IP Library Granted Patent US 11,685,978
Granted Patent B2
US 11,685,978 · App. 17/869,992 · Granted Jun 27, 2023

Non-pyrophoric hydrogen storage alloys and hydrogen storage systems using the alloys

Inventor: Baoquan Huang (Troy, MI)
Assignee: Harnyss IP, LLC
C22C30/00B22F10/28B22F12/41F17C1/10F17C1/14B33Y10/00B33Y70/00B33Y80/00C22C2202/04F17C2201/0109F17C2201/0119F17C2203/0646F17C2203/0648F17C2209/2109F17C2209/2181F17C2221/012F17C2223/035F17C2260/05F17C2260/053
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Quick Facts
Patent No.
US 11,685,978
App. No.
17/869,992
Granted
Jun 27, 2023
Kind
B2
Abstract

A non-pyrophoric AB 2 -type Laves phase hydrogen storage alloy and hydrogen storage systems using the alloy. The alloy has an A-site to B-site elemental ratio of no more than about 0.5. The alloy has an alloy composition including about (in at %): Zr: 2.0-5.5, Ti: 27-31.3, V: 8.3-9.9, Cr: 20.6-30.5, Mn: 25.4-33.0, Fe: 1.0-5.9, Al: 0.1-0.4, and/or Ni: 0.0-4.0. The hydrogen storage system has one or more hydrogen storage alloy containment vessels with the alloy disposed therein.

Claims (32)

1. A non-pyrophoric AB 2 Laves phase hydrogen storage alloy comprising:

an A-site to B-site elemental ratio of not more than about 0.5; and

an alloy composition including about (in at %): Zr: 2.0-5.5, Ti: 27-31.3, V: 8.3-9.9, Cr: 20.6-30.5, Mn: 25.4-33.0, Fe: 1.0-5.9, and Al: 0.1-0.4.

2. The non-pyrophoric AB 2 Laves phase hydrogen storage alloy of claim 1 , wherein said alloy composition includes (in at %): Zr: 2.9-5.5, Ti: 27-30.3, V: 8.3-9.3, Cr: 20.6-26.5, Mn: 29.4-32.1, Fe: 1.5-5.9, and Al: 0.1-0.4.

3. The non-pyrophoric AB 2 Laves phase hydrogen storage alloy of claim 1 , wherein said alloy composition further includes up to about 4 at % nickel as an equal substitute for up to about 2 at % chromium or up to about 2 at % manganese or both.

4. The non-pyrophoric AB 2 Laves phase hydrogen storage alloy of claim 1 , wherein said alloy has a total hydrogen storage capacity of at least about 1.7 wt % at about 500 psi and about 20° C.

5. The non-pyrophoric AB 2 Laves phase hydrogen storage alloy of claim 1 , wherein said alloy has a total hydrogen storage capacity of at least about 1.8 wt % at about 500 psi and about 20° C.

6. The non-pyrophoric AB 2 Laves phase hydrogen storage alloy of claim 1 , wherein said alloy has a trapped hydrogen capacity of no more than about 0.25 wt % at about 14.5 psi and about 20° C.

7. The non-pyrophoric AB 2 Laves phase hydrogen storage alloy of claim 1 , wherein said alloy has a trapped hydrogen capacity of no more than about 0.20 wt % at about 14.5 psi and about 20° C.

8. The non-pyrophoric AB 2 Laves phase hydrogen storage alloy of claim 1 , wherein said alloy has a trapped hydrogen capacity of no more than about 0.15 wt % at about 14.5 psi and about 20° C.

9. The non-pyrophoric AB 2 Laves phase hydrogen storage alloy of claim 1 , wherein said alloy has a trapped hydrogen capacity of no more than about 0.10 wt % at about 14.5 psi and about 20° C.

10. The non-pyrophoric AB 2 Laves phase hydrogen storage alloy of claim 1 , wherein said alloy has a pressure composition temperature (PCT) isotherm slope of no more than about 0.8.

11. The non-pyrophoric AB 2 Laves phase hydrogen storage alloy of claim 1 , wherein said alloy has a PCT isotherm slope of no more than about 0.7.

