Granted Patent B2

US 12,427,439 · App. 18/253,058 · Granted Sep 30, 2025

Inventors: Justin Donghoon Lee (Richmond, CA); Benjamin Sparrow (Richmond, CA)

Assignee: SALTWORKS TECHNOLOGIES INC.

B01D9/0031B01D5/006B01D9/0059B01D9/0063B08B9/0321C02F1/041C02F1/5209F28G9/00B01D2009/0086B08B2209/032C02F2001/5218C02F2103/08C02F2209/02C02F2209/03C02F2209/40C02F2303/22

Abstract

Claims (48)

1. A process comprising:

a. producing salt solids and a distillate using a forced-circulation evaporative crystallizer, the crystallizer comprising:

i. a circulation pump for circulating a slurry resulting from evaporating a saltwater using the crystallizer;

ii. a heat exchanger fluidly coupled to the circulation pump to receive and heat the slurry;

iii. a separator fluidly coupled to the heat exchanger to receive the slurry after the heat exchanger has heated the slurry and to evaporate water from the slurry to produce water vapor for the distillate and the salt solids;

iv. a vapor processor fluidly coupled to the separator for processing the water vapor, wherein solids deposits accumulate during the producing of the salt solids within at least one of the circulation pump, the heat exchanger, or the separator;

b. measuring a solids deposits metric representative of an amount of the accumulated solids deposits;

c. determining that the solids deposits metric deviates from a baseline by at least a cleaning threshold;

d. based on the solids deposits metric, making determinations comprising determining a cleaning mode and determining at least one of:

i. a type of cleaning solution; or

ii. a duration for which the at least one of the circulation pump, the heat exchanger, or the separator is to be cleaned; and

e. cleaning the at least one of the circulation pump, the heat exchanger, or the separator in accordance with the determinations.

2. The process of claim 1 , wherein processing the water vapor comprises compressing the water vapor as a steam, and wherein the steam is directed to the heat exchanger to heat the slurry in the heat exchanger.

3. The process of claim 1 , wherein measuring the solids deposits metric comprises measuring a flow rate of the slurry through the circulation pump, and wherein the solids deposits metric is less than the baseline.

4. The process of claim 1 , wherein measuring the solids deposits metric comprises measuring a hydraulic pressure differential across the circulation pump, and wherein the solids deposits metric is greater than the baseline.

5. The process of claim 1 , wherein measuring the solids deposits metric comprises measuring a temperature differential across the heat exchanger, and wherein the solids deposits metric is less than the baseline.

6. The process of claim 1 , wherein measuring the solids deposits metric comprises measuring an amount of the distillate produced by the crystallizer, and wherein the solids deposit metric is less than the baseline.

7. The process of claim 3 , wherein the solids deposits metric deviates from the baseline by less than 15%, and wherein the saltwater is selected as the cleaning solution.

8. The process of claim 3 , wherein the solids deposits metric deviates from the baseline by between 15% to 20%, and wherein the distillate produced by the forced-circulation evaporative crystallizer is selected as the cleaning solution.

9. The process of claim 3 , wherein the solids deposits metric deviates from the baseline by more than 20%, and wherein a chemical solution comprising at least one of an acid solution, a base solution, a surfactant solution, or a chelating solution is selected as the cleaning solution.

10. The process of claim 3 , wherein the cleaning mode is determined to be cleaning the circulation pump, wherein at least one of the saltwater or the distillate produced by the crystallizer is selected as the cleaning solution, wherein the circulation pump is cleaned by flowing the cleaning solution through the circulation pump, and wherein production of the salt solids continues during cleaning.

11. The process of claim 5 , wherein the cleaning mode is determined to be forward flushing the heat exchanger, wherein at least one of the saltwater or a distillate produced by the crystallizer is selected as the cleaning solution, wherein the heat exchanger is cleaned by flowing the cleaning solution through the heat exchanger, and wherein production of the salt solids continues during cleaning.

12. The process of claim 11 , wherein the cleaning mode is determined to be back flushing the heat exchanger after the forward flushing of the heat exchanger fails to restore the solids deposits metric to within the cleaning threshold of the baseline, wherein at least one of the saltwater or a distillate produced by the crystallizer is selected as the cleaning solution, wherein the heat exchanger is cleaned by flowing the cleaning solution through the heat exchanger, and wherein production of the salt solids is paused during cleaning.

