IP Library Granted Patent US 12,636,607
Granted Patent B2
US 12,636,607 · App. 18/543,951 · Granted May 26, 2026

Processes and apparatuses for reducing molecular weight fluctuation in a tail gas stream from a pressure swing adsorption process

Inventors: Anh Ngo (Carol Stream, IL); Shubhra J. Bhadra (Naperville, IL); Garrett Lukin (Seatlle, WA); William Cady (Chicago, IL); Nasser Khazeni (Arlington Heights, IL)
Assignee: UOP LLC
B01D53/047B01D2253/102B01D2253/104B01D2253/106B01D2256/16B01D2257/702B01D2259/40007B01D2259/40013B01D2259/4003B01D2259/40043B01D2259/40064B01D2259/40079B01D2259/40081B01D2259/404
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Quick Facts
Patent No.
US 12,636,607
App. No.
18/543,951
Granted
May 26, 2026
Kind
B2
Abstract

Processes and apparatuses for reducing molecular weight fluctuation in a tail gas stream from a pressure swing adsorption process. Multiple PSA separation zone are synchronized such that when one of the PSA units is generating a low molecular weight tail gas, there is another PSA unit generating a high molecular weight tail gas.

Claims (33)

1 . A method for reducing molecular weight fluctuation in a tail gas stream from a pressure swing adsorption process, the method comprising:

providing a first PSA separation zone comprising a plurality of vessels each containing an adsorbent configured to adsorb a species from a multi-component feed and provide a product stream, and a first tail gas stream by cycling through a first plurality of steps, wherein a molecular weight of the first tail gas stream fluctuates between a relatively high molecular weight and a relatively low molecular weight;

providing a second PSA separation zone a second plurality of vessels each containing an adsorbent configured to adsorb a species from a multi-component feed and provide a product stream, and a second tail gas stream by cycling through a second plurality of steps, wherein a molecular weight of the second tail gas stream fluctuates between a relatively high molecular weight and a relatively low molecular weight;

synchronizing the first plurality of steps with the second plurality of steps so that when the first tail gas stream has the high molecular weight, the second tail gas stream has the low molecular weight.

2 . The method of claim 1 , wherein the first plurality of steps are synchronized with the second plurality of steps so that when the first tail gas stream has the low molecular weight, the second tail gas stream has the high molecular weight.

3 . The method of claim 1 , wherein the synchronizing comprises: a controller for the first PSA separation zone sending a signal to a controller for a second PSA separation zone.

4 . The method of claim 3 , wherein the signal relates to a current step of the first PSA separation zone.

5 . The method of claim 3 , wherein the signal relates to a future step of the first PSA separation zone.

6 . The method of claim 3 , wherein the signal comprises an instruction for the second PSA separation zone to start a vessel on a specific step.

7 . The method of claim 1 , wherein the first and second plurality of steps both comprise: an adsorption step, a co-current depressurization step, a counter-current depressurization step, a purge step, and a repressurization step.

8 . The method of claim 1 , further comprising:

combining the first tail gas stream and the second tail gas stream to provide a net tail gas stream.

9 . The method of claim 8 , further comprising:

compressing the net tail gas stream in a compression zone.

10 . The method of claim 9 , wherein the compression zone has at least one compressor.

11 . A method for reducing molecular weight fluctuation in a tail gas stream from a pressure swing adsorption process, the method comprising:

operating a plurality of PSA separation zones to adsorb a species from a multi-component feed, wherein each PSA separation zone comprises a plurality of vessels each containing an adsorbent configured by cycling through a plurality of steps, wherein each PSA separation zone provides a product stream and a tail gas stream, and wherein a molecular weight of each tail gas stream fluctuates between a relatively high molecular weight and a relatively low molecular weight;

combining the tail gas streams from each PSA separation zone to form a net tail gas stream; and

controlling each PSA separation zone such that when a tail gas stream from a first PSA separation zone has the high molecular weight, a tail gas stream from a second PSA separation zone has the low molecular weight.

12 . The method of claim 11 , wherein the controlling comprises: a controller for the first PSA separation zone sending a signal to a controller for the second PSA separation zone.

13 . The method of claim 12 , wherein the signal relates to a current step of the first PSA separation zone.

14 . The method of claim 12 , wherein the signal relates to a future step of the first PSA separation zone.

15 . The method of claim 12 , wherein the signal comprises an instruction for the second PSA separation zone to start a vessel on a specific step.

16 . The method of claim 11 , wherein the plurality of steps comprise: an adsorption step, a co-current depressurization step, a counter-current depressurization step, a purge step, and a repressurization step.

17 . The method of claim 11 , further comprising:

compressing the net tail gas stream in a compression zone.

18 . The method of claim 17 , wherein the compression zone has at least one compressor.

19 . A method for reducing molecular weight fluctuation in a tail gas stream from a pressure swing adsorption process, the method comprising:

operating a plurality of PSA separation zones to adsorb a species from a multi-component feed, wherein each PSA separation zone comprises a plurality of vessels each containing an adsorbent configured by cycling through a plurality of steps, wherein each PSA separation zone provides a product stream and a tail gas stream, and wherein a molecular weight of each tail gas stream fluctuates between a relatively high molecular weight and a relatively low molecular weight, and wherein the plurality of steps comprise: an adsorption step, a co-current depressurization step, a counter-current depressurization step, a purge step, and a repressurization step;

combining the tail gas streams from each PSA separation zone to form a net tail gas stream; and

controlling each PSA separation zone such that when a tail gas stream from a first PSA separation zone has the high molecular weight, a tail gas stream from a second PSA separation zone has the low molecular weight, and when the tail gas stream from the first PSA separation zone has the low molecular weight, the tail gas stream from the second PSA separation zone has the high molecular weight.

20 . The method of claim 19 , further comprising:

compressing the net tail gas stream in a compression zone, wherein the compression zone has at least one compressor.

Assignments (1)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded May 10, 2024
From: NGO, ANH; BHADRA, SHUBHRA J.; LUKIN, GARRETT; CADY, WILLIAM; KHAZENI, NASSER
To: UOP LLC
Reel/Frame 067369/0756 →
Continuity (1)
Related Publication 20250196053A1 · Jun 19, 2025
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