IP Library Granted Patent US 11,957,048
Granted Patent B2
US 11,957,048 · App. 18/163,528 · Granted Apr 9, 2024

Key materials for organic photovoltaics reliability

Inventors: Stephen R. Forrest (Ann Arbor, MI); Yongxi Li (Ann Arbor, MI)
H10K85/657H10K30/81
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Quick Facts
Patent No.
US 11,957,048
App. No.
18/163,528
Granted
Apr 9, 2024
Kind
B2
Abstract

Organic photovoltaic cells (OPVs) and their compositions are described herein. one or more embodiments, the acceptor with an active layer of an OPV includes is a non-fullerene acceptor. Such non-fullerene acceptors may provide improved OPV performance characteristics such as improved power conversion efficiency, open circuit voltage, fill factor, short circuit current, and/or external quantum efficiency.

Claims (84)

1. A compound having a structure represented by one of the Formulae (I)-(VI):

wherein:

A and B are individually selected from the group consisting of:

each Ar 1 is individually selected from the group consisting of:

each Ar 2 is individually selected from the group consisting of:

each Ar 3 is individually selected from the group consisting of:

each Ar 4 is individually selected from the group consisting of:

M 1 -M 4 are individually selected from the group consisting of hydrogen, fluorine, chlorine, bromine, iodine, astatine, and a cyano group, wherein at least one of M 1 -M 4 is a halogen;

each X is individually selected from the group consisting of S, NR, Se, Te, and O;

each R is individually a C 1 -C 20 hydrocarbon or an aromatic hydrocarbon;

each Y is individually selected from the group consisting of:

each m is an integer from 0 to 10; and

each n is an integer from 0 to 10.

2. The compound of claim 1 , wherein each Ar 1 , each Ar 3 or each Ar 1 and Ar 3 is:

3. The compound of claim 1 , wherein A or B is:

4. The compound of claim 1 , wherein Ar 4 is:

5. The compound of claim 1 , wherein A or B is:

6. The compound of claim 1 , wherein at least one of M 1 -M 4 is chloride.

7. The compound of claim 1 , wherein each R is selected from the group consisting of:

8. The compound of claim 1 , wherein each R is 2-ethylhexyl.

9. The compound of claim 1 , wherein each Y is:

10. The compound of claim 1 , wherein the compound has one of formulae (Ia), (Ib), (IIIa) and (IIIb):

wherein:

each X is independently selected from the group consisting of S, NR, Se, Te, and O;

each R is independently selected from a C 1 -C 20 hydrocarbon, an aromatic hydrocarbon wherein the hydrocarbon, and aromatic hydrocarbon are each optionally substituted;

each R′ is independently a halogen; and

each p is independently an integer from 0-4.

11. The compound of claim 1 , wherein the compound is selected from the group consisting of:

12. An organic photovoltaic device comprising:

an anode;

a cathode; and

an organic layer, disposed between the anode and the cathode, comprising a compound having a structure represented by one of the Formulae (I)-(VI):

wherein:

A and B are individually selected from the group consisting of:

each Ar 1 is individually selected from the group consisting of:

each Ar 2 is individually selected from the group consisting of:

each Ar 3 is individually selected from the group consisting of:

each Ar 4 is individually selected from the group consisting of:

M 1 -M 4 are individually selected from the group consisting of hydrogen, fluorine, chlorine, bromine, iodine, astatine, and a cyano group, wherein at least one of M 1 -M 4 is a halogen;

each X is individually selected from the group consisting of S, NR, Se, Te, and O;

each R is individually a Ci-Cao hydrocarbon or an aromatic hydrocarbon;

each Y is individually selected from the group consisting of:

each m is an integer from 0 to 10; and

each n is an integer from 0 to 10.

13. The organic photovoltaic device of claim 12 , wherein each R is independently selected from the group consisting of

14. The organic photovoltaic device of claim 12 , wherein the device further comprises at least one selected from the group consisting of hole transporting layer, an electrode transporting layer, an anode buffer, and a cathode buffer.

