IP Library Granted Patent US 12,009,509
Granted Patent B2
US 12,009,509 · App. 18/101,663 · Granted Jun 11, 2024

Solvents and catalyst preparations for lithium-oxygen batteries

Inventors: Hsien-Han Wang (Downers Grove, IL); Ritesh Jagatramka (Chicago, IL); Samuel Plunkett (Chicago, IL); Larry A. Curtiss (Downers Grove, IL); Khalil Amine (Oak Brook, IL)
Assignee: UCHICAGO ARGONNE, LLC
H01M4/366H01M4/134H01M4/382H01M4/62H01M4/885H01M4/8882H01M4/926H01M12/08H01M2004/027H01M2004/028H01M2300/0028H01M2300/0037
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Quick Facts
Patent No.
US 12,009,509
App. No.
18/101,663
Granted
Jun 11, 2024
Kind
B2
Abstract

An electrochemical device includes a lithium anode having a red poly(benzonitrile) coating covering at least a portion of the anode; a separator and an air cathode comprising reduced graphene oxide over gas diffusion layer; and an electrolyte comprising an ether solvent, benzonitrile, and a lithium salt.

Claims (5)

1. A method of preparing a lithium-oxygen battery, the method comprising:

providing a lithium anode, an air cathode comprising reduced graphene oxide, and an electrolyte comprising an ether solvent, benzonitrile, and a lithium salt forming an electrochemical cell; and

cycling the electrochemical cell to form a coating of red poly(benzonitrile) on at least a portion of the lithium anode.

2. The method of claim 1 further comprising prior to cycling, exposing the electrochemical cell to CO 2 and cycling the cell to deposit a coating of Li 2 CO 3 on at least a portion of the lithium anode.

3. The method of claim 2 , where in the cycling in the presence of CO 2 is conducted for at least three cycles.

Assignments (2)
CONFIRMATORY LICENSE Recorded Aug 13, 2024
From: UCHICAGO ARGONNE LLC
To: U.S. DEPARTMENT OF ENERGY
Reel/Frame 068590/0177 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jan 26, 2023
From: AMINE, KHALIL; CURTISS, LARRY A.; JAGATRAMKA, RITESH; PLUNKETT, SAMUEL; WANG, HSIEN-HAU
To: UCHICAGO ARGONNE, LLC
Reel/Frame 062496/0365 →
Continuity (2)
Division 16941249 · Jul 28, 2020
Related Publication 20230170473A1 · Jun 1, 2023