IP Library › Granted Patent US 12,703,647
Granted Patent B2
US 12,703,647 · App. 18/176,630 · Granted Aug 11, 2026

Accelerated synthesis of nickel-rich cathode materials using flame-assisted spray pyrolysis

Inventors: Sili Deng (Cambridge, MA); Jianan Zhang (Cambridge, MA); Valerie L Muldoon (Cambridge, MA)
Assignee: Massachusetts Institute of Technology
C01G53/50C01G53/82C01P2006/40
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Quick Facts
Patent No.
US 12,703,647
App. No.
18/176,630
Filed
Mar 1, 2023
Granted
Aug 11, 2026
Kind
B2
Art Unit
1722
USPC
429/223
Abstract

Methods of synthesis of nickel-rich cathode materials can include preheating droplets, decomposing the droplets in a burner, collecting solid particles, and calcinating the solid particles.

Claims (37)

1 . A method of synthesis of a nickel-rich cathode material comprising:

i) preparing a precursor solution by dissolving lithium nitrate, nickel nitrate, manganese nitrate, and cobalt nitrate in water;

ii) aerosolizing the precursor solution in a stream of air using an ultrasonic sprayer to form droplets;

iii) preheating the droplets;

iv) generating a flame in a burner;

v) decomposing the droplets by passing through the burner;

vi) depositing solid particles on a powder collector; and

vii) calcinating the solid particles in a furnace in the presence of an oxidizing agent for up to 20 minutes at about 875° C.

2 . The method of claim 1 , further comprising adding excess LiNO 3 to the precursor solution.

3 . The method of claim 1 , wherein the precursor solution includes urea.

4 . The method of claim 1 , wherein the nickel-rich cathode material comprises lithium-nickel-cobalt-manganese oxide (NCM).

5 . The method of claim 1 , wherein the nickel nitrate of the precursor solution includes nickel nitrate hexahydrate (Ni(NO 3 ) 2 ·6H 2 O).

6 . The method of claim 1 , wherein the manganese nitrate of the precursor solution includes manganese nitrate tetrahydrate (Mn(NO 3 ) 2 ·4H 2 O).

7 . The method of claim 1 , wherein the cobalt nitrate of the precursor solution includes cobalt nitrate hexahydrate (Co(NO 3 ) 2 ·6H 2 O).

8 . The method of claim 1 , wherein the droplets are passed through the co-flow burner at a flow rate of about 10 L/min.

9 . The method of claim 1 , wherein the nickel-rich cathode material comprises an ordered layered structure.

10 . The method of claim 1 , wherein the nickel-rich cathode material comprises LiNi 0.8 Co 0.1 Mn 0.1 O 2 (NCM811) or LiNi 0.6 Co 0.2 Mn 0.2 O 2 (NCM822).

11 . The method of claim 10 , wherein the nickel-rich cathode material has a discharge capacity of about 198.3 mAh/g (1st cycle at 0.1 C).

12 . The method of claim 10 , wherein the nickel-rich cathode material has a capacity retention ratio of about 63.15% after 50 cycles at 1 C.

13 . The method of claim 1 , comprising a liquid-feed flame assisted spray pyrolysis (FASP) method.

14 . The method of claim 1 , wherein the method is a continuous-flow process.

15 . The method of claim 1 , wherein the ultrasonic sprayer is a 1.7 MHz ultrasonic sprayer.

16 . The method of claim 1 , wherein the preheating of the aerosolized droplets comprises heating by passage through two low-temperature preheating sections.

17 . The method of claim 1 , wherein depositing the solid particles on a powder collector comprises depositing the solid particles on a glass-fiber filter.

18 . A method of synthesis of a nickel-rich cathode material comprising:

i) forming droplets of a precursor solution including a nickel salt in a stream of air;

ii) preheating the droplets;

iii) generating a flame in a burner;

iv) decomposing the droplets by passing through the burner;

v) collecting solid particles on a powder collector; and

vi) calcinating the solid particles in a furnace in the presence of an oxidizing agent for up to 20 minutes at about 875°C.

19 . The method of claim 18 , wherein the precursor solution includes urea.

20 . The method of claim 18 , wherein the nickel-rich cathode material comprises lithium-nickel-cobalt-manganese oxide (NCM).

21 . The method of claim 18 , wherein the droplets are passed through a preheating zone at a flow rate of between 5 L/min and 20 L/min.

22 . The method of claim 21 , wherein the droplets are passed through the preheating zone at a flow rate of about 10 L/min.

23 . The method of claim 18 , wherein preheating the droplets includes tuning the morphology and electrochemical performance of the nickel-rich cathode material by adjusting a preheating temperature and preheating time.

24 . The method of claim 18 , wherein preheating the droplets includes exposing the droplets to a temperature of 125° C. to 325°C.

Assignments (1)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Aug 30, 2023
From: DENG, SILI; MULDOON, VALERIE L.; ZHANG, JIANAN
To: MASSACHUSETTS INSTITUTE OF TECHNOLOGY
Reel/Frame 064750/0879 →
Continuity (2)
Provisional Application 63317130 · Mar 7, 2022
Related Publication 20230278888A1 · Sep 7, 2023
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