15. The organic photovoltaic device of claim 14 , wherein the cathode buffer comprises a material selected from the group consisting of:

wherein each X is individually selected from the group consisting of oxygen, carbon, hydrogen, sulfur, selenium, and nitrogen;

each Y is individually selected from the group consisting of:

each Ar 1 is independently selected from the group consisting of:

M 1 -M 4 are each independently selected from the group consisting of hydrogen, fluorine, chlorine, bromine, iodine, astatine, and a cyano group, wherein at least one of M 1 -M 4 is a halogen; and

each R is independently a C 1 -C 20 hydrocarbon or an aromatic hydrocarbon.

16. The organic photovoltaic device of claim 14 , wherein the cathode buffer comprises a material selected from the group consisting of:

wherein each AO is independently selected from the group consisting of:

M 1 -M 4 are each independently selected from the group consisting of hydrogen, fluorine, chlorine, bromine, iodine, astatine, and a cyano group, wherein at least one of M 1 -M 4 is a halogen; and

each R is independently a C 1 -C 20 hydrocarbon or an aromatic hydrocarbon.

17. The organic photovoltaic device of claim 14 , wherein the anode buffer comprises a material selected from the group consisting of:

18. A formulation comprising the compound of claim 1 .

19. A composition comprising a compound represented by one of formulae (I)-(VI) and at least one of a cathode buffer and an anode buffer:

wherein:

A and B are individually selected from the group consisting of:

each Ar 1 is individually selected from the group consisting of:

each Ar 2 is individually selected from the group consisting of:

each Ar 3 is individually selected from the group consisting of:

each Ar 4 is individually selected from the group consisting of:

M 1 -M 4 are individually selected from the group consisting of hydrogen, fluorine, chlorine, bromine, iodine, astatine, and a cyano group, wherein at least one of M 1 -M 4 is a halogen;

each X is individually selected from the group consisting of S, NR, Se, Te, and O;

each X A is individually selected from the group consisting of CRR, O, S, Se and NR;

each R is individually a Ci-Cao hydrocarbon or an aromatic hydrocarbon;

each Y is individually selected from the group consisting of:

each m is an integer from 0 to 10; and

each n is an integer from 0 to 10;

the anode buffer comprises a material selected from the group consisting of:

 and

the cathode buffer comprises a material selected from the group consisting of:

wherein each X is individually selected from the group consisting of oxygen, carbon, hydrogen, sulfur, selenium, and nitrogen;

each Y is individually selected from the group consisting of:

each Ar 1 is independently selected from the group consisting of:

M 1 -M 4 are each independently selected from the group consisting of hydrogen, fluorine, chlorine, bromine, iodine, astatine, and a cyano group, wherein at least one of M 1 -M 4 is a halogen; and

each R is independently a C 1 -C 20 hydrocarbon or an aromatic hydrocarbon; or

wherein the cathode buffer comprises a material selected from the group consisting of:

each Ar 1 is independently selected from the group consisting of:

M 1 -M 4 are each independently selected from the group consisting of hydrogen, fluorine, chlorine, bromine, iodine, astatine, and a cyano group, wherein at least one of M 1 -M 4 is a halogen; and

each R is independently a C 1 -C 20 hydrocarbon or an aromatic hydrocarbon.

Assignments (2)
CONFIRMATORY LICENSE Recorded Jan 16, 2024
From: UNIVERSITY OF MICHIGAN
To: UNITED STATES DEPARTMENT OF ENERGY
Reel/Frame 066306/0655 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Nov 28, 2023
From: HUANG, XIAHENG; LI, YONGXI; FORREST, STEPHEN R.
To: THE REGENTS OF THE UNIVERSITY OF MICHIGAN
Reel/Frame 065683/0647 →
Continuity (3)
Continuation 17515690 · Nov 1, 2021
Provisional Application 63109459 · Nov 4, 2020
Related Publication 20230180602A1 · Jun 8, 2023