IP Library Granted Patent US 8,202,886
Granted Patent B2
US 8,202,886 · App. 12/872,263 · Granted Jun 19, 2012

Small molecule E2F inhibitor

Assignees: H. Lee Moffitt Cancer Center and Research Institute, Inc.; University of South Florida
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Quick Facts
Patent No.
US 8,202,886
App. No.
12/872,263
Granted
Jun 19, 2012
Kind
B2
Abstract

A small molecular inhibitor of E2F (HLM006474) was identified using a computer-based virtual screen and the known crystal structure of the DNA bound E2F4/DP2 heterodimer. Treatment of multiple cell lines resulted in the loss of intracellular E2F4 DNA-binding activity. Overnight exposure to HLM006474 resulted in down regulation of total E2F4 protein as well as several known E2F targets. The effects of treatment on different cell lines included a reduction in cell proliferation and an increase in apoptosis. Apoptosis was induced in a manner distinct from cisplatin and doxorubicin. E2F4-null MEFs (mouse embryo fibroblasts) were less sensitive than wildtype counterparts to the apoptosis-inducing activity of the compound revealing its biological specificity. A375 cells were extremely sensitive to the apoptosis-inducing activity of the compound in two-dimensional culture and HLM006474 was a potent inhibitor of melanocytes proliferation and subsequent invasion in a three-dimensional tissue culture model system.

Claims (14)

1. A method of modulating E2F activity in a cell, comprising contacting the cell with a small molecule inhibitor having the formula:

or a pharmaceutically acceptable salt thereof.

2. The method of claim 1 , wherein the cell is contacted with between about 40 μM and 80 μM of the small molecular inhibitor.

3. A method of treating a proliferative cellular disorder, comprising the step of administering a therapeutically effective amount of a small molecule inhibitor having the formula:

or a pharmaceutically acceptable salt thereof to a subject in need of said treatment, wherein the proliferative cell disorder is characterized by a disruption of the E2F/Rb pathway.

4. The method of claim 3 , wherein proliferative cellular disorder is selected from the group consisting of melanomas, renal cancer, CNS cancer, leukemia, ovarian cancer, breast cancer, colon cancer and non-small cell lung cancer.

5. The method of claim 3 , wherein the small molecular inhibitor is co-administered with at least one compound selected from the group consisting of doxorubicin, VP16 (etoposide), taxol, cisplatin and gemacitabine.

6. The method of claim 3 , wherein between about 40 μM and 80 μM of the small molecular inhibitor is administered to the subject.

7. A method of down-regulating total E2F4 protein in a cell, comprising contacting the cell with a small molecule inhibitor having the formula:

or a pharmaceutically acceptable salt thereof.

8. The method of claim 7 , wherein the cell is contacted with between about 40 μM and 80 μM of the small molecular inhibitor.

9. A method of inducing apoptosis in a cell, comprising contacting the cell with a small molecule inhibitor having the formula:

or a pharmaceutically acceptable salt thereof.

10. The method of claim 9 , wherein the cell is contacted with between about 40 μM and 80 μM of the small molecular inhibitor.

Assignments (3)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Sep 17, 2010
From: CRESS, DOUGLAS W.
To: UNIVERSITY OF SOUTH FLORIDA
Reel/Frame 025004/0686 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Sep 17, 2010
From: MA, YIHONG
To: H. LEE MOFFITT CANCER CENTER AND RESEARCH INSTITUTE, INC.
Reel/Frame 025004/0892 →
CONFIRMATORY LICENSE Recorded Sep 15, 2010
From: H. LEE MOFFITT CANCER CTR & RESEARCH INS
To: NATIONAL INSTITUTES OF HEALTH (NIH), U.S. DEPT. OF HEALTH AND HUMAN SERVICES (DHHS), U.S. GOVERNMENT
Reel/Frame 024987/0615 →
Continuity (3)
Continuation PCTUS2009037510 · Mar 18, 2009
Provisional Application 61037547 · Mar 18, 2008
Related Publication 20110053977A1 · Mar 3, 2011