IP Library Granted Patent US 8,535,467
Granted Patent B2
US 8,535,467 · App. 12/921,467 · Granted Sep 17, 2013

Process for manufacturing an anti-ballistic article

Inventors: Hen H. Hoefnagels (Hulsberg, NL); Albert A. Vunderink (Selfkant-Tüddern, DE)
Assignee: DSM IP Assets B.V.
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Quick Facts
Patent No.
US 8,535,467
App. No.
12/921,467
Granted
Sep 17, 2013
Kind
B2
Abstract

The invention relates to a process for the manufacture of an antiballistic article comprising the steps of forming a stack of sheets by stacking 2 or more sheets, each sheet comprising one or more mono-layers of anti-ballistic fibers and optionally a thermoplastic binder, followed by subjecting the stack of sheets to a reduced atmospheric pressure environment; and while maintaining the reduced atmospheric pressure environment, consolidating said stack of sheets to a pressure of at least 10 MPa at an elevated temperature. The invention also relates to an anti-ballistic article.

Claims (21)

1. A process for the manufacture of an anti-ballistic article comprising the steps of:

(a) forming a stack of sheets by stacking 2 or more sheets, each sheet comprising one or more mono-layers of anti-ballistic fibers, followed by

(b) subjecting the stack of sheets to a reduced atmospheric pressure environment having an absolute gaseous pressure of no more than 0.1 MPa; and

(c) while maintaining the reduced atmospheric pressure environment, consolidating said stack of sheets to a pressure of at least 10 MPa at an elevated temperature of at least 10° C. below either a melting temperature of the anti-ballistic fibers or a temperature at which the anti-ballistic fibers lose mechanical properties.

2. The process according to claim 1 , wherein the sheets are unidirectional sheets and the direction of the anti-ballistic fibers in the sheets is at an angle α to the fiber direction in an adjacent mono-layer.

3. The process according to claim 1 , wherein each sheet further comprises a thermoplastic binder.

4. The process according to claim 3 , wherein the thermoplastic binder content is in the range of at least 5 wt % to at most 30 wt % relative to the total weight of anti-ballistic fibers and the binder in the stack.

5. The process according to claim 1 , wherein the stack of sheets is subjected to a reduced atmospheric pressure environment by placing the stack of unidirectional sheets into a vacuum bag and connecting a vacuum source to said bag.

6. The process according to claim 5 , wherein at least a portion of the vacuum bag forms part of the anti-ballistic article.

7. The process according to claim 1 , wherein each sheet in the stack comprises two or more monolayers of unidirectional anti-ballistic fibers and a thermoplastic binder.

8. The process according to claim 1 , wherein the stack of sheets has an areal density of at least 2 kg/m 2 .

9. The process according to claim 1 , wherein the anti-ballistic fibers have a cross sectional aspect ratio of greater than 5:1.

10. The process according to claim 1 , wherein at least one monolayer comprises a plurality of fibers, aligned such that the fibers form a woven sheet.

11. The process according to claim 1 , wherein step (c) further comprises placing the stack of sheets into a curved mould prior to consolidating the stack into the curved mould, thereby forming a curved anti-ballistic article.

12. The process according to claim 1 , wherein steps (b) and (c) occur co-currently.

13. The process according to claim 5 , wherein the vacuum bag has a melting temperature at or below the elevated temperature according to step (c).

14. The process according to claim 1 , wherein step (b) is practiced at a reduced atmospheric pressure environment having an absolute gaseous pressure of no more than 0.005 MPa.

15. The process according to claim 1 , wherein step (b) is practiced at a reduced atmospheric pressure environment having an absolute gaseous pressure of no more than 0.001 MPa.

16. The process according to claim 1 , wherein step (b) is practiced at a reduced atmospheric pressure environment having an absolute gaseous pressure of no more than 0.0005 MPa.

17. The process according to claim 1 , wherein step (c) is practiced at an elevated temperature of at least 20° C. lower than the melting temperature of the anti-ballistic fibers.

18. The process according to claim 1 , wherein step (c) is practiced at an elevated temperature of at least 25° C. lower than the melting temperature of the anti-ballistic fibers.

Assignments (3)
CHANGE OF NAME Recorded Mar 17, 2023
From: DSM PROTECTIVE MATERIALS B.V.
To: AVIENT PROTECTIVE MATERIALS B.V.
Reel/Frame 063115/0134 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Nov 8, 2022
From: DSM IP ASSETS B.V.
To: DSM PROTECTIVE MATERIALS B.V.
Reel/Frame 061897/0987 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Sep 8, 2010
From: VUNDERINK, ALBERT; HOEFNAGELS, HEN
To: DSM IP ASSETS B.V.
Reel/Frame 024954/0581 →
Priority Claims (1)
EP 08006711 · Apr 2, 2008 · regional
Continuity (1)
Related Publication 20110036235A1 · Feb 17, 2011