13. The process of claim 9 , wherein the cleaning mode is determined to be chemical cleaning of the heat exchanger, wherein the solids deposits metric comprises the temperature differential across the heat exchanger and deviates from the baseline by more than 20%, wherein the chemical solution is selected as the cleaning solution, wherein the heat exchanger is cleaned by flowing the cleaning solution through the heat exchanger, and wherein production of the salt solids is paused during cleaning.

14. The process of claim 13 , wherein the cleaning mode is determined to be chemical cleaning of a whole of the forced-circulation evaporative crystallizer, wherein the solids deposits metric further comprises at least one of the hydraulic pressure differential across the circulation pump, the amount of the distillate produced by the crystallizer, or the flow rate of the slurry through the circulation pump also deviating from the baseline by more than 20%, wherein the slurry within the crystallizer is transferred out of the crystallizer during cleaning, wherein a chemical solution is selected as the cleaning solution, wherein cleaning circulation is circulated through all of the circulation pump, heat exchanger, and separator, and wherein production of the salt solids is paused during cleaning.

15. A system comprising:

a. a forced-circulation evaporative crystallizer, the crystallizer comprising:

i. a circulation pump for circulating a slurry resulting from evaporating a saltwater using the crystallizer;

ii. a heat exchanger fluidly coupled to the circulation pump to receive and heat the slurry;

iii. a separator fluidly coupled to the heat exchanger to receive the slurry after the heat exchanger has heated the slurry and to evaporate water from the slurry to produce water vapor and salt solids;

iv. a vapor processor fluidly coupled to the separator for processing the water vapor, wherein solids deposits accumulate during the producing of the salt solids within at least one of the circulation pump, the heat exchanger, or the separator;

b. a cleaning sub-system comprising:

i. a cleaning solution container for storing a chemical solution;

ii. at least one conduit fluidly coupling the circulation pump, the heat exchanger, and the separator to a source of the saltwater and to the cleaning solution container;

iii. at least one valve disposed along the at least one conduit to permit selective flowing of at least one of the saltwater or the cleaning solution to the circulation pump, the heat exchanger, and the separator;

c. at least one sensor to measure a solids deposits metric representative of an amount of the solids deposits that have accumulated within the crystallizer;

d. a controller communicatively coupled to the at least one sensor, the crystallizer, and the cleaning sub-system, the controller configured to:

i. determine the solids deposits metric measured by the at least one sensor;

ii. determine that the solids deposits metric deviates from a baseline by at least a cleaning threshold; and

iii. based on the solids deposits metric, make determinations comprising determining a cleaning mode and determining at least one of:

1. a type of cleaning solution; or

2. a duration for which the at least one of the circulation pump, the heat exchanger, or the separator is to be cleaned; and

iv. clean the at least one of the circulation pump, the heat exchanger, or the separator in accordance with the determinations.

16. The system of claim 15 , wherein the vapor processor comprises a vapor compressor configured to compress the water vapor to generate a steam for the heat exchanger.

17. The system of claim 15 , wherein the at least one sensor comprises a flow sensor positioned to measure a flow rate of the slurry through the circulation pump, wherein the solids deposits metric comprises the flow rate of the slurry through the circulation pump, and wherein the solids deposits metric is less than the baseline.

18. The system of claim 15 , wherein the at least one sensor comprises a pair of pressure sensors positioned to measure a hydraulic pressure differential across the circulation pump, wherein the solids deposits metric comprises the hydraulic pressure differential across the circulation pump, and wherein the solids deposits metric is greater than the baseline.

19. The system of claim 15 , wherein the at least one sensor comprises a pair of temperature sensors positioned to measure a temperature differential across the heat exchanger, wherein the solids deposits metric comprises the temperature differential across the heat exchanger, and wherein the solids deposits metric is less than the baseline.

20. The system of claim 15 , wherein the at least one sensor comprises a flow sensor positioned to measure a flow rate of distillate produced by the crystallizer, wherein the solids deposits metric comprises the flow rate of the distillate produced by the crystallizer, and wherein the solids deposit metric is less than the baseline.

Assignments (1)

Continuity (2)

References Cited (21)