IP Library Granted Patent US 12,168,819
Granted Patent B2
US 12,168,819 · App. 17/803,110 · Granted Dec 17, 2024

Modified La—Fe—Si magnetocaloric alloys

Inventors: Arjun K. Pathak (Willamsville, NY); Yaroslav Mudryk (Ames, IA); Oleksandr Dolotko (Karlsruhe, DE); Vitalij K. Pecharsky (Ames, IA)
Assignee: Iowa State University Research Foundation, Inc.
C22C33/04B33Y70/00C22C38/005C22C38/02C22C38/06H01F1/015B22F10/28C22C2202/02
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Quick Facts
Patent No.
US 12,168,819
App. No.
17/803,110
Granted
Dec 17, 2024
Kind
B2
Abstract

A magnetocaloric material comprising a La—Fe—Si based alloy composition that is compositionally modified to include a small but effective amount of at least one of Al, Ga, and In to improve mechanical stability of the alloy (substantially reduce alloy brittleness), improve thermal conductivity, and preserve comparable or provide improved magnetocaloric effects. The alloy composition may be further modified by inclusion of at least one of Co, Mn, Cr, and V as well as interstitial hydrogen.

Claims (9)

1. A magnetocaloric alloy comprising a magnetocaloric intermetallic compound phase having a crystal structure which comprises La, Fe and Si and at least one of Al, Ga, and/or In are present in solid solution in an amount of 0.07 atomic % to 3.5 atomic % of the alloy which amount is selected to reduce alloy brittleness as compared to an identical alloy devoid of Al, Ga, and In to increase the number of temperature/magnetic field cycles without alloy cracking or decrepitating.

2. The alloy of claim 1 wherein said at least one of Al, Ga, and/or In is/are substituted for an amount of the Si of the alloy.

3. The alloy of claim 1 also including at least one of Co, Mn, Cr, and V.

4. The alloy of claim 3 wherein said at least one of Co, Mn, Cr, and V is/are substituted for some of the Fe of the alloy.

5. The alloy of claim 1 including interstitial hydrogen.

6. The alloy of claim 1 which is solidified from a bulk alloy melt.

7. The alloy of claim 6 which is solidified and then heat treated.

8. The alloy of claim 1 wherein said at least one of Al, Ga, and/or In is/are present in an amount of 0.6 atomic % to 3.5 atomic % of the alloy.

9. The alloy of claim 1 wherein said at least one of Al, Ga, and/or In is/are present in an amount of 0.7 atomic % to 3.5 atomic % of the alloy.

Assignments (2)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Oct 23, 2024
From: PATHAK, ARJUN K.; MUDRYK, YAROSLAV; DOLOTOKO, OLEKSANDR; PECHARSKY, VITALIJ K.
To: IOWA STATE UNIVERSITY RESEARCH FOUNDATION, INC.
Reel/Frame 068984/0151 →
CONFIRMATORY LICENSE Recorded Jun 22, 2022
From: IOWA STATE UNIVERSITY
To: UNITED STATES DEPARTMENT OF ENERGY
Reel/Frame 060414/0178 →
Continuity (3)
Continuation 16501027 · Feb 11, 2019
Provisional Application 62710968 · Mar 5, 2018
Related Publication 20220238262A1 · Jul 28, 2022