IP Library › Granted Patent US 12,448,334
Granted Patent B2
US 12,448,334 · App. 17/865,747 · Granted Oct 21, 2025

High temperature sag resistant gypsum panel

Inventors: Mark K. Hemphill (Hawthorn Woods, IL); Qinghua Li (Rolling Meadows, IL); Aaron D. Johnson (Antioch, IL)
Assignee: KNAUF GIPS KG
C04B28/14B28B19/0092B32B5/18C04B14/46B32B17/066B32B29/007B32B2266/053B32B2307/3065B32B2307/72B32B2315/08B32B2315/18B32B2607/00C04B2111/0062C04B2111/28C04B2111/34C04B2201/20
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Quick Facts
Patent No.
US 12,448,334
App. No.
17/865,747
Granted
Oct 21, 2025
Kind
B2
Abstract

A fire-resistant gypsum panel comprises: a gypsum core layer comprising set gypsum and a high temperature sag-resistant material including mineral wool in an amount between 0.2% and 3.0% by weight of gypsum.

Claims (51)

1. A fire-resistant gypsum panel comprising:

a gypsum core layer comprising set gypsum and mineral wool in an amount of between greater than 0.9% and less than or equal to and 3.0% by weight of stucco, wherein the mineral wool includes spun or drawn mineral rock material, and wherein the gypsum panel at a temperature of 1600° F. has a sag reduction of at least 10% compared to a gypsum panel that includes glass fiber in place of the mineral wool but is otherwise likewise configured.

2. The gypsum panel of claim 1 , further comprising:

a facing material.

3. The gypsum panel of claim 1 , wherein the gypsum core further comprises a shrinkage-resistant material.

4. The gypsum panel of claim 1 , wherein the gypsum core further comprises one or more of a starch, a binder, a set accelerator, a dispersant, a set retarder, or a reinforcing fiber.

5. The gypsum panel of claim 1 , wherein the gypsum core has a chloride level of 300 ppm or greater.

6. The gypsum panel of claim 1 , wherein the gypsum core does not include glass fiber.

7. The gypsum panel of claim 1 , wherein the set gypsum core has a density between about 15 pcf and about 60 pcf.

8. The gypsum panel of claim 1 , wherein the gypsum panel comprises ceiling board, wallboard, or surface board.

9. A set gypsum core for a gypsum panel comprising:

a. set gypsum; and

b. a mineral wool in an amount greater than 0.9% and less than or equal to 3.0% by weight of the stucco, wherein the mineral wool includes spun or drawn mineral rock material,

wherein the gypsum panel at a temperature of 1600° F. has a sag reduction of at least 10% compared to a gypsum panel that includes glass fiber in place of the mineral wool but is otherwise likewise configured.

10. The set gypsum core of claim 9 , further comprising:

a shrinkage-resistant material.

11. The set gypsum core of claim 9 , wherein the gypsum core does not include glass fiber.

12. The set gypsum core of claim 9 , wherein the gypsum core has a chloride level of 300 ppm or greater.

13. A composition for forming a gypsum core for a gypsum panel comprising:

a. water;

b. stucco; and

c. mineral wool in an amount greater than 0.9% and less than or equal to and 3.0% by weight of the stucco, wherein the mineral wool includes spun or drawn mineral rock material;

wherein the gypsum panel at a temperature at 1600° F. has a sag reduction of at least 10% compared to a gypsum panel that includes glass fiber in place of the mineral wool but is otherwise likewise configured.

14. The composition of claim 13 , further comprising:

a shrinkage-resistant material.

15. The composition of claim 13 , further comprising:

a starch.

16. The composition of claim 13 , wherein the composition does not include glass fiber.

17. The set gypsum core of claim 16 , wherein the gypsum panel is a ceiling board.

18. The composition of claim 13 , wherein the gypsum panel is a ceiling board.

19. The composition of claim 13 , wherein the gypsum core has a chloride level of 300 ppm or greater.

20. A method for making a gypsum panel comprising:

a. preparing a slurry comprising water, stucco, and mineral wool in an amount greater than 0.9% and less than or equal to 3.0% by weight of the stucco, and wherein the mineral wool includes spun or drawn mineral rock material;

b. combining the prepared slurry with aqueous foam to provide an air-foamed slurry;

c. forming a gypsum core from the air-foamed slurry;

d. allowing the formed gypsum core to set; and

e. drying the gypsum core,

wherein the gypsum panel at a temperature at 1600° F. has a sag reduction of at least 10% compared to a gypsum panel that includes glass fiber in place of the mineral wool but is otherwise likewise configured.

21. The method of claim 20 , wherein the slurry further comprises a shrinkage-resistant material.

22. The method of claim 20 , wherein said forming a gypsum core comprises depositing the air-foamed slurry over a facing material.

