IP Library Granted Patent US 12,518,787
Granted Patent B2
US 12,518,787 · App. 18/285,527 · Granted Jan 6, 2026

Fluorine-containing ether compound, lubricant for magnetic recording medium, and magnetic recording medium

Inventors: Natsumi Shibata (Tokyo, JP); Naoya Fukumoto (Tokyo, JP); Ayano Asano (Tokyo, JP); Tsuyoshi Kato (Tokyo, JP); Takuma Kuroda (Tokyo, JP); Daisuke Yagyu (Tokyo, JP); Chizuru Kasahara (Tokyo, JP); Yutaka Tanji (Tokyo, JP)
Assignee: Resonac Corporation
G11B5/7257C08G65/226C10M107/38C10M2213/0606C10N2040/18C10N2050/025
View Patent ↗
Loading inventors, assignments & file history…
Monitor This Case
Get email alerts when status or documents change.
Order Certified Copies
Most orders are placed with the USPTO same day — all within 24 business hours.
Order via The Patent Place →
Pre-filled with this patent's details
Quick Facts
Patent No.
US 12,518,787
App. No.
18/285,527
Granted
Jan 6, 2026
Kind
B2
Abstract

The present invention provides a fluorine-containing ether compound represented by the following formula. R 1 —CH 2 —R 2 —CH 2 —R 3 —CH 2 —R 4 —CH 2 —R 5 —CH 2 —R 6 —CH 2 —R 7 (In Formula (1), R 2 , R 4 , and R 6 are perfluoropolyether chains, R 3 is Formula (2), R 5 is Formula (3), and R 1 and R 7 are each independently a terminal group having two or three polar groups, in which individual polar groups are bound to different carbon atoms and the carbon atoms to which the polar groups are bound are bound to each other via a linking group containing a carbon atom to which no polar group is bound).

Claims (46)

1 . A fluorine-containing ether compound represented by Formula (1) below,

R 1 —CH 2 —R 2 —CH 2 —R 3 —CH 2 —R 4 —CH 2 —R 5 —CH 2 —R 6 —CH 2 —R 7   (1)

(in Formula (1),

R 1 and R 7 are each independently a terminal group having two or three polar groups, in which individual polar groups are bound to different carbon atoms, wherein

the different carbon atoms, to which the individual polar groups are bound, are bound to each other via a linking group containing a carbon atom to which no polar group is bound,

R 2 , R 4 , and R 6 are the same or different perfluoropolyether chains,

R 3 is a linking group represented by Formula (2) below,

R 5 is a linking group represented by Formula (3) below),

(in Formula (2), a is an integer of 1 to 3 and b is an integer of 1 to 2, and in Formula (3), c is an integer of 1 to 3 and d is an integer of 1 to 2, provided that a in Formula (2) and c in Formula (3) are not 1 at the same time).

2 . The fluorine-containing ether compound according to claim 1 ,

wherein a in Formula (2) above is an integer of 2 to 3, and c in Formula (3) above is an integer of 2 to 3.

3 . The fluorine-containing ether compound according to claim 1 ,

wherein all of the polar groups in R 1 and R 7 in Formula (1) above are hydroxyl groups.

4 . The fluorine-containing ether compound according to claim 1 ,

wherein —R 1 and —R 7 in Formula (1) above are each independently a terminal group represented by Formulae (4-1) to (4-5) below,

(in Formula (4-1), e is an integer of 0 to 1 and f is an integer of 1 to 4),

(in Formula (4-2), g is an integer of 1 to 2 and h is an integer of 1 to 3),

(in Formula (4-3), i is an integer of 1 to 3), and

(in Formula (4-4), j is an integer of 1 to 2).

5 . The fluorine-containing ether compound according to claim 1 ,

wherein R 2 , R 4 , and R 6 in Formula (1) above are each independently any of Formulae (5) to (9) below,

—CF 2 O—(CF 2 CF 2 O) k —(CF 2 O) l —CF 2 —  (5)

(in Formula (5), k and 1 indicate the average degree of polymerization and each independently represent 0.1 to 20),

—CF 2 O—(CF 2 CF 2 O) m —CF 2 —  (6)

(in Formula (6), m indicates the average degree of polymerization and represents 0.1 to 20),

—CF 2 CF 2 O—(CF 2 CF 2 CF 2 O) n —CF 2 CF 2 —  (7)

(in Formula (7), n indicates the average degree of polymerization and represents 0.1 to 20,

—CF 2 CF 2 CF 2 O—(CF 2 CF 2 CF 2 CF 2 O),—CF 2 CF 2 CF 2 —  (8)

(in Formula (8), o indicates the average degree of polymerization and represents 0.1 to 10, and

—CF(CF 3 )O—(CF 2 CF(CF 3 )O) p —CF(CF 3 )—  (9)

(in Formula (9), p indicates the average degree of polymerization and represents 0.1 to 20).

6 . The fluorine-containing ether compound according to claim 1 ,

wherein R 1 and R 7 in Formula (1) above are the same as each other.

7 . The fluorine-containing ether compound according to claim 1 ,

wherein R 2 and R 6 in Formula (1) above are the same as each other.

8 . The fluorine-containing ether compound according to claim 1 ,

wherein a number average molecular weight thereof is within a range of 500 to 10,000.

9 . A lubricant for a magnetic recording medium comprising:

the fluorine-containing ether compound according to claim 1 .

10 . A magnetic recording medium,

wherein at least a magnetic layer, a protective layer, and a lubricating layer are sequentially provided on a substrate, and

wherein the lubricating layer contains the fluorine-containing ether compound according to claim 1 .

11 . The magnetic recording medium according to claim 10 ,

wherein an average film thickness of the lubricating layer is 0.5 nm to 2.0 nm.

12 . The fluorine-containing ether compound according to claim 1 , wherein R 1 and R 7 are different from each other.

13 . The fluorine-containing ether compound according to claim 1 , wherein R 2 and R 6 are different from each other.

Assignments (2)
CHANGE OF ADDRESS Recorded Feb 9, 2024
From: RESONAC CORPORATION
To: RESONAC CORPORATION
Reel/Frame 066547/0677 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Oct 4, 2023
From: SHIBATA, NATSUMI; FUKUMOTO, NAOYA; ASANO, AYANO; KATO, TSUYOSHI; KURODA, TAKUMA; YAGYU, DAISUKE; KASAHARA, CHIZURU; TANJI, YUTAKA
To: RESONAC CORPORATION
Reel/Frame 065119/0342 →
Priority Claims (1)
JP 2021-065869 · Apr 8, 2021 · national
Continuity (1)
Related Publication 20240203453A1 · Jun 20, 2024
References Cited (30)
US 8518564B2 · Burns et al. · 2013 [cited by applicant]
US 11261394B2 · Kato · 2022 [cited by examiner]
US 11332686B2 · Fukumoto · 2022 [cited by examiner]
US 12264290B2 · Shibata · 2025 [cited by examiner]
US 20150235664A1 · Deng et al. · 2015 [cited by applicant]
US 20160260452A1 · Pathem · 2016 [cited by applicant]
US 20170260472A1 · Sagata et al. · 2017 [cited by applicant]
US 20200002640A1 · Lu et al. · 2020 [cited by applicant]
US 20230242829A1 · Shibata · 2023 [cited by examiner]
US 20240043612A1 · Asano · 2024 [cited by examiner]
US 20240101759A1 · Yagyu · 2024 [cited by examiner]
US 20240279395A1 · Shibata · 2024 [cited by examiner]
US 20240331726A1 · Kasahara · 2024 [cited by examiner]
US 20250129208A1 · Tanji · 2025 [cited by examiner]
JP 2010248463A · 2010 [cited by applicant]
JP 4632144B2 · 2011 [cited by applicant]
JP 20127008A · 2012 [cited by applicant]
JP 2012184339A · 2012 [cited by applicant]
WO 2013054393A1 · 2013 [cited by applicant]
WO 2015022871A1 · 2015 [cited by applicant]
WO 2016084781A1 · 2016 [cited by applicant]
WO 2017145995A1 · 2017 [cited by applicant]
WO WO2018116742A1 · 2018 [cited by examiner]
WO WO2019054148A1 · 2019 [cited by examiner]
WO 2021020066A1 · 2021 [cited by applicant]
WO 2021020076A1 · 2021 [cited by applicant]
Guo et al., “A multidentate lubricant for use in hard disk drives at sub-nanometer thickness”, Journal of Applied Physics, 2012, vol. 111, 024503-1 to 024503-7 (7 pages). [cited by applicant]
United States Office Action dated Aug. 23, 2021 in U.S. Appl. No. 16/470,713. [cited by applicant]
Notice of Allowance dated Jan. 28, 2022 in U.S. Appl. No. 16/470,713. [cited by applicant]
International Search Report dated Feb. 27, 2018 in Application No. PCT/JP2017/042189. [cited by applicant]