IP Library Granted Patent US 12,467,157
Granted Patent B2
US 12,467,157 · App. 18/323,847 · Granted Nov 11, 2025

Enclosed crystal growth

Inventors: David J. Weeden (Concord, NH); Brian J. McAndrews (Brookline, NH); Guilford Leroy Mack, III (Manchester, NH); Ralph L. Maclean, Jr. (Manchester, NH)
Assignee: LUXIUM SOLUTIONS, LLC
C30B9/04C30B29/60
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Quick Facts
Patent No.
US 12,467,157
App. No.
18/323,847
Granted
Nov 11, 2025
Kind
B2
Abstract

Various single crystals are disclosed including sapphire as well as methods of forming the same. A method of forming a crystalline structure is disclosed as well. The method can include providing a melt in a crucible having a die. The die can include a ventilation opening. The method can further include growing the crystalline structure from the die using an enclosed seed. The single crystals can have desirable geometric properties, including a length greater than a diameter greater than a thickness.

Claims (15)

1 . A method of forming an enclosed crystalline structure, the method comprising:

providing a melt in a crucible having a die, wherein the die comprises a ventilation opening; and

growing the crystalline structure from the die using a seed to form an enclosed crystalline structure.

2 . The method of claim 1 , wherein the ventilation opening goes through the body of the die from one end to another end along a diameter of the die.

3 . The method of claim 2 , wherein the ventilation opening comprises a vertical portion and a horizontal portion.

4 . The method of claim 3 , wherein the horizontal structure goes through the body of the die from one end to another end and the vertical structure intersects the horizontal structure.

5 . The method of claim 4 , wherein the vertical structure has an end that connects to an opening of the die.

6 . The method of claim 1 , wherein the crystalline structure is hollow.

7 . The method of claim 1 , wherein the crystalline structure is a single crystalline structure.

8 . The method of claim 1 , wherein the body is not machined.

9 . The method of claim 1 , wherein the crystalline structure comprises sapphire.

10 . A method of forming an enclosed crystalline structure, the method comprising:

providing a melt in a crucible having a die, wherein the die comprises a ventilation opening;

contacting a crystalline seed to the melt; and

growing a body of the crystalline structure from the die using the crystalline seed, wherein the crystalline seed becomes a cover for the enclosed crystalline structure.

Assignments (2)
INTELLECTUAL PROPERTY SECURITY AGREEMENT SUPPLEMENT Recorded May 8, 2026
From: LUXIUM SOLUTIONS, LLC
To: GOLUB CAPITAL MARKETS LLC, AS COLLATERAL AGENT
Reel/Frame 075574/0443 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Dec 5, 2023
From: WEEDEN, DAVID J.; MCANDREWS, BRIAN J.; MACK, GUILFORD LEROY, III; MACLEAN, RALPH L., JR.
To: LUXIUM SOLUTIONS, LLC
Reel/Frame 065759/0928 →
Continuity (2)
Provisional Application 63365321 · May 25, 2022
Related Publication 20230383432A1 · Nov 30, 2023
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