23. The method of claim 20 , further comprising:

providing a facing material over the deposited air-foamed slurry.

24. The method of claim 20 , further comprising:

forming a densified layer on the gypsum core; and

providing the facing material over the densified layer.

25. The method of claim 20 , further comprising:

cutting the gypsum core into one or more panels.

26. The method of claim 25 , wherein the gypsum panels comprise ceiling boards, wallboards, or surface boards.

27. The method of claim 20 , further comprising:

applying the gypsum panel to a ceiling of a structure.

28. The method of claim 20 , wherein the gypsum core has a chloride level of 300 ppm or greater.

Assignments (2)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Sep 13, 2022
From: UNITED STATES GYPSUM COMPANY
To: KNAUF GIPS KG
Reel/Frame 061075/0379 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Aug 5, 2022
From: HEMPHILL, MARK K.; LI, QINGHUA; JOHNSON, AARON D.
To: UNITED STATES GYPSUM COMPANY
Reel/Frame 061099/0751 →
Continuity (2)
Provisional Application 63225252 · Jul 23, 2021
Related Publication 20230045576A1 · Feb 9, 2023
References Cited (47)
US 2078199A · King · 1937 [cited by applicant]
US 2526066A · Croce · 1950 [cited by examiner]
US 3376147A · Dean · 1968 [cited by applicant]
US 3462341A · Littin · 1969 [cited by applicant]
US 3573947A · Kinkade et al. · 1971 [cited by applicant]
US 3616173A · Green et al. · 1971 [cited by applicant]
US 4557973A · Ali · 1985 [cited by examiner]
US 4647486A · Ali · 1987 [cited by applicant]
US 4676835A · Green et al. · 1987 [cited by applicant]
US 5155959A · Richards et al. · 1992 [cited by applicant]
US 5158612A · Savoly et al. · 1992 [cited by applicant]
US 5240639A · Diez et al. · 1993 [cited by applicant]
US 5601888A · Fowler · 1997 [cited by applicant]
US 5643510A · Sucech et al. · 1997 [cited by applicant]
US 5683635A · Sucech et al. · 1997 [cited by applicant]
US 6342284B1 · Yu et al. · 2002 [cited by applicant]
US 6409825B1 · Yu et al. · 2002 [cited by applicant]
US 6494609B1 · Wittbold et al. · 2002 [cited by applicant]
US 6632550B1 · Yu et al. · 2003 [cited by applicant]
US 6815049B2 · Veeramasuneni et al. · 2004 [cited by applicant]
US 6822033B2 · Yu et al. · 2004 [cited by applicant]
US 7364676B2 · Sucech et al. · 2008 [cited by applicant]
US 7851057B2 · Englert et al. · 2010 [cited by applicant]
US 8323785B2 · Yu et al. · 2012 [cited by applicant]
US 10421250B2 · Li et al. · 2019 [cited by applicant]
US 10421251B2 · Li et al. · 2019 [cited by applicant]
US 11040513B2 · Li et al. · 2021 [cited by applicant]
US 20060278128A1 · Liu et al. · 2006 [cited by applicant]
US 20100247937A1 · Liu et al. · 2010 [cited by applicant]
US 20120219785A1 · Yu · 2012 [cited by examiner]
US 20140113124A1 · Sang et al. · 2014 [cited by applicant]
US 20150010767A1 · Sang et al. · 2015 [cited by applicant]
US 20160376191A1 · Li et al. · 2016 [cited by applicant]
US 20180009129A1 · Whittington et al. · 2018 [cited by applicant]
CN 110078456A · 2019 [cited by applicant]
EP 2045227A1 · 2009 [cited by applicant]
ES 2561730A1 · 2016 [cited by applicant]
JP S57196753A · 1982 [cited by applicant]
KR 2008105776A · 2008 [cited by examiner]
WO 9516515A1 · 1995 [cited by applicant]
WO 2008045217A2 · 2008 [cited by applicant]
WO 2020256980A1 · 2020 [cited by applicant]
WO 2021104602A1 · 2021 [cited by applicant]
“Rock Wool, Stone Wool, Mineral Wool, & Slag Wool Building Insulation Identification,” https://inspectapedia.com/insulation/Rock_Wool_Insulation.php (Year: 2019). [cited by examiner]
International Search Report and Written Opinion received for PCT/IB2022/056642 mailed Nov. 3, 2022. [cited by applicant]
Kazuo, S., et al., “Inorganic building materials with high nonflammability and small shrinkage,” Chemical Abstracts, vol. 98, No. 22, 184631J, May 30, 1983, p. 312. [cited by applicant]
Piñeiro, S., et al., “New Plaster Composite with Mineral Wool Fibres from CDW Recycling” Advances in Materials Science and Engineering, vol. 2015, Jan. 2015, Article ID: 854192, 9 pages. [cited by applicant]