IP Library › Granted Patent US 11,866,349
Granted Patent B1
US 11,866,349 · App. 18/242,418 · Granted Jan 9, 2024

Method of chromium (CR

Inventors: Muhammad Aamir (Al-Ahsa, SA); Muhammad Hassan (Al-Ahsa, SA)
Assignee: KING FAISAL UNIVERSITY
C02F1/283B01J20/0237B01J20/20B01J20/3028B01J20/3078B01J20/3085B01J20/3214B01J20/3236C02F1/62A61K36/899B01J20/28009C02F1/683C02F2101/22
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Quick Facts
Patent No.
US 11,866,349
App. No.
18/242,418
Granted
Jan 9, 2024
Kind
B1
Abstract

A method of chromium removal from wastewater comprising providing a copper augmented biochar and contacting the copper augmented biochar with the wastewater to remove chromium from the wastewater. The copper augmented biochar can remove chromium from wastewater with about 99% efficiency in about 1 hour.

Claims (9)

1. A method of preparing copper augmented biochar comprising:

pyrolyzing wheat straw to provide a biochar; and

adding copper to the biochar to provide a copper augmented biochar, wherein adding the copper to the biochar comprises mixing CuSO 4 and water with the biochar while heating to form a heated solution; obtaining a wet biochar from the heated solution; and heating the wet biochar for a period of time ranging from about 1 hour to about 3 hours at a temperature ranging from about 550° C. to about 650° C. to provide the copper augmented biochar.

2. The method of claim 1 , wherein the wheat straw is dried and ground prior to pyrolyzing.

3. The method of claim 2 , wherein the wheat straw is ground to particle sizes ranging from about 0.3 mm to about 1.0 m-mm.

4. The method of claim 1 , wherein the wheat straw is pyrolyzed for a period of time ranging from about 1.5 hours to about 3 hours at a temperature ranging from about 400° C. to about 600° C.

5. The method of claim 1 , wherein the wheat straw is pyrolyzed for a period of time ranging from about 2 hours to about 2.5 hours at a temperature ranging from about 400° C. to about 600° C.

6. The method of claim 1 , wherein the wet biochar is heated in a muffle furnace for about 2 hours at about 600° C.

7. The method of claim 1 , wherein the pyrolyzing step occurs in a presence of nitrogen gas.

Assignments (1)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Sep 6, 2023
From: AAMIR, MUHAMMAD; HASSAN, MUHAMMAD
To: KING FAISAL UNIVERSITY
Reel/Frame 064816/0066 →