IP Library Granted Patent US 11,935,975
Granted Patent B2
US 11,935,975 · App. 18/074,665 · Granted Mar 19, 2024

Methods of producing a photovoltaic junction including ligand exchange of quantum dots of a film

Inventors: Mathew Kelley (Columbia, SC); Andrew B. Greytak (Columbia, SC); Mvs Chandrashekhar (Lexington, SC); Joshua Letton (Columbia, SC)
Assignee: UNIVERSITY OF SOUTH CAROLINA
H01L31/035218H01L31/022408H01L31/03048H01L31/0312H01L31/0324H01L31/0336H01L31/07H01L31/108H01L31/18H01L31/1848H10K30/00
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Quick Facts
Patent No.
US 11,935,975
App. No.
18/074,665
Granted
Mar 19, 2024
Kind
B2
Abstract

The present disclosure is directed to methods for producing a photovoltaic junction that can include coating a bare junction with a composition. In one embodiment, the composition includes a plurality of quantum dots to create a film; exposing the film to a ligand to create a first layer; coating the first layer with the composition to form a film on the first layer; and exposing the film on the first layer to the ligand to create a second layer.

Claims (22)

1. A method for producing a photovoltaic junction, the method comprising:

applying a metallic contact to a first surface area of a semiconductor layer to form a first physical junction between a first surface area of the metallic contact and the first surface area of the semiconductor layer, the first physical junction forming a Schottky diode;

coating a second surface area of the semiconductor layer and a second surface area of the metallic contact with a composition including a plurality of ligand-protected quantum dots;

carrying out a ligand-exchange with the ligand-protected quantum dots to form a light absorbing layer, wherein a second physical junction exists between a first surface area of the light absorbing layer and the second surface area of the semiconductor layer and a third physical junction exists between a second surface area of the light absorbing layer and the second surface area of the metallic contact, the second physical junction forming a diode that exhibits Shockley-Read Hall trap-assisted recombination, and the third physical junction forming an ohmic contact; wherein

the photovoltaic junction exhibits absorption across one or more wavelengths in the range from about 200 nm to about 2000 nm.

2. The method of claim 1 , wherein the composition is spin coated on the second surface area of the semiconductor layer and the second surface area of the metallic contact.

3. The method of claim 1 , wherein the composition is painted on the second surface area of the semiconductor layer and the second surface area of the metallic contact.

4. The method of claim 1 , wherein the semiconductor layer comprises a nitride or a carbide.

5. The method of claim 1 , wherein the semiconductor layer comprises a semiconductor that has a bandgap greater than a bandgap of the light absorbing layer.

6. The method of claim 1 , wherein the ligand exchange comprises exchanging a 1,2-ethane dithiol with a ligand of the ligand-protected quantum dots.

7. The method of claim 1 , wherein the ligand-protected quantum dots comprise lead sulfide quantum dots.

8. The method of claim 1 , wherein the light absorbing layer has thickness from about 8 nm to about 400 nm.

9. The method of claim 1 , wherein the light absorbing layer has a thickness of from about 10 nm to about 300 nm.

10. The method of claim 1 , wherein the semiconductor layer has a thickness that is greater than the thickness of the light absorbing layer.

11. The method of claim 1 , wherein the semiconductor layer has a thickness that is from about 5 micrometers to about 200 micrometers.

12. The method of claim 1 , wherein the metallic contact comprises graphene, graphite, or a metal.

13. The method of claim 1 , further comprising:

coating the light absorbing layer with a further amount of the composition including the plurality of ligand-protected quantum dots; and

carrying out a ligand-exchange with the ligand-protected quantum dots and thereby increasing the thickness of the light absorbing layer.

14. The method of claim 13 , further comprising repeating the coating and ligand-exchange steps one or more additional times.

15. The method of claim 1 , wherein the metallic contact includes multiple monolayers of graphene.

16. The method of claim 1 , wherein the ligand-protected quantum dots comprise alkyl carboxylate coated quantum dots.

Assignments (1)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Dec 5, 2022
From: KELLEY, MATHEW; GREYTAK, ANDREW B.; CHANDRASHEKHAR, MVS; LETTON, JOSHUA
To: UNIVERISTY OF SOUTH CAROLINA
Reel/Frame 061973/0365 →
Continuity (3)
Division 16857687 · Apr 24, 2020
Provisional Application 62866857 · Jun 26, 2019
Related Publication 20230223485A1 · Jul 13, 2023