IP Library Granted Patent US 8,733,142
Granted Patent B2
US 8,733,142 · App. 12/834,162 · Granted May 27, 2014

Process for manufacturing stamped products, and stamped products prepared from the same

Inventors: Dominique Spehner (Sedan, FR); Ronald Kefferstein (Saint Mitre les Remparts, FR); Pascal Drillet (Rozerieulles, FR)
Assignee: ArcelorMittal France
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Quick Facts
Patent No.
US 8,733,142
App. No.
12/834,162
Granted
May 27, 2014
Kind
B2
Abstract

The invention relates to a process for making a hot stamped coated steel sheet product, comprising the steps of pre-coating a steel strip or sheet with aluminum—or aluminum alloy, cutting said pre-coated steel strip or sheet to obtain a pre-coated steel blank, heating the blank in a furnace preheated to a temperature and during a time defined by diagram according to thickness, at a heating rate V c between 20 and 700° C. comprised between 4 and 12° C./s and at a heating rate V c ′ between 500 and 700° C. comprised between 1.5 and 6° C./s, to obtain a heated blank; then transferring said heated blank to a die, hot stamping the heated blank in the die obtain a hot stamped steel sheet product, cooling at a mean rate V r between the exit of the heated blank from the furnace, down to 400° C., of at least 30° C./s.

Claims (72)

1. A process for making a hot stamped coated steel sheet product, comprising:

pre-coating a steel strip or sheet with aluminum or aluminum alloy by hot dipping said steel strip or sheet having a first side and a second side in an aluminum or aluminum alloy bath to provide a pre-coating having a thickness t p of from 20 to 33 micrometers;

cutting said pre-coated steel strip or sheet to obtain a pre-coated steel blank; heating said aluminum or aluminum alloy pre-coated steel blank in a furnace;

transferring said heated blank to a die;

hot stamping said heated blank in said die, to thereby obtain a hot stamped steel product, and

cooling said hot stamped steel sheet product at a mean rate Vr during an interval between when said product exits said furnace and when said product reaches 400° C., of at least 30° C./s so as to obtain a hot stamped coated steel sheet product with a coating having a plurality of layers;

the plurality of layers including, from the steel strip or sheet outwards, an interdiffusion layer, an intermediate layer, an intermetallic layer and a superficial layer,

the superficial layer having a hardness HV50 g from 810 to 1100.

2. The process according to claim 1 , wherein an elapsed time between when said heated blank exits said furnace and said stamping commences is not more than 10 seconds.

3. The process according to claim 1 , wherein the heating said aluminum or aluminum alloy pre-coated steel sheet in a furnace includes preheating to a temperature and during a time defined by trapezoid ABCD having heating time, temperature coordinates of about A(3 minutes, 930° C.), B(6 minutes, 930° C.), C(13 minutes, 880° C.), and D(4.5 minutes, 880° C.) if the thickness of said sheet is greater than or equal to 0.7 rnrn and less than or equal to 1.5 mm, and by trapezoid EFGH having heating time, temperature coordinates of about E(4 minutes, 940° C.), F(8 minutes, 940° C.), G(13 minutes, 900° C.), and H(6.5 minutes, 900° C.) if the thickness of said sheet is greater than 1.5 mm and less than or equal to 3 mm, at a heating rate Vc between 20 and 700° C. comprised between 4 and 12° C./s, to obtain a heated blank, and at a heating rate Vc′ between 500 and 700° C. comprised between 1.5 and 6° C./s, to obtain a heated blank.

4. The process according to claim 3 , wherein the heating rate Vc and Vc′ are the same.

5. The process according to claim 3 , wherein an elapsed time between when said heated blank exits said furnace and said stamping commences is not more than 10 seconds.

6. The process according to claim 1 , wherein the thickness t p is from 20 to 33 micrometers at every location on said first and second sides of said strip or sheet.

7. The process according to claim 1 , wherein the coating has, in surfacic fraction, less than 10% of porosities.

8. The process according to claim 1 , wherein the superficial layer has less than 20% of porosities.

9. The process according to claim 1 , wherein a composition of the steel includes by weight:

0.10%<carbon<0.5%;

0.5%<manganese<3%;

0.1%<silicon<1%;

0.01%<chromium<1%;

nickel<0.1%;

copper<0.1%;

titanium<0.2%;

aluminum<0.1%;

phosphorus<0.1%;

sulfur<0.05%; and

0.0005%<boron<0.010%.

10. The process according to claim 1 , wherein a composition of the superficial layer includes by weight: 39 to 47% Fe, 53 to 61% Al and 0 to 2% Si.

11. A process for making a hot stamped coated steel sheet product, comprising:

pre-coating a steel strip or sheet with aluminum or aluminum alloy by hot dipping said steel strip or sheet having a first side and a second side in an aluminum or aluminum alloy bath to provide a pre-coating having a thickness t p of from 20 to 33 micrometers;

cutting said pre-coated steel strip or sheet to obtain a pre-coated steel blank; heating said aluminum or aluminum alloy pre-coated steel blank in a furnace;

transferring said heated blank to a die;

hot stamping said heated blank in said die, to thereby obtain a hot stamped steel product, and

cooling said hot stamped steel sheet product at a