworth · 2021 [cited by examiner]
GB 2584300A · 2020 [cited by applicant]
WO WO2019053414 · 2019 [cited by applicant]
WO WO2019102221 · 2019 [cited by applicant]
WO WO2020049300A1 · 2020 [cited by examiner]
Adam, Mina E., et al. “Mass-spectrometry analysis of mixed-breath, isolated-bronchial-breath, and gastric-endoluminal-air volatile fatty acids in esophagogastric cancer.” Analytical chemistry 91.5 (2019): 3740-3746. [cited by applicant]
International Search Report and Written Opinion for Application No. PCT/GB2021/050104 mailed on May 7, 2022, 17 pages. [cited by applicant]
Kumar, Sacheen, et al. “Mass spectrometric analysis of exhaled breath for the identification of volatile organic compound biomarkers in esophageal and gastric adenocarcinoma.” Annals of surgery 262.6 (2015): 981-990. [cited by applicant]
Kumar, Sacheen, et al. “Selected ion flow tube mass spectrometry analysis of exhaled breath for volatile organic compound profiling of esophago-gastric cancer.” Analytical chemistry 85.12 (2013): 6121-6128. [cited by applicant]
Markar, Sheraz R., et al. “Assessment of a noninvasive exhaled breath test for the diagnosis of oesophagogastric cancer.” [cited by applicant]
Nishiumi, Shin, et al. “Metabolomics for biomarker discovery in gastroenterological cancer.” Metabolites 4.3 (2014): 547-571. [cited by applicant]
Silva, C. L., M. Passos, and J. S. Câmara. “Investigation of urinary volatile organic metabolites as potential cancer biomarkers by solid-phase microextraction in combination with gas chromatography-mass spectrometry.” … [cited by applicant]
Suzuki, Makoto, et al. “Metabolome analysis for discovering biomarkers of gastroenterological cancer.” Journal of Chromatography B 966 (2014): 59-69. [cited by applicant]