IP Library Granted Patent US 11,660,566
Granted Patent B2
US 11,660,566 · App. 17/850,624 · Granted May 30, 2023

Hydrogen purification using molecular dynamics

Inventors: Glen Robles (Santa Maria, CA); Robert Nimocks (Santa Barbara, CA); Mike Rocke (Flower Mound, TX); Charity Cheiky (Thousand Oaks, CA)
Assignee: H24US Corp.
B01D53/228B01D53/226B01D69/02B01D69/1216B01D69/1218B01D69/148B01D71/021B01D71/36C01B3/503B01D2325/0231B01D2325/0233C01B2203/0405C01B2203/048C01B2203/0475
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Quick Facts
Patent No.
US 11,660,566
App. No.
17/850,624
Granted
May 30, 2023
Kind
B2
Abstract

A membrane is described for purifying or separating hydrogen from a multi-component gas stream such as syngas. This membrane uses a molecular pre-treatment, a transition metal, fluorine containing polymer, carbon fibers and carbon matrix sintered on a supportive screen. The membrane may be a bilayer membrane comprised of a layer containing high surface area carbon and another layer containing lower surface area carbon. Methods for purifying hydrogen are also described.

Claims (14)

1. A method for hydrogen purification, comprising:

providing a hydrogen comprising a multi-stage hybrid membrane, each membrane comprising a screen, a first layer formed on the screen and a second layer formed on the first layer;

pumping a gas stream through the hydrogen concentrator, the gas stream comprising syngas including hydrogen and at least one additional gas; and

separating hydrogen from the mixture containing hydrogen and the at least one additional gas;

wherein pumping the gas stream comprises keeping the hydrogen moving within the hydrogen concentrator and pulsing in the at least one additional gas.

2. The method of claim 1 , further comprising forming the first layer from a mixture of carbon fibers, transition metal compounds, a fluorine containing polymer, and an additional carbon material.

3. The method of claim 2 , further comprising forming the second layer from a mixture of carbon fibers, transition metal compounds, a fluorine containing polymer, and activated carbon.

4. The method of claim 1 , further comprising forming the first layer to be a more porous structure than the second layer to provide prefiltering and faster throughput of material.

5. The method of claim 1 , further comprising forming the first layer from at least one lower density carbon material such that it comprises a more permeable and open structure than the second layer.

6. The method of claim 5 , wherein the at least one lower density carbon material precursor is selected from the group consisting of: carbon nanotube, carbon nanofiber, carbon black derived from pet coke, acetylene or natural gas, and graphene.

7. The method of claim 3 , further comprising deriving the activated carbon from sources selected from the group consisting of: coconut shells, almond shells, wood, biomass trimmings, and coal.

8. The method of claim 1 , further comprising pre-treating the membrane with gas molecules from a gas stream containing methane and carbon dioxide.

9. The method of claim 1 , wherein the at least one additional gas comprises carbon dioxide.

10. The method of claim 1 , wherein the at least one additional gas comprises carbon dioxide and methane.

Assignments (1)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Sep 2, 2022
From: ROBLES, GLEN; NIMOCKS, ROBERT; ROCKE, MIKE; CHEIKY, CHARITY
To: H24US CORP
Reel/Frame 060984/0812 →
Continuity (3)
Continuation In Part 17389014 · Jul 29, 2021
Provisional Application 63061608 · Aug 5, 2020
Related Publication 20220331733A1 · Oct 20, 2022