LIGHT-WEIGHT FAST-DRY SELF-LEVELING CEMENTITIOUS GYPSUM UNDERLAYMENT WITH PARTICLE FILLERS
Stucco-cement compositions with a shortened drying time, lighter weight, high strength and reduced expansion, the compositions comprising expanded perlite and preferably also calcium aluminate cement and/or calcium sulfoaluminate cement, and methods for making and using these compositions, including pourable and/or pumpable floor underlayment slurries and methods for forming high strength underlayment on different substrates.
1 . A composition for cementitious gypsum underlayment, wherein the composition is a dry mixture and comprises:
a) stucco;
b) expanded perlite in an amount ranging from about 0.5 wt % to about 15 wt %;
c) optionally, hydraulic cement comprising one or more of the following cements:
Portland cement, calcium aluminate cement, calcium sulfoaluminate cement or any combination therefore, wherein the hydraulic cement is in an amount from about 0.5 to about 20 wt %;
d) a plasticizer;
e) a stabilizer comprising one or more polysaccharide gums; and
f) a defoamer.
2 . The composition of claim 1 , wherein the expanded perlite is coated with a silicone, silane or siloxane coating.
3 . The composition of claim 1 , wherein the expanded perlite is coated with a silicone, silane or siloxane coating and has a relative density in the range from about 0.112 g/cm 3 to about 0.350 g/cm 3 , particle sizes ranging from about 1 μm to about 150 μm, and an average particle size less than 45 μm.
4 . The composition of claim 1 , wherein the expanded perlite is coated with an organometallic silane monomer coating or an organometallic silicone polymer coating.
5 . The composition of claim 1 , wherein the composition comprises Portland cement in an amount from about 0.5 wt % to about 20 wt %, or calcium aluminate cement in an amount from about 0.5 wt % to about 20 wt %.
6 . The composition of claim 1 , wherein the plasticizer comprises a polycarboxylate ether (PCE) dispersant in an amount from about 0.1 wt % to about 1 wt % and/or sodium lignosulfonate in an amount from about 0.05 wt % to about 0.5 wt %.
7 . The composition of claim 1 , wherein the stabilizer comprises diutan gum.
8 . The composition of claim 1 , wherein the polysaccharide gum includes one or more of the following: xanthan gum, welan gum and/or diutan gum.
9 . The composition of claim 1 , wherein the composition consists essentially of:
82-90 wt % stucco;
1-15 wt % expanded perlite having an average particle size ranging from about 30 to about 37 μm and having a relative density ranging from about 0.244 g/cm 3 to about 0.350 g/cm 3 ;
2-10 wt % Portland cement;
1-10 wt % calcium aluminate cement and/or calcium sulfoaluminate cement;
0.1-1 wt % Polycarboxylate ether (PCE) based dispersant;
0.05-0.5 wt % lignosulfonate;
0.01-0.1 wt % polysaccharide gum; and
0.1-0.5 wt % defoamer.
10 . The composition of claim 1 , wherein the composition further comprises at least one of the following: a set accelerator, a set retarding agent, or any combination thereof.
11 . The composition of claim 1 , wherein the composition further comprises sand and wherein the sand-to-the-composition ratio by weight is in the range from about 1:1 w/w to about 4:1 w/w.
12 . The composition of claim 1 , wherein the composition further comprises one or more of the following aggregates: sand, lime, calcium carbonate, rock, gravel, silica fume, clay, pumice, vermiculite, fly ash, slag, silica fume, or any combination thereof.
13 . The composition of claim 1 , wherein the composition further comprises hollow glass, glass and/or borosilicate microspheres in addition to or instead of expanded perlite.
14 . A gypsum cement slurry comprising:
a) the composition of claim 1 ;
b) sand; and
c) water in an amount ranging from about 100 cc to about 400 cc of water per 1,000 grams of the composition and sand;
wherein a ratio of sand to the composition is in the range from 0.8:1 to 2.3:1 cubic feet of sand per an 80 lb of the composition.
15 . A method for making a gypsum cement slurry, the method comprising: mixing the composition of claim 1 with water.
16 . A method for producing floor or floor underlayment, the method comprising:
i. mixing a gypsum cement slurry comprising the composition of claim 1 , water and sand in a mixing vessel, wherein water is used in an amount from about 150 cubic centimeters (cc) to about 300 cubic centimeters (cc) per 1,000 grams of the composition and sand; and wherein the weight by weight (w/w) ratio of the sand to the composition is in the range from 1:1 to 4:1; and
ii. applying the gypsum cement slurry to a substrate.
17 . The method of claim 16 , wherein the gypsum cement slurry is applied by pumping the gypsum cement slurry through a hose or by dumping out of a reservoir.
18 . The method of claim 16 , wherein the mixing further comprises adding one or more set retarders and/or set accelerators to the gypsum cement slurry.
19 . The method of claim 16 , wherein the slurry is applied to the substrate at the ¾ inch to 4 inch thickness.
20 . The method of claim 16 , wherein the underlayment has a compressive strength of at least 1,800 psi.