12. The non-pyrophoric AB 2 Laves phase hydrogen storage alloy of claim 1 , wherein said alloy has a PCT isotherm slope of no more than about 0.6.

13. The non-pyrophoric AB 2 Laves phase hydrogen storage alloy of claim 1 , wherein said alloy has a hysteresis of not more than about 0.5.

14. The non-pyrophoric AB 2 Laves phase hydrogen storage alloy of claim 1 , wherein said alloy has a hysteresis of not more than about 0.4.

15. The non-pyrophoric AB 2 Laves phase hydrogen storage alloy of claim 1 , wherein said alloy has a hysteresis of not more than about 0.3.

16. The non-pyrophoric AB 2 Laves phase hydrogen storage alloy of claim 1 , wherein said alloy has a hysteresis of not more than about 0.2.

17. The non-pyrophoric AB 2 Laves phase hydrogen storage alloy of claim 1 , wherein said alloy has a hysteresis of not more than about 0.1.

18. The non-pyrophoric AB 2 Laves phase hydrogen storage alloy of claim 1 , wherein in the alloy composition further comprises about 1.0-10.0 at % total of at least one element selected from the group consisting of Ba, Co, Cu, Cs, K, Li, Mm, Mo, Na, Nb, Ni, Rb, Ta, Tl, and W (where Mm is mischmetal).

19. A hydrogen storage system comprising:

one or more hydrogen storage alloy containment vessels; and

a non-pyrophoric AB 2 Laves phase hydrogen storage alloy disposed within the hydrogen storage alloy containment vessel, wherein said non-pyrophoric AB 2 Laves phase hydrogen storage alloy comprises:

an A-site to B-site elemental ratio of not more than about 0.5; and

an alloy composition including about (in at %): Zr: 2.0-5.5, Ti: 27-31.3, V: 8.3-9.9, Cr: 20.6-30.5, Mn: 25.4-33.0, Fe: 1.0-5.9, and Al: 0.1-0.4.

20. The hydrogen storage system of claim 19 , wherein said alloy composition includes (in at %): Zr: 2.9-5.5, Ti: 27-30.3, V: 8.3-9.3, Cr: 20.6-26.5, Mn: 29.4-32.1, Fe: 1.5-5.9, and Al: 0.1-0.4.

21. The hydrogen storage system of claim 19 , wherein said alloy composition further includes up to about 4 at % nickel as an equal substitute for up to about 2 at % chromium or up to about 2 at % manganese or both.

22. The hydrogen storage system of claim 19 , wherein said alloy has a total hydrogen storage capacity of at least about 1.7 wt % at about 500 psi and about 20° C.

23. The hydrogen storage system of claim 19 , wherein said alloy has a trapped hydrogen capacity of no more than about 0.25 wt % at about 14.5 psi and about 20° C.

24. The hydrogen storage system of claim 19 , wherein said alloy has a PCT isotherm slope of no more than about 0.8.

25. The hydrogen storage system of claim 19 , wherein said alloy has a hysteresis of not more than about 0.5.

26. The hydrogen storage system of claim 19 , wherein the alloy composition further comprises about 1.0-10.0 at % total of at least one element selected from the group consisting of Ba, Co, Cu, Cs, K, Li, Mm, Mo, Na, Nb, Ni, Rb, Ta, Tl, and W (where Mm is mischmetal).

Assignments (4)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Dec 3, 2025
From: HARNYSS, LLC; HARNYSS HOLDINGS, LLC; HARYNSS IP, LLC
To: SESAME SOLAR INC.
Reel/Frame 073098/0422 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Aug 3, 2022
From: HUANG, BAOQUAN
To: HARNYSS IP, LLC
Reel/Frame 060709/0275 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Aug 3, 2022
From: HUANG, BAOQUAN
To: HARNYSS IP, LLC
Reel/Frame 060709/0361 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Aug 3, 2022
From: HUANG, BAOQUAN
To: HARNYSS IP, LLC
Reel/Frame 060707/0849 →
Continuity (4)
Provisional Application 63225389 · Jul 23, 2021
Provisional Application 63225366 · Jul 23, 2021
Provisional Application 63225399 · Jul 23, 2021
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