IP Library Patent Application 18822354
Patent Application
App. No. 18/822,354

Destruction of PFAS Via an Oxidation Process and Apparatus Suitable for Transportation to Contaminated Sites

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Patent No.
US None
App. No.
18/822,354
Abstract

Per-and polyfluoroalkyl substances (PFAS) are destroyed by oxidation in supercritical conditions. PFAS in water can be concentrated and prepared for destruction in a pretreatment phase. Following annihilation of the PFAS in supercritical conditions to levels below 5 parts per trillion (ppt), the water effluent can be used to recover heat, returned to sub-critical conditions, and then released back into the environment.

Claims (26)

1 - 36 . (canceled)

37 . A method of destroying PFAS, comprising:

passing an aqueous PFAS mixture into a system comprising a SCWO reactor;

reacting the aqueous PFAS mixture under supercritical conditions under continuous operation in the SCWO reactor;

wherein the SCWO reactor comprises metallic walls; and

during the step of reacting, supplying an electron flood from an external source to the system.

38 . The method of claim 37 wherein the external source comprises a controllable electronic board.

39 . The method of claim 37 further comprising reacting the aqueous PFAS mixture in the presence of a eutectic mixture of alkali and/or alkaline earth salts.

40 . The method of claim 37 further comprising reacting the aqueous PFAS mixture with an aqueous oxidant and, subsequently, reacting with an alkali or alkaline earth compound or mixtures thereof.

41 . The method of claim 40 wherein the alkaline earth compound is calcium oxide.

42 . The method of claim 38 wherein the controllable electronic board supplies electrons to increase electron flow without increasing DC voltage.

43 . The method of claim 40 wherein the aqueous oxidant is hydrogen peroxide.

44 . A method of handling effluent from a process of destroying PFAS, comprising:

the effluent comprising the decomposition products of PFAS; and

filtering and/or centrifuging precipitates from the effluent; or

flashing and/or evaporating the effluent; or

spray drying the effluent; or

any combination of these.

45 . The method of claim 44 further comprising subjecting the effluent to reverse osmosis.

46 . The method of claim 44 further comprising passing the effluent through a heat exchanger, wherein heat from the effluent is transferred to an aqueous PFAS mixture entering a SCWO reactor or system.

47 . The method of claim 44 further comprising adding chelating agents to the effluent.

48 . The method of claim 44 further comprising passing the effluent through a sorbent.

49 . A method of destroying PFAS, comprising:

passing an aqueous PFAS mixture through a plurality of electrodes;

forming HF from the aqueous PFAS mixture;

and, subsequently, reacting the HF with an alkali or alkaline earth element.

Assignments (2)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Dec 17, 2024
From: DEJARME, LINDY E.; DASU, KAVITHA; SIRABIAN, RUSSELL R.; BUURMA, CHRISTOPHER F.; ELLIS, JEFFREY; MILLER, MICHAEL M.; GARBARK, DAN; BRYANT, NATHAN; TALLARICO, JOHN; CASCIANO, JOSEPH; WINECKI, SLAWOMIR; HOLLEY, DAVID; JAMES, JOSHUA; BROWN, KEITH; HENDRY, DOUG; ARGUMEDO, DARWIN; FRANK, AARON; SCHEITLIN, CHRISTOPHER GORDON
To: BATTELLE MEMORIAL INSTITUTE
Reel/Frame 069616/0364 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Dec 17, 2024
From: BATTELLE MEMORIAL INSTITUTE
To: REVIVE ENVIRONMENTAL TECHNOLOGY, LLC
Reel/Frame 069616/0506 →