IP Library Granted Patent US 12,168,748
Granted Patent B2
US 12,168,748 · App. 17/900,113 · Granted Dec 17, 2024

Treated geothermal brine compositions with reduced concentration of silica, iron and lithium

Inventors: Stephen Harrison (Benicia, CA); John Burba, III (Parker, CO)
Assignee: Terralithium LLC
C09K5/10B01J20/08C01B33/26C01D3/04C01D15/00C01F7/46C02F9/00C09K5/048C22B3/14C22B13/00C22B19/00C22B26/00E21B43/25C02F1/26C02F1/281C02F1/42C02F2001/5218C02F1/5245C02F1/56C02F1/66C02F1/74C02F5/00C02F2101/10C02F2101/203C02F2103/06C02F2103/08C02F2103/10C02F2209/02C02F2209/06Y02W10/37
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Quick Facts
Patent No.
US 12,168,748
App. No.
17/900,113
Granted
Dec 17, 2024
Kind
B2
Abstract

This invention relates to treated geothermal brine compositions containing reduced concentrations of lithium, iron and silica compared to the untreated brines. Exemplary compositions contain concentration of lithium ranges from 0 to 200 mg/kg, concentration of silica ranges from 0 to 30 mg/kg, concentration of iron ranges from 0 to 300 mg/kg. Exemplary compositions also contain reduced concentrations of elements like arsenic, barium, and lead.

Claims (18)

1. A method for producing lithium hydroxide or lithium carbonate from a brine solution, the method comprising the steps of,

providing a brine solution comprising lithium and silica;

supplying the brine solution to a silica management step to remove silica from the brine solution to produce a silica-lean lithium containing solution;

supplying the silica-lean lithium containing solution to a lithium capture step, the lithium capture step being operable to capture lithium from the silica-lean lithium containing solution, wherein the lithium capture step selectively isolates lithium from the silica-lean lithium containing solution;

wherein the lithium capture step includes the step of contacting the silica-lean lithium containing solution with an intercalate operable to capture the lithium from the silica-lean lithium containing solution;

recovering the lithium from the lithium capture step using wash water to produce a lithium-rich stream comprising at least one of calcium, magnesium, manganese or zinc, and

contacting the lithium-rich stream with a base and a carbonate such that a portion of the at least one of calcium, magnesium, manganese or zinc present in the lithium-rich stream is removed as a solid precipitate to produce a purified lithium-rich stream comprising lithium hydroxide or lithium carbonate.

2. The method of claim 1 , wherein the brine solution is a geothermal brine.

3. The method of claim 1 , wherein the brine solution is a Salton Sea geothermal brine.

4. The method of claim 1 , wherein the silica-lean lithium containing solution is substantially free of silica.

5. The method of claim 1 , wherein the silica-lean lithium containing solution comprises a lithium chloride containing solution.

6. The method of claim 1 , further comprising the step of:

increasing the concentration of lithium in the lithium-rich stream by removing at least a portion of the water in the lithium-rich stream.

7. The method of claim 1 , wherein the intercalate is an intercalated lithium absorbent.

8. The method of claim 1 , wherein the intercalate is a lithium aluminate intercalate.

9. The method of claim 1 , further comprising:

separating precipitate from the lithium-rich stream to produce a solid waste precipitate and a purified lithium-rich stream, the purified lithium-rich stream having a lower concentration of the at least one of calcium, magnesium, manganese or zinc, wherein the purified lithium-rich stream comprises at least one of ions selected from the group consisting of borate, calcium, magnesium, manganese and zinc; and

contacting the purified lithium-rich stream with an ion selective media to reduce the concentration of at least one of the ions selected from the group consisting of borate, calcium, magnesium, manganese and zinc.

Assignments (5)
LICENSE Recorded Mar 23, 2023
From: TERRALITHIUM LLC
To: ENERGYSOURCE MINERALS LLC
Reel/Frame 063153/0792 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Oct 25, 2022
From: HARRISON, STEPHEN; BURBA, JOHN, III
To: SIMBOL INC.
Reel/Frame 061529/0510 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Oct 25, 2022
From: SIMBOL, INC.
To: ALGER ALTERNATIVE ENERGY, LLC
Reel/Frame 061529/0629 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Oct 25, 2022
From: ALL AMERICAN LITHIUM LLC
To: TERRALITHIUM LLC
Reel/Frame 061529/0815 →
CHANGE OF NAME Recorded Oct 25, 2022
From: ALGER ALTERNATIVE ENERGY, LLC
To: ALL AMERICAN LITHIUM LLC
Reel/Frame 061769/0316 →
Continuity (19)
Continuation 17061106 · Oct 1, 2020
Continuation 16258023 · Jan 25, 2019
Continuation 14190032 · Feb 25, 2014
Continuation In Part 14107689 · Dec 16, 2013
Continuation In Part 14062781 · Oct 24, 2013
Continuation In Part 13283311 · Oct 27, 2011
Continuation 12972728 · Dec 20, 2010
Continuation In Part 12945519 · Nov 12, 2010
Continuation 12822580 · Jun 24, 2010
Continuation In Part 12823000 · Jun 24, 2010
Continuation In Part 12766589 · Apr 23, 2010
Provisional Application 61873212 · Sep 3, 2013
Provisional Application 61408452 · Oct 29, 2010
Provisional Application 61287983 · Dec 18, 2009
Provisional Application 61261114 · Nov 13, 2009
Provisional Application 61239275 · Sep 2, 2009
Provisional Application 61220000 · Jun 24, 2009
Provisional Application 61172540 · Apr 24, 2009
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