IP Library Granted Patent US 11,918,701
Granted Patent B2
US 11,918,701 · App. 17/947,265 · Granted Mar 5, 2024

Polymer coating for medical devices and method of manufacture thereof

Inventor: Alex Hill (South Windsor, CT)
Assignee: MOTT CORPORATION
A61L27/34A61L27/56A61L2400/12A61L2420/02
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Quick Facts
Patent No.
US 11,918,701
App. No.
17/947,265
Granted
Mar 5, 2024
Kind
B2
Abstract

Disclosed herein is a bio-resistant article comprising a porous metal substrate; a self-assembled monolayer disposed on the substrate; wherein the self-assembled monolayer comprises a coupling agent that has a first end that is reactively bonded to the porous metal substrate and a second end that is reactively bonded to a zwitterionic polymer. Disclosed herein too is a method comprising disposing upon a porous metal substrate a self-assembled monolayer; and bonding the zwitterionic polymer to the self-assembled monolayer.

Claims (19)

1. A bio-resistant article comprising:

a porous metal substrate;

a self-assembled monolayer disposed on the substrate; wherein the self-assembled monolayer comprises a coupling agent that has a first end that is reactively bonded to the porous metal substrate and a second end that is reactively bonded to a zwitterionic polymer,

wherein the article is a sparger.

2. The bio-resistant article of claim 1 , wherein the porous metal surface comprises a metal; wherein the metal comprises iron, zinc, magnesium, aluminum, gold, platinum, stainless steel, titanium, tantalum, iridium, molybdenum, niobium, palladium, chromium, or alloys thereof.

3. The bio-resistant article of claim 1 , wherein the porous metal surface has an average pore diameter of about 10 nanometers to about 100 micrometers.

4. The bio-resistant article of claim 3 , wherein the porous metal surface has an average pore diameter of about 100 nanometers to about 1 micrometer.

5. The bio-resistant article of claim 1 , wherein the porous metal surface comprises a metal oxide; wherein the metal oxide comprises tantalum oxide, titanium oxide, iridium oxide, niobium oxide, zirconium oxide, tungsten oxide, rhodium oxide, or a combination thereof.

6. The bio-resistant article of claim 1 , wherein the first end comprises a first reactive functionality that comprises a silane, a thiol, a carboxyl, an amide, an imide, an ester, a sulfate ester, a phosphate ester, a thiophosphate ester, a borate ester, a urea, an epoxide, a carbamate, a thiocarbamate, a thiosulfate, a sulfonate, a phosphonate, a halogen thiophosphonate, a nitro, a nitroso, a nitrate, a nitrite, or a combination thereof.

7. The bio-resistant article of claim 1 , wherein the zwitterionic polymer is polymerized from a monomer by a reactive initiator located at the second end of the coupling agent.

8. The bio-resistant article of claim 1 , wherein the zwitterionic polymer is polyphosphorylcholine, polysulfobetaine, polycarboxybetaine, polytrimethylamine N-oxide, or a combination thereof.

9. The bio-resistant article of claim 1 , wherein the zwitterionic polymer is polytrimethylamine N-oxide.

10. The bio-resistant article of claim 9 , wherein the zwitterionic polymer forms a layer that is less than 1000 nanometers thick.

11. A method for fabricating an article comprising:

disposing upon a porous metal substrate a self-assembled monolayer; and

bonding a zwitterionic polymer to the self-assembled monolayer;

wherein the article is a sparger.

12. The method of claim 11 , further comprising reactively bonding the self-assembled monolayer to the substrate.

13. The method of claim 12 , further comprising initiating polymerization of the zwitterionic polymer via a reactive initiating functionality disposed on an end of the self-assembled monolayer.

Assignments (4)
SECURITY INTEREST Recorded Oct 14, 2025
From: PNC BANK, NATIONAL ASSOCIATION, AS ADMINISTRATIVE AGENT
To: MOTT CORPORATION; DIGESTED ORGANICS LLC
Reel/Frame 072559/0785 →
SECURITY INTEREST Recorded Apr 18, 2024
From: MOTT CORPORATION; DIGESTED ORGANICS LLC
To: PNC BANK, NATIONAL ASSOCIATION, AS ADMINISTRATIVE AGENT
Reel/Frame 067162/0539 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Mar 13, 2023
From: HILL, ALEX
To: MOTT CORPORATION
Reel/Frame 062961/0243 →
SECURITY INTEREST Recorded Feb 14, 2023
From: MOTT CORPORATION
To: PNC BANK, NATIONAL ASSOCIATION, AS ADMINISTRATIVE AGENT
Reel/Frame 062695/0152 →
Continuity (2)
Provisional Application 63246012 · Sep 20, 2021
Related Publication 20230087962A1 · Mar 23, 2023