IP Library Granted Patent US 8,157,918
Granted Patent B2
US 8,157,918 · App. 11/526,813 · Granted Apr 17, 2012

Menthol cigarette

Assignee: Philip Morris USA Inc.
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Quick Facts
Patent No.
US 8,157,918
App. No.
11/526,813
Granted
Apr 17, 2012
Kind
B2
Abstract

Cigarettes are provided which contain a filtering system and flavorants encapsulated with polyvinyl acetate, wherein deactivation of a sorbent by the flavorant is reduced through the encapsulation of the flavorant within the polyvinyl acetate. A preferred flavorant is menthol. The encapsulated flavorants are prepared by mixing at least one flavorant with polyvinyl acetate and a solvent, such as ethanol, and forming the encapsulated flavorants. Methods of making cigarettes and smoking the articles are also provided.

Claims (22)

1. A method of making a cigarette including a sorbent in a filter thereof, comprising:

incorporating an encapsulated flavorant comprising a triacetin-free polyvinyl acetate matrix with flavorant bound within the polyvinyl acetate matrix in a component of the cigarette,

wherein the flavorant comprises menthol and wherein the menthol is substantially uniformly distributed throughout the matrix.

2. The method of claim 1 , wherein the sorbent comprises activated carbon, molecular sieves, zeolites, or combinations thereof.

3. The method of claim 1 , wherein the encapsulated flavorant is:

formed by:

(i) mixing alcohol and polyvinyl acetate;

(ii) mixing menthol into the alcohol-polyvinyl acetate mixture in an amount effective to provide at least 10 μg/puff of menthol flavoring tobacco smoke produced during smoking of the cigarette;

(iii) reducing the alcohol content in the menthol-alcohol-polyvinyl acetate mixture or aging the menthol-alcohol-polyvinyl acetate mixture; and

(iv) forming a menthol-polyvinyl acetate fiber, film, monolith, bead, powder or granule from the menthol-alcohol-polyvinyl acetate mixture.

4. The method of claim 1 , wherein the incorporating the encapsulated flavorant in a component of the cigarette comprises injecting a liquid encapsulated flavorant mixture into a tobacco portion of the cigarette, injecting the liquid encapsulated flavorant into a center portion of a tobacco portion of the cigarette, spraying or coating a liquid encapsulated flavorant onto a tobacco filler and forming a tobacco rod for the cigarette from the sprayed or coated tobacco filler, distributing a liquid or solid encapsulated flavorant throughout a tobacco rod of the cigarette, incorporating a solid encapsulated flavorant into a tobacco filler and forming a tobacco rod for the cigarette from the tobacco filler mixed with the encapsulated flavorant, or placing a fiber, monolith, bead, powder or granule encapsulated flavorant in a cavity in a filter portion of the cigarette or in a tobacco filler in the cigarette.

5. A method of flavoring mainstream tobacco smoke, comprising:

retaining a flavorant with a triacetin-free polyvinyl acetate matrix; and

releasing the flavorant from the matrix while generating mainstream tobacco smoke, said releasing step including an application of heat and/or moisture to the matrix, wherein the flavorant is released by heat and/or moisture from the tobacco smoke;

wherein the flavorant comprises menthol and wherein the menthol is substantially uniformly distributed throughout the matrix.

6. The method of claim 5 , wherein the releasing the flavorant from the matrix comprises gradually releasing the menthol into the tobacco smoke.

7. The method of claim 5 , further comprising:

(a) passing the mainstream tobacco smoke through a sorbent, wherein the sorbent reduces benzene, acrolein and/or 1,3-butadiene levels when tobacco smoke is drawn through the cigarette; and/or

(b) passing the mainstream tobacco smoke through a sorbent, wherein the sorbent comprises activated carbon, molecular sieves, zeolites, or combinations thereof.

8. The method of claim 5 , wherein releasing the flavorant from the matrix comprises:

(a) gradually releasing the flavorant using the heat and/or moisture from the smoke drawn through a cigarette; and/or

(b) gradually releasing the flavorant located in (i) cut filler, (ii) on cigarette paper and/or (iii) in a filter of the cigarette.

Assignments (2)
CORRECTIVE ASSIGNMENT TO CORRECT THE SPELLING OF THE ASSIGNEE'S NAME PREVIOUSLY RECORDED ON REEL 019902 FRAME 0908. ASSIGNOR(S) HEREBY CONFIRMS THE ASSIGNMENT. Recorded Jan 22, 2019
From: BECKER, ULRIKE; HOWELL, TONY; XUE, LIXIN; KARLES, GEORGIOS D.; FOURNIER, JAY A.
To: PHILIP MORRIS USA INC.
Reel/Frame 049668/0700 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Sep 28, 2007
From: BECKER, ULRIKE; HOWELL, TONY; XUE, LIXIN; KARLES, GEORGIOS D.; FOURNIER, JAY A
To: PHILLIP MORRIS USA INC.
Reel/Frame 019902/0908 →
Continuity (2)
Provisional Application 60722033 · Sep 30, 2005
Related Publication 20080017206A1 · Jan 24, 2008