IP Library Granted Patent US 12,398,347
Granted Patent B2
US 12,398,347 · App. 18/318,532 · Granted Aug 26, 2025

Parts-washing method

Inventor: Tom Sands (Maidenhead, GB)
Assignee: Terrafend Limited
C11D17/0008B08B3/003B08B3/02B08B3/08B08B3/102B08B3/12B08B3/14C11D1/72C11D1/825C11D1/83C11D2111/16C11D2111/46C11D2111/48
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Quick Facts
Patent No.
US 12,398,347
App. No.
18/318,532
Granted
Aug 26, 2025
Kind
B2
Abstract

A parts-washing method is described. The method comprises: (a) contacting a part with an aqueous liquid cleaning composition in a contact zone at a temperature of less than 45 degrees C., wherein the aqueous liquid cleaning composition comprises at least one alkoxylate surfactant; (b) passing at least part of the aqueous liquid cleaning composition from the contact zone to a separation housing; (c) separating the aqueous liquid cleaning composition in the separation housing to form an upper oily phase, an intermediate aqueous phase and a lower particulate phase; and (d) withdrawing at least a portion of the intermediate aqueous phase for use as the aqueous liquid cleaning composition in the contact zone.

Claims (24)

1. A parts-washing method comprising:

a) contacting a part with an aqueous liquid cleaning composition in a contact zone at a temperature of less than 45 degrees C., wherein the aqueous liquid cleaning composition comprises at least one alkoxylate surfactant and is not heated prior to contact with the part in the contact zone, wherein the at least one alkoxylate surfactant comprises an ethoxylated non-ionic surfactant prepared by a reaction of an ethylene oxide with a monohydroxy alkanol or an alkylphenol, wherein the monohydroxy alkanol or the alkylphenol each having 2 to 20 carbon atoms, and wherein a total amount of the at least one alkoxylate surfactant in the aqueous liquid cleaning composition is 1 weight % to 20 weight % based on a total weight of the aqueous liquid cleaning composition;

b) passing at least part of the aqueous liquid cleaning composition from the contact zone to a separation housing;

c) separating the aqueous liquid cleaning composition by allowing it to settle only under gravity in the separation housing to form a separated aqueous liquid cleaning composition having an upper oily phase, an intermediate aqueous phase and a lower particulate phase; and

d) withdrawing at least a portion of the intermediate aqueous phase from the separated aqueous liquid cleaning composition in the separation housing, wherein the at least a portion of the intermediate aqueous phase is for use as the aqueous liquid cleaning composition in the contact zone.

2. A parts-washing method as claimed in claim 1 , wherein the separation housing comprises a base portion and an outlet, said base portion being configured to facilitate withdrawal of the lower particulate phase through the outlet.

3. A parts-washing method as claimed in claim 1 , which further comprises withdrawing the lower particulate phase for disposal.

4. A parts-washing method as claimed in claim 1 , wherein the portion of the intermediate aqueous phase is filtered prior to use as the aqueous liquid cleaning composition in the contact zone.

5. A parts-washing method as claimed in claim 1 , wherein the separation housing comprises a further outlet positioned to allow withdrawal of the intermediate aqueous phase for use as the aqueous liquid cleaning composition in the contact zone.

6. A parts-washing method as claimed in claim 1 , wherein the aqueous liquid cleaning composition is delivered onto the part using a nozzle.

7. A parts-washing method as claimed in claim 1 , wherein the contact zone comprises a soaking bath.

8. A parts-washing method as claimed in claim 1 , wherein the aqueous liquid cleaning composition comprises at least two ethoxylated surfactants.

9. A parts-washing method as claimed in claim 1 , wherein the part is contacted with the aqueous liquid cleaning composition in the contact zone at a temperature of 10 to 35 degrees C., and the aqueous liquid cleaning composition additionally comprises an anionic surfactant.

10. A parts-washing method as claimed in claim 1 , wherein the part is contacted with the aqueous liquid cleaning composition in the contact zone at a temperature of 10 to 35 degrees C.

11. A parts-washing method as claimed in claim 1 , wherein the separation step is carried out at a temperature of 10 to 35 degrees C.

12. A parts-washing method as claimed in claim 1 , wherein the part comprises a metal part.

13. A parts-washing method as claimed in claim 1 , wherein steps a) to d) are repeated for a plurality of cycles.

14. A parts-washing method as claimed in claim 1 , wherein the separation step is carried out at a temperature of 10 to 30 degrees C.

15. A parts-washing method as claimed in claim 1 , wherein the contacting a part with an aqueous liquid cleaning composition and the separating the aqueous liquid cleaning composition occur at temperatures within 5 degrees C. of one another.

16. A parts-washing method as claimed in claim 5 , wherein a filter is positioned in or adjacent the further outlet.

17. A parts-washing method as claimed in claim 6 , wherein the aqueous liquid composition is delivered as a foam.

18. A parts-washing method as claimed in claim 7 , wherein the part and aqueous liquid cleaning composition are introduced into the soaking bath and ultrasonic waves are propagated through the aqueous liquid cleaning composition in the soaking bath.

19. A parts-washing method as claimed in claim 7 , wherein the part and aqueous liquid cleaning composition are introduced into the soaking bath and the aqueous liquid composition is mechanically agitated.

20. A parts-washing method as claimed in claim 13 , wherein, once steps a) to d) are repeated for a plurality of cycles, the separation housing is emptied and re-filled with a fresh source of the aqueous liquid cleaning composition before steps a) to d) repeated for a further plurality of cycles.

Assignments (2)
CHANGE OF NAME Recorded Aug 8, 2023
From: SAFE SOLVENTS EUROPE LIMITED
To: TERRAFEND LTD.
Reel/Frame 064523/0342 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jul 21, 2023
From: SANDS, TOM
To: SAFE SOLVENTS EUROPE LIMITED
Reel/Frame 064339/0017 →
Priority Claims (1)
GB 1720206 · Dec 5, 2017 · national
Continuity (2)
Continuation 16769221
Related Publication 20230374422A1 · Nov 23, 2023
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