IP Library Granted Patent US 12,064,747
Granted Patent B2
US 12,064,747 · App. 18/328,634 · Granted Aug 20, 2024

Carbon-based compositions with highly efficient volumetric gas sorption

Inventors: Henry R. Costantino (Woodinville, WA); Alan Tzu-Yang Chang (Renton, WA); Chad Goodwin (Seattle, WA); Cory Mekelburg (Hagerstown, MD); Liam Cover (Seattle, WA); Benjamin E. Kron (Seattle, WA); Katharine Geramita (Seattle, WA); Aaron M. Feaver (Seattle, WA); Leah A. Thompkins (Seattle, WA)
Assignee: Group14 Technologies, Inc.
B01J20/20B01J20/28004B01J20/28011B01J20/28016B01J20/28066B01J20/28073C01B3/0021C01B3/0084C01B32/30C10L3/06C10L3/10C01P2006/12C01P2006/14Y02E60/32
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Quick Facts
Patent No.
US 12,064,747
App. No.
18/328,634
Granted
Aug 20, 2024
Kind
B2
Abstract

The present application is generally directed to gas storage materials such as activated carbon comprising enhanced gas adsorption properties. The gas storage materials find utility in any number of gas storage applications. Methods for making the gas storage materials are also disclosed.

Claims (40)

1. A carbon material having:

a tap density of 0.5 g/cm 3 or greater;

a surface area of 1000 m 2 /g or greater;

a total pore volume of 0.5 cm 3 /g or greater; and

a gravimetric methane adsorption of 0.10 g/g or greater at room temperature and 50 bar pressure.

2. The carbon material of claim 1 , wherein the surface area is 1200 m 2 /g or greater.

3. The carbon material of claim 1 , wherein the surface area is 1500 m 2 /g or greater.

4. The carbon material of claim 1 , wherein the total pore volume is 0.7 cm 3 /g or greater.

5. The carbon material of claim 1 , wherein the gravimetric methane adsorption is 0.11 g/g or greater at room temperature and 50 bar pressure.

6. The carbon material of claim 1 , wherein the gravimetric methane adsorption is 0.12 g/g or greater at room temperature and 50 bar pressure.

7. The carbon material of claim 1 , wherein the gravimetric methane adsorption is 0.15 g/g or greater at room temperature and 50 bar pressure.

8. The carbon material of claim 1 , wherein the gravimetric methane adsorption is 0.17 g/g or greater at room temperature and 50 bar pressure.

9. The carbon material of claim 1 , wherein the carbon material comprises a mixture of two or more populations of particles, wherein from 5%-30% of the particles have a surface area below 1500 m 2 /g, from 10%-80% of the particles have a surface area of from 1500 m 2 /g to 1800 m 2 /g and from 5-30% of the particles have a surface area greater than 1800 m 2 /g.

10. The carbon material of claim 1 , wherein the carbon material comprises a mixture of two or more populations of particles, wherein from 20-80% of the particles have a surface area of 1600 m 2 /g or lower and from 20-80% of particles have a surface area of 2000 m 2 /g or higher.

11. The carbon material of claim 1 , wherein the carbon material comprises a pore volume and from 1-40% of the pore volume resides in mesopores, and from 1-50% of the pore volume resides in macropores.

12. The carbon material of claim 1 , wherein the volume average particle size Dv,50 of the carbon material is between 0.1 um and 50 mm.

13. A gas storage device comprising the carbon material of claim 1 .

14. The device of claim 13 , wherein the gas storage capacity retention of the device at 1000 cycles is 80% or greater.

15. The carbon material of claim 1 , further comprising nitrogen, silicon, sulfur or combinations thereof.

16. The carbon material of claim 15 , comprising the silicon.

17. A carbon material having a gravimetric methane adsorption of 0.10 g/g or greater at room temperature and 50 bar pressure, wherein the carbon material comprises a mixture of two or more populations of particles, wherein from 5%-30% of the particles have a surface area below 1500 m 2 /g, from 10%-80% of the particles have a surface area of from 1500 m 2 /g to 1800 m 2 /g and from 5-30% of the particles have a surface area greater than 1800 m 2 /g.

18. The carbon material of claim 17 , wherein the gravimetric methane adsorption is 0.11 g/g or greater at room temperature and 50 bar pressure.

19. The carbon material of claim 17 , wherein the gravimetric methane adsorption is 0.12 g/g or greater at room temperature and 50 bar pressure.

20. The carbon material of claim 17 , wherein the tap density is 0.6 g/cm 3 or greater, the surface area is 1200 m 2 /g or greater and the total pore volume is 0.7 cm 3 /g or greater.

21. The carbon material of claim 17 , wherein the carbon material comprises a pore volume and from 1-40% of the pore volume resides in mesopores, and from 1-50% of the pore volume resides in macropores.

22. The carbon material of claim 17 , wherein the volume average particle size Dv,50 of the carbon material is between 0.1 μm and 50 mm.

23. The carbon material of claim 17 , further comprising nitrogen, silicon, sulfur or combinations thereof.

24. The carbon material of claim 23 , comprising the silicon.

25. A gas storage device comprising the carbon material of claim 17 .

26. The device of claim 25 , wherein a gas storage capacity retention of the device at 1000 cycles is 80% or greater.

27. A carbon material having a gravimetric methane adsorption of 0.10 g/g or greater at room temperature and 50 bar pressure, wherein the carbon material comprises a mixture of two or more populations of particles, wherein from 20-80% of the particles have a surface area of 1600 m 2 /g or lower and from 20-80% of particles have a surface area of 2000 m 2 /g or higher.

28. The carbon material of claim 27 , wherein the gravimetric methane adsorption is 0.11 g/g or greater at room temperature and 50 bar pressure.

29. The carbon material of claim 27 , wherein the specific gravimetric methane adsorption is 0.12 g/g or greater at room temperature and 50 bar pressure.

30. The carbon material of claim 27 , wherein the tap density is 0.6 g/cm 3 or greater, the surface area is 1200 m 2 /g or greater and the total pore volume is 0.7 cm 3 /g or greater.

31. The carbon material of claim 27 , wherein the carbon material comprises a pore volume and from 1-40% of the pore volume resides in mesopores, and from 1-50% of the pore volume resides in macropores.

32. The carbon material of claim 27 , wherein the volume average particle size Dv,50 of the carbon material is between 0.1 μm and 50 mm.

33. The carbon material of claim 27 , further comprising nitrogen, silicon, sulfur or combinations thereof.

34. The carbon material of claim 33 , comprising the silicon.

35. A gas storage device comprising the carbon material of claim 27 .

36. The device of claim 35 , wherein the gas storage capacity retention of the device at 1000 cycles is 80% or greater.

Continuity (5)
Continuation 17023019 · Sep 16, 2020
Continuation 16219678 · Dec 13, 2018
Division 14533956 · Nov 5, 2014
Provisional Application 61900310 · Nov 5, 2013
Related Publication 20230321629A1 · Oct 12, 2023