IP Library Granted Patent US 12,036,535
Granted Patent B2
US 12,036,535 · App. 18/320,931 · Granted Jul 16, 2024

Perovskite material for methane to ethylene conversion

Inventors: Kannan Ramaiyan (Albuquerque, NM); Angelica Benavidez (Albuquerque, NM); Fernando Garzon (Albuquerque, NM); Luke Denoyer (Albuquerque, NM)
Assignee: UNM Rainforest Innovations
B01J23/8474B01J23/002B01J23/20C01G33/006C07C2/84C01P2002/34C01P2002/52C01P2002/72C01P2002/85C01P2002/88C01P2004/03C07C2529/076
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Quick Facts
Patent No.
US 12,036,535
App. No.
18/320,931
Granted
Jul 16, 2024
Kind
B2
Abstract

A catalyst comprising a barium niobate-based cubic perovskite structure where, Mg and Ca has been used to dope the niobium sites along with Fe, Ni, Co, Y, and Pr.

Claims (22)

1. A catalyst comprising: a barium niobate-based cubic perovskite structure where, Mg and Ca has been used to dope the niobium sites along with Fe, Ni, Co, Y, and Pr.

2. The catalyst of claim 1 wherein said barium niobate-based cubic perovskite structure has the chemical formula of BaCa 0.33 Nb 0.67-x M x O 3-δ and BaMg 0.33 Nb 0.67-x M x O 3-δ where M is one or more of Fe, Co, Ni, Y, or Pr and the M content is varied from x=0 to x=33.

3. The catalyst of claim 1 wherein said barium niobate-based cubic perovskite structure has the chemical formula of BaCa 0.33 Nb 0.67-x Fe x O 3-δ and BaMg 0.33 Nb 0.67-x Fe x O 3-δ .

4. The catalyst of claim 3 wherein the Fe content is varied from x=0 to x=33.

5. The catalyst of claim 4 wherein said Mg and said Fe are incorporated on said Nb site resulting in oxide ion vacancy creation.

6. The catalyst of claim 4 wherein said barium sites act as adsorption sites for methane while adjacent lattice oxygen remove two hydrogen atoms as water.

7. The catalyst of claim 3 wherein the Fe content is varied from x=0 to x=60.

8. A catalyst for oxidizing methane comprising: a barium niobate-based cubic perovskite structure where, Mg and Ca has been used to dope the niobium sites along with Fe.

9. The catalyst of claim 8 wherein said barium niobate-based cubic perovskite structure has the chemical formula of BaCa 0.33 Nb 0.67-x Fe x O 3-δ and BaMg 0.33 Nb 0.67-x Fe x O 3-δ .

10. The catalyst of claim 9 wherein the Fe content is varied from x=0 to x=33.

11. The claim of catalyst 9 wherein the Mg and Ca content is varied from 0.20 to 0.40.

12. The catalyst of claim 9 wherein said Ca and said Fe are incorporated on said Nb site resulting in oxide ion vacancy creation.

13. The catalyst of claim 9 wherein said barium sites act as adsorption sites for methane while adjacent lattice oxygen remove two hydrogen atoms as water.

14. The catalyst of claim 9 wherein the Fe content is varied from x=0 to x=60.

15. The catalyst of claim 8 wherein said barium niobate-based cubic perovskite structure has the chemical formula of BaCa 0.33 Nb 0.67-x M x O 3-δ and BaMg 0.33 Nb 0.67-x M x O 3-δ where M is one or more of Fe, Co, Ni, Y, or Pr and the M content is varied from x=0 to x=60.

16. A method for the oxidation of methane comprising: providing a feed comprising said light hydrocarbon mixtures; and

contacting said feed with a catalyst comprising a barium niobate-based cubic perovskite structure where, Mg and Ca has been used to dope the niobium sites along with Fe.

17. The method of claim 16 wherein said barium niobate-based cubic perovskite structure has the chemical formula of BaCa 0.33 Nb 0.67-x Fe x O 3-δ and BaMg 0.33 Nb 0.67-x Fe x O 3-δ .

18. The method of claim 16 wherein the Fe content is varied from x=0 to x=60.

19. The method of claim 17 wherein said Mg and said Fe are incorporated on said Nb site resulting in oxide ion vacancy creation.

20. The method of claim 17 wherein said barium sites act as adsorption sites for methane while adjacent lattice oxygen remove two hydrogen atoms as water.

21. The method according to claim 17 , further comprising maintaining said catalyst at a temperature between about 200° C. and about 1000° C.

Assignments (4)
CONFIRMATORY LICENSE Recorded May 12, 2025
From: UNIVERSITY OF NEW MEXICO
To: NATIONAL SCIENCE FOUNDATION
Reel/Frame 071249/0732 →
CONFIRMATORY LICENSE Recorded May 12, 2025
From: UNIVERSITY OF NEW MEXICO
To: NATIONAL SCIENCE FOUNDATION
Reel/Frame 071249/0736 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Feb 29, 2024
From: BENAVIDEZ, ANGELICA; GARZON, FERNANDO; RAMAIYAN, KANNAN; DENOYER, LUKE
To: THE REGENTS OF THE UNIVERSITY OF NEW MEXICO
Reel/Frame 066608/0183 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Feb 29, 2024
From: THE REGENTS OF THE UNIVERSITY OF NEW MEXICO
To: UNM RAINFOREST INNOVATIONS
Reel/Frame 066608/0231 →
Continuity (2)
Provisional Application 63343887 · May 19, 2022
Related Publication 20230372911A1 · Nov 23, 2023