Method for continuous production of carbon nanotubes
The present disclosure relates to a method for the continuous production of carbon nanotubes, the method comprising: a mixture preparing step for mixing and stirring a solvent, a metal salt, a surfactant, a reducing agent, and a function improving agent to prepare an emulsion mixture; a gaseous mixture forming step for mixing the emulsion mixture with a carrier gas to form a gas phase mixture; and a reacting step for introducing the gas phase mixture into a heated reactor to form carbon nanotubes, wherein the diameter of the carbon nanotubes can be uniformly controlled, and the production yield of the carbon nanotubes can be increased.
1 . A method for continuous production of carbon nanotubes, the method comprising:
a liquid mixture forming step of mixing and stirring a solvent, a metal salt, a surfactant, a reducing agent, and a functional enhancer to prepare an emulsion mixture,
a gas phase mixture forming step of mixing the emulsion mixture with a carrier gas to form a gas phase mixture; and
a reacting step of introducing the gas phase mixture into a heated reactor to form carbon nanotubes,
wherein the functional enhancer comprises at least one indole, imidazole, and hectorite compounds.
2 . The method of claim 1 , wherein in the gas phase mixture forming step, a carbon source is additionally mixed.
3 . The method of claim 1 , wherein the liquid mixture forming step comprises:
a first mixing step of mixing and stirring the solvent, the metal salt, and the surfactant; and
a second mixing step of adding the reducing agent and the functional enhancer to the mixture obtained through the first mixing step.
4 . The method of claim 1 , wherein the solvent is at least one selected from the group consisting of aromatic hydrocarbons, aliphatic hydrocarbons, alcohol compounds, and water.
5 . The method of claim 1 , wherein the emulsion mixture comprises 0.01 to 5 parts by weight of the metal salt, 5 to 17 parts by weight of the surfactant, 0.02 to 10 parts by weight of the reducing agent, and 0.1 to 0.4 parts by weight of the functional enhancer based on 100 parts by weight of solvent.
6 . The method of claim 1 , wherein the functional enhancer is a mixture of a first compound selected from the group consisting of indole and imidazole and a second compound comprising a hectorite compound.