IP Library Granted Patent US 12,397,345
Granted Patent B2
US 12,397,345 · App. 17/914,026 · Granted Aug 26, 2025

Powder for film formation or sintering

Inventors: Kento Matsukura (Omuta, JP); Shuichi Tateoka (Omuta, JP); Hirochika Ogawa (Omuta, JP)
Assignee: MITSUI MINING & SMELTING CO., LTD.
B22F1/00C01F17/34C23C4/11C01P2002/74C01P2002/76C01P2004/61C01P2006/12C01P2006/14C01P2006/16
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Quick Facts
Patent No.
US 12,397,345
App. No.
17/914,026
Granted
Aug 26, 2025
Kind
B2
Abstract

A powder for coating or sintering exhibits a peak assigned to orthorhombic YAlO 3 in an X-ray diffractometry. Of peaks exhibited in the X-ray diffractometry, the peak assigned to the (112) plane of orthorhombic YAlO 3 is a peak that has the highest peak intensity. Preferably, the value of the ratio of S2 to S1, S2/S1, is less than 1 in an X-ray diffractometry using CuKα radiation, where SI represents the peak intensity of the peak assigned to the (112) plane of orthorhombic YAlO 3 and S2 represents the peak intensity of the peak assigned to the (104) plane of trigonal Al 2 O 3 .

Claims (13)

1. A powder for coating or sintering,

wherein, in an X-ray diffractometry of the powder, a peak assigned to orthorhombic YAlO 3 , and a peak assigned to cubic Y 3 Al 5 O 12 or monoclinic Y 4 Al 2 O 9 are exhibited,

of peaks exhibited in the X-ray diffractometry, a peak assigned to a (112) plane of orthorhombic YAlO 3 is a peak that has the highest peak intensity,

in an X-ray diffractometry using CuKα radiation, a value of a ratio of S3 to S1, S3/S1, and a value of a ratio of S4 to S1, S4/S1, are each independently less than 1, where S 1 represents a peak intensity of a peak assigned to a (112) plane of orthorhombic YAlO 3 , S3 represents a peak intensity of a peak assigned to a (420) plane of cubic Y 3 Al 5 O 12 , and S4 represents a peak intensity of a peak assigned to a (−221) plane of monoclinic Y 4 Al 2 O 9 , and

in a pore volume distribution relative to pore sizes as measured by mercury intrusion porosimetry, the powder exhibits at least one peak in each of a range of pore sizes from 0.1 to 1 μm and a range of pore sizes from 5 to 50 μm, a volume of pores with a pore size from 0.1 to 1 μm is 0.1 mL/g or greater, and a volume of pores with a pore size from 5 to 50 μm is 0.1 mL/g or greater.

2. The powder for coating or sintering according to claim 1 ,

wherein, in the X-ray diffractometry of the powder, no peak assigned to trigonal Al 2 O 3 is exhibited, or if a peak assigned to trigonal Al 2 O 3 is exhibited, a value of a ratio of S2 to S1, S2/S1, is less than 1 in an X-ray diffractometry using CuKα radiation, where S1 represents a peak intensity of a peak assigned to a (112) plane of orthorhombic YAlO 3 and S2 represents a peak intensity of a peak assigned to a (104) plane of trigonal Al 2 O 3 .

3. The powder for coating or sintering according to claim 1 ,

wherein, in the X-ray diffractometry of the powder, no peak assigned to cubic Y 2 O 3 is exhibited, or if a peak assigned to cubic Y 2 O 3 is exhibited, a value of a ratio of S5 to S1, S5/S1, is 1 or less in an X-ray diffractometry using CuKα radiation, where S1 represents a peak intensity of a peak assigned to a (112) plane of orthorhombic YAlO 3 , and S5 represents a peak intensity of a peak assigned to a (222) plane of cubic Y 2 O 3 .

4. The powder for coating or sintering according to claim 1 , having a crystallite size of 50 nm or greater as determined from a full width at half maximum of the peak assigned to a (112) plane of orthorhombic YAlO 3 in the X-ray diffractometry of the powder.

5. The powder for coating or sintering according to claim 1 , having a BET specific surface area of 1 to 5 m 2 /g.

6. The powder for coating or sintering according to claim 1 , wherein the powder is granular and has an average particle size of 15 μm or greater.

7. A method for producing a coating, comprising forming a coating of the powder for coating or sintering according to claim 1 by thermal spraying or PVD.

Assignments (3)
CHANGE OF NAME Recorded Mar 31, 2026
From: MITSUI MINING AND SMELTING COMPANY, LIMITED
To: MITSUI KINZOKU COMPANY, LIMITED
Reel/Frame 075357/0342 →
MERGER AND CHANGE OF NAME Recorded May 21, 2025
From: NIPPON YTTRIUM CO., LTD.; MITSUI MINING & SMELTING CO., LTD.
To: MITSUI MINING & SMELTING CO., LTD.
Reel/Frame 071344/0177 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Sep 23, 2022
From: MATSUKURA, KENTO; TATEOKA, SHUICHI; OGAWA, HIROCHIKA
To: NIPPON YTTRIUM CO., LTD.
Reel/Frame 061194/0294 →
Priority Claims (1)
JP 2020-084052 · May 12, 2020 · national
Continuity (1)
Related Publication 20230133847A1 · May 4, 2023
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