IP Library Granted Patent US 8,629,210
Granted Patent B2
US 8,629,210 · App. 13/123,323 · Granted Jan 14, 2014

Zwitterionic/amphiphilic pentablock copolymers and coatings therefrom

Inventors: Dean C. Webster (Fargo, ND); Robert J. Pieper (West Bend, WI); Mohammed J. Nasrullah (Fargo, ND)
Assignee: NDSU Research Foundation
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Quick Facts
Patent No.
US 8,629,210
App. No.
13/123,323
Granted
Jan 14, 2014
Kind
B2
Abstract

A zwitterionic/amphiphilic pentablock copolymer was prepared using atom transfer radical polymerization (ATRP). The pentablock copolymer is prepared for the atom transfer radical polymerization of a PDMS-PEO-Br macroinitiator and SBMA. The pentablock copolymer is incorporated into a polyurethane coating composition which is useful for antifouling and/or fouling release applications.

Claims (13)

1. A pentablock copolymer prepared from atom transfer radical polymerization of a Poly(dimethylsiloxane)-Poly(ethyleneoxide)-Br macroinitiator and [2-(Methacryloyloxy)ethyl]dimethyl-(3-sulfopropyl)ammonium hydroxide).

2. A curable coating composition comprising: the pentablock copolymer according to claim 1 , a polyol and a polyisocyanate.

3. A curable coating composition according to claim 2 , wherein the polyol is selected from the group consisting of: polyester, polyether, polycarbonate, and acrylic.

4. A curable coating composition according to claim 3 , wherein the polyol is an an acrylic polyol.

5. A curable coating composition according to claim 2 , wherein the polyisocyanate is selected from the group consisting of: an aromatic isocyanate; a cycloaliphatic isocyanate; and an aliphatic isocyanate.

6. A curable coating composition according to claim 5 , wherein the polyisocyanate is a triisocyanurate resin prepared from isophorone diisocyanate.

7. A curable coating composition according to claim 2 , wherein the polyol is an acrylic polyol comprising 80% by weight butyl acrylate and 20% by weight of 2-hydroxyethyl acrylate and wherein the polyisocyanate is a triisocyanurate resin prepared from isophorone diisocyanate.

8. A curable coating composition according to claim 2 , wherein the copolymer comprises from about 1 to about 50 percent by weight of the coating composition.

9. A curable coating composition according to claim 8 , wherein the copolymer comprises from about 1 to about 15 percent by weight.

10. A cured coating prepared from the coating composition according to claim 2 , wherein the cured coating is non-fouling.

11. A cured coating according to claim 2 , wherein the cured coating is antifouling.

12. A cured coating according to claim 2 , wherein the cured coating has a hydrophilic surface.

13. An object coated with the curable coating composition according to claim 2 wherein the curable coating composition is subsequently cured.

Assignments (3)
CONFIRMATORY LICENSE Recorded Aug 2, 2017
From: NORTH DAKOTA STATE UNIVERSITY
To: NAVY, SECRETARY OF THE UNITED STATES OF AMERICA
Reel/Frame 043493/0176 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded May 19, 2011
From: WEBSTER, DEAN C.; PIEPER, ROBERT J.; NASRULLAH, MOHAMMED J.
To: NORTH DAKOTA STATE UNIVERSITY
Reel/Frame 026306/0420 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded May 19, 2011
From: NORTH DAKOTA STATE UNIVERSITY
To: NDSU RESEARCH FOUNDATION
Reel/Frame 026306/0531 →
Continuity (2)
Provisional Application 61104343 · Oct 10, 2008
Related Publication 20110218290A1 · Sep 8, 2011