IP Library Granted Patent US 8,461,374
Granted Patent B2
US 8,461,374 · App. 13/055,607 · Granted Jun 11, 2013

Method for producing hydroxyalkyl (meth)acrylate

Inventors: Masanori Tokuda (Hatsukaichi, JP); Michiyuki Kouno (Otake, JP); Junichi Morioka (Otake, JP)
Assignee: Mitsubishi Rayon Co., Ltd.
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Quick Facts
Patent No.
US 8,461,374
App. No.
13/055,607
Granted
Jun 11, 2013
Kind
B2
Abstract

Disclosed is a method for producing a hydroxyalkyl (meth)acrylate having high production efficiency and placing little burden on a production system. The method for producing a hydroxyalkyl (meth)acrylate comprises a reaction step of reacting (meth)acrylic acid with an alkylene oxide in a reactor while stirring a liquid containing (meth)acrylic acid and the alkylene oxide with a stirrer to obtain a reaction liquid containing a hydroxyalkyl (meth)acrylate, and thereafter a deaeration step of reducing a pressure in the reactor while stirring the reaction liquid with the stirrer to vaporize and remove an unreacted alkylene oxide in the reaction liquid, a number of stirring revolutions of the stirrer in the deaeration step being reduced to 30 to 85% of a number of stirring revolutions of the stirrer in the reaction step.

Claims (2)

1. A method for producing a hydroxyalkyl (meth)acrylate, comprising:

a reaction step of reacting (meth)acrylic acid with an alkylene oxide in a reactor while stirring a liquid containing (meth)acrylic acid and the alkylene oxide with a stirrer to obtain a reaction liquid containing a hydroxyalkyl (meth)acrylate; and thereafter a deaeration step of reducing a pressure in the reactor while stirring the reaction liquid with the stirrer to vaporize and remove an unreacted alkylene oxide in the reaction liquid, a number of stirring revolutions of the stirrer in the deaeration step being reduced to 30 to 85% of a number of stirring revolutions of the stirrer in the reaction step.

Assignments (2)
CHANGE OF NAME Recorded Sep 5, 2017
From: MITSUBISHI RAYON CO., LTD.
To: MITSUBISHI CHEMICAL CORPORATION
Reel/Frame 043750/0834 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Feb 1, 2011
From: TOKUDA, MASANORI; KOUNO, MICHIYUKI; MORIOKA, JUNICHI
To: MITSUBISHI RAYON CO., LTD.
Reel/Frame 025727/0657 →
Priority Claims (1)
JP 2008-219548 · Aug 28, 2008 · national
Continuity (1)
Related Publication 20110124906A1 · May 26, 2011