IP Library Granted Patent US 12,473,410
Granted Patent B2
US 12,473,410 · App. 18/311,650 · Granted Nov 18, 2025

Depolymerized lignosulfonate and lignin as extender for phenolic resin

Inventor: Mahesh Subramanian (Centerville, OH)
Assignee: WILSONART LLC
C08J5/246B32B29/005C08J5/245C08J5/248B32B2250/26B32B2250/40B32B2260/028B32B2260/046C08J2300/00C08J2497/00
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Quick Facts
Patent No.
US 12,473,410
App. No.
18/311,650
Granted
Nov 18, 2025
Kind
B2
Abstract

A resin composition for impregnating paper products used in manufacture of high-pressure decorative laminates includes a resin and lignin derivatives.

Claims (19)

1 . A high-pressure decorative laminate, comprising:

a decorative layer; and

a core layer composed of at least one resin impregnated sheet of core paper, which is impregnated with a resin composition, the resin composition comprising a resin and lignin derivatives;

wherein the resin composition is prepared according to a method comprising:

mixing and cooking ammonium lignosulfonate, acetic acid, and methanol;

adding KOH or MgO and epicholorohydrin;

cooking the mixture;

mixing and cooking, with the mixture produced above, water, dioctyl sulfosuccinate sodium salt, resin, KOH, glyoxal, and methanol; and

adjusting to desired pH and viscosity.

2 . The high-pressure decorative laminate according to claim 1 , wherein the lignin derivatives are lignosulfonate and kraft lignin.

3 . The high-pressure decorative laminate according to claim 2 , wherein the lignosulfonate is ammonium lignosulfonates.

4 . The high-pressure decorative laminate according to claim 1 , wherein the decorative layer and the resin impregnated core sheet are layered to form a laminate lay-up and the laminate lay-up is heated and pressed to consolidate and cure the high-pressure laminate.

5 . The high-pressure decorative laminate according to claim 4 , further including an overlay paper layer.

6 . The high-pressure decorative laminate according to claim 1 , wherein the core layer includes two sheets of 160 to 550 grams/meter 2 resin impregnated Kraft paper.

7 . The high-pressure decorative laminate according to claim 6 , wherein the Kraft paper is impregnated with the resin composition and is partially cured.

8 . The high-pressure decorative laminate according to claim 7 , wherein the Kraft paper is impregnated with a resin content of approximately 28% to 37%.

9 . The high-pressure decorative laminate according to claim 1 , wherein the core layer includes an impregnation enhancing surfactant composition including an anionic surfactant and a non-ionic surfactant.

10 . The high-pressure decorative laminate according to claim 1 , wherein the core paper includes no more than 50% recycled materials.

11 . The high-pressure decorative laminate according to claim 10 , wherein the core paper includes an impregnation enhancing surfactant composition including an anionic surfactant and a non-ionic surfactant.

Assignments (2)
NOTICE AND CONFIRMATION OF GRANT OF SECURITY INTEREST IN PATENTS Recorded Aug 5, 2024
From: WILSONART LLC
To: DEUTSCHE BANK AG NEW YORK BRANCH
Reel/Frame 068550/0979 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jun 29, 2023
From: SUBRAMANIAN, MAHESH
To: WILSONART LLC
Reel/Frame 064112/0744 →
Continuity (2)
Provisional Application 63364088 · May 3, 2022
Related Publication 20230357518A1 · Nov 9, 2023
References Cited (4)
US 4402780A · Ogoe · 1983 [cited by examiner]
US 20210009618A1 · Jobber · 2021 [cited by examiner]
“Characterization of a Novolac Resin Substituting Phenol by Ammonium Lignosulfonate as Filler or Extender,” Perez et al., BioResources 2 (2) p. 270-283, 2007 (Year: 2007). [cited by examiner]
Perez et al (Year: 2007). [cited by examiner]