IP Library Granted Patent US 12,006,565
Granted Patent B2
US 12,006,565 · App. 17/821,367 · Granted Jun 11, 2024

Method for coating stainless steel press plates and coated press plates produced thereby

Inventor: Muyuan M. Ma (Austin, TX)
Assignee: WILSONART LLC
C23C14/0688B30B15/062B32B15/00B32B15/01B32B15/012B32B37/0046C23C14/025C23C14/067C23C14/352
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Quick Facts
Patent No.
US 12,006,565
App. No.
17/821,367
Granted
Jun 11, 2024
Kind
B2
Abstract

A method for coating stainless steel press plates includes preparing the stainless steel press plate for coating and coating the stainless steel press plate with a diboride doped with 1%-5% by weight aluminum to produce a diboride-aluminum coating. The step of coating includes applying the diboride-aluminum coating to a stainless steel press plate using a magnetron sputter coating system.

Claims (14)

1. A method for coating a substrate, comprising:

preparing a substrate for coating;

coating the substrate with a diboride doped with 1%-5% by weight aluminum to produce a diboride-aluminum coating, wherein the step of coating consists of applying the diboride using a first applicator of a magnetron sputter coating system and simultaneously doping the diboride with 1%-5% by weight aluminum by applying aluminum using a second applicator consisting of aluminum of the magnetron sputter coating system producing the diboride-aluminum coating consisting of the diboride and the aluminum upon the substrate.

2. The method according to claim 1 , wherein the diboride-aluminum coating has a Vickers hardness of at least 35 GPa.

3. The method according to claim 2 , wherein the diboride-aluminum coating has a Vickers hardness of 46 GPa.

4. The method according to claim 1 , wherein the diboride-aluminum coating has a thickness of about 3 microns.

5. The method according to claim 1 , wherein the step of coating includes doping the diboride with 2% by weight aluminum.

6. The method according to claim 5 , wherein the step of coating includes applying the diboride-aluminum coating at a substrate bias of 60-90 V and at temperature of 200° C.

7. The method according to claim 1 , wherein the diboride-aluminum coating has a minimum bond strength of 1.6 kilogram force.

8. The method according to claim 7 , wherein the diboride-aluminum coating has a minimum bond strength of 1.8 kilogram force.

9. The method according to claim 1 , wherein the step of coating includes applying multiple layers of the diboride-aluminum coating.

10. The method according to claim 1 , wherein the diboride-aluminum coating is applied in a two-stage process composed of a gradient based diboride-aluminum coating layer and a top titanium diboride-aluminum coating layer.

11. The method according to claim 10 , wherein the gradient based diboride-Al coating layer is 600 nm in thickness.

12. The method according to claim 11 , wherein the top diboride-aluminum coating layer is 1,240 nm in thickness.

Assignments (1)
NOTICE AND CONFIRMATION OF GRANT OF SECURITY INTEREST IN PATENTS Recorded Aug 5, 2024
From: WILSONART LLC
To: DEUTSCHE BANK AG NEW YORK BRANCH
Reel/Frame 068550/0979 →
Continuity (4)
Continuation 16902594 · Jun 16, 2020
Division 15426439 · Feb 7, 2017
Provisional Application 62293032 · Feb 9, 2016
Related Publication 20220396868A1 · Dec 15, 2022