IP Library › Granted Patent US 12,636,270
Granted Patent B2
US 12,636,270 · App. 18/545,880 · Granted May 26, 2026

Levothyroxine liquid formulations

Inventors: Arunya Usayapant (Mundelein, IL); Basma M. Ibrahim (Lincolnshire, IL)
Assignee: Fresenius Kabi USA, LLC
A61K31/198A61K9/0019A61K9/08A61K33/18A61K47/02A61K47/18
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Quick Facts
Patent No.
US 12,636,270
App. No.
18/545,880
Granted
May 26, 2026
Kind
B2
Abstract

The present invention is directed to a pharmaceutical product which includes a liquid formulation comprising levothyroxine or a pharmaceutically acceptable salt thereof. The formulation of the present invention includes a cyclodextrin, water, and an amine, and has a pH above the buffering range of the amine. The liquid formulation of the invention is stable and ready-to-use.

Claims (39)

1 . A pharmaceutical product comprising a liquid formulation comprising about 5 mcg/mL to about 100 mcg/mL of levothyroxine sodium, a stabilizing agent comprising an alkanolamine and a salt of iodine, and water, wherein the formulation has a pH of from about 9.0 to about 11.5 and retains about least about 95% of the initial concentration of levothyroxine or pharmaceutically acceptable salt thereof after storage for two months at 40° C. and is stable for at least 12 months at room temperature.

2 . The pharmaceutical product of claim 1 , wherein the formulation is provided in a clear glass container selected from the group consisting of a flint colored molded vial, a flint colored tubing vial, an ampoule, a cartridge, and a syringe.

3 . The pharmaceutical product of claim 1 , wherein the clear glass container is not treated with ammonium sulfate.

4 . The pharmaceutical product of claim 1 , wherein the alkanolamine is selected from one or more of tromethamine, bis(2-hydroxyethyl)-imino-tris (hydroxymethyl) methane, monoethanolamine, diethanolamine, triethanolamine, 2-amino-2-methyl-1,3-propanediol, 2-dimethylamino-2-methyl-1-propanediol, 2-amino-2-ethylpropanol, 2-amino-1-butanol, and 2-amino-2-methyl-1-propanol.

5 . The pharmaceutical product of claim 4 , wherein the alkanolamine is tromethamine which is present at a concentration of about 1 mg/mL to about 50 mg/mL.

6 . The pharmaceutical product of claim 1 , wherein the salt of iodine is sodium iodide or potassium iodide.

7 . The pharmaceutical product of claim 6 , wherein the salt of iodine is sodium iodide which is present at a concentration of about 10 mcg/mL to about 500 mcg/mL.

8 . The pharmaceutical product of claim 1 , wherein the formulation has a pH of from about 9.8 to about 10.8.

9 . The pharmaceutical product of claim 1 , wherein the formulation contains not more than 2.0% liothyronine (T3).

10 . The pharmaceutical product of claim 1 , wherein the formulation contains not more than 5.0% total impurities.

11 . The pharmaceutical product of claim 1 , wherein the formulation is stable for at least 18 months at room temperature.

12 . The pharmaceutical product of claim 1 , wherein the formulation retains at least about 90% of the initial concentration of levothyroxine or pharmaceutically acceptable salt thereof after storage for at least 12 months at room temperature.

13 . The pharmaceutical product of claim 1 , wherein the formulation retains at least about 90% of the initial concentration of levothyroxine or pharmaceutically acceptable salt thereof after storage for at least 18 months at room temperature.

14 . The pharmaceutical product of claim 1 , wherein the formulation does not contain a buffer.

15 . A method of preparing a pharmaceutical product comprising:

(a) filling purified water into a container,

(b) dissolving a stabilizing agent comprising an alkanolamine and a salt of iodine in the water to form a solution,

(c) adjusting the pH of the solution to 9.0 to 11.5 with sodium hydroxide and/or hydrochloric acid to form a pH adjusted solution,

(d) adding levothyroxine sodium to the pH adjusted solution to form an initial drug solution,

(e) adding purified water to the drug solution to form a final drug solution,

(f) filtering the final drug solution through a 0.22 mm filter to form a filtered final drug solution, and

(g) filling the filtered final drug solution into one or more clear glass containers and sealing the containers, thereby preparing the pharmaceutical product.

16 . The method of claim 15 , wherein nitrogen is bubbled through the solutions of steps (b)-(e).

17 . The method of claim 15 , wherein the containers are filled and sealed under nitrogen.

18 . The method of claim 15 , wherein the pH is adjusted to about 10.3.

19 . A pharmaceutical product comprising a liquid formulation comprising about 5 mcg/mL to about 100 mcg/mL of levothyroxine sodium, glycerol, and water, wherein the formulation has a pH of from about 7.0 to about 9.0.

20 . The pharmaceutical product of claim 19 , wherein the glycerol is present in a concentration of about 100 mg/mL.

21 . The pharmaceutical product of claim 5 , wherein the salt of iodine is sodium iodide or potassium iodide.

22 . The pharmaceutical product of claim 21 , wherein the salt of iodine is sodium iodide which is present at a concentration of about 10 mcg/mL to about 500 mcg/mL.

23 . The pharmaceutical product of claim 22 , wherein the formulation has a pH of from about 9.8 to about 10.8.

24 . The pharmaceutical product of claim 23 , wherein the formulation contains not more than 2.0% liothyronine (T3) and not more than 5.0% total impurities.

25 . The pharmaceutical product of claim 23 , wherein the formulation retains at least about 90% of the initial concentration of levothyroxine or pharmaceutically acceptable salt thereof after storage for at least 18 months at room temperature.

26 . The pharmaceutical product of claim 5 , wherein the tromethamine is present at a concentration of about 10 mg/mL.

27 . The pharmaceutical product of claim 26 , wherein the salt of iodine is sodium iodide or potassium iodide.

28 . The pharmaceutical product of claim 27 , wherein the salt of iodine is sodium iodide which is present at a concentration of about 140 mcg/mL.

29 . The pharmaceutical product of claim 28 , wherein the formulation has a pH of from about 9.8 to about 10.8.

30 . The pharmaceutical product of claim 29 , wherein the formulation contains not more than 2.0% liothyronine (T3) and not more than 5.0% total impurities.

31 . The pharmaceutical product of claim 29 , wherein the formulation retains at least about 90% of the initial concentration of levothyroxine or pharmaceutically acceptable salt thereof after storage for at least 18 months at room temperature.

32 . The pharmaceutical product of claim 30 , wherein the formulation retains at least about 90% of the initial concentration of levothyroxine or pharmaceutically acceptable salt thereof after storage for at least 18 months at room temperature.

Assignments (1)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Dec 20, 2023
From: USAYAPANT, ARUNYA; IBRAHIM, BASMA M.
To: FRESENIUS KABI USA LLC
Reel/Frame 066091/0035 →
Continuity (6)
Continuation 17550253 · Dec 14, 2021
Continuation 17306504 · May 3, 2021
Continuation 16511220 · Jul 15, 2019
Continuation 15700258 · Sep 11, 2017
Continuation 15366864 · Dec 1, 2016
Related Publication 20240382441A1 · Nov 21, 2024
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