IP Library Granted Patent US 12,241,153
Granted Patent B2
US 12,241,153 · App. 18/207,721 · Granted Mar 4, 2025

Sputtering target and manufacturing method therefor

Inventors: Tomio Otsuki (Ibaraki, JP); Yasushi Morii (Ibaraki, JP)
Assignee: JX Advanced Metals Corporation
C23C14/3414C22C9/01C22C9/05C22C9/06C22F1/08
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Quick Facts
Patent No.
US 12,241,153
App. No.
18/207,721
Granted
Mar 4, 2025
Kind
B2
Abstract

A sputtering target according to one embodiment is an integrated sputtering target comprising a target portion and a backing plate portion, both of them being made of copper and unavoidable impurities, wherein a Vickers hardness Hv is 90 or more, and wherein a flat ratio of crystal grains in a cross section orthogonal to a sputtering surface is 0.35 or more and 0.65 or less.

Claims (13)

1. An integrated sputtering target comprising a target portion and a backing plate portion, both of them containing from 0.1% by mass to 8% by mass of at least one element selected from aluminum, manganese, nickel and cobalt, the balance being copper and unavoidable impurities, wherein a Vickers hardness Hv is 90 or more, and wherein a flat ratio of crystal grains in a cross section orthogonal to a sputtering surface to be used for sputtering is 0.35 or more and 0.85 or less.

2. The sputtering target according to claim 1 , wherein the sputtering target has an average crystal grain size of 5 μm or more and 50 μm or less.

3. The sputtering target according to claim 1 , wherein the target portion and the backing plate portion further contain one or more elements selected from the group consisting of Fe, Cr, Si, Ag, S, and P in a total nonzero amount of 0.01% by mass or less.

4. The sputtering target according to claim 1 , wherein the sputtering target contains from 0.1% by mass to 6% by mass of at least one element selected from aluminum, manganese, nickel, and cobalt.

5. A method for manufacturing the integrated sputtering target according to claim 1 , the method comprising:

melting a raw material to cast an ingot comprising the element, copper and the unavoidable impurities; and subjecting the ingot to hot forging, first cold rolling or first cold forging, a heat treatment, and a second cold rolling or a second cold forging in this order,

wherein the second cold rolling or the second cold forging is carried out at a change rate of from 20% to 60%, and

wherein in the second cold rolling or the second cold forging, crystal grains are crushed in a thickness direction to change a flat ratio of the crystal grains in a cross section orthogonal to a sputtering surface to be used for sputtering.

6. The method according to claim 5 , wherein the heat treatment is carried out at a temperature of from 200° C. to 500° C. for 0.5 hours to 3 hours.

7. The method according to claim 5 , wherein the first cold rolling or the first cold forging is carried out at a change rate of 70% or more.

8. The method according to claim 5 , wherein the hot forging is carried out at a temperature of from 300° C. to 900° C.

9. The method according to claim 5 , wherein the ingot further contains one or more elements selected from the group consisting of Fe, Cr, Si, Ag, S, and P in a total amount of 0.01% by mass or less.

10. The method according to claim 5 , wherein the method manufactures a sputtering target containing 0.1% by mass to 6% by mass of at least one element selected from aluminum, manganese, nickel, and cobalt.

Assignments (3)
CHANGE OF NAME Recorded Jan 23, 2025
From: JX NIPPON MINING AND METALS CORPORATION
To: JX METALS CORPORATION
Reel/Frame 069995/0785 →
CHANGE OF NAME Recorded Jan 23, 2025
From: JX METALS CORPORATION
To: JX ADVANCED METALS CORPORATION
Reel/Frame 069997/0026 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Oct 20, 2023
From: OTSUKI, TOMIO; MORII, YASUSHI
To: JX NIPPON MINING & METALS CORPORATION
Reel/Frame 065288/0339 →
Priority Claims (2)
JP 2017-068457 · Mar 30, 2017 · national
JP 2018-040212 · Mar 6, 2018 · national
Continuity (2)
Division 16491151
Related Publication 20230349035A1 · Nov 2, 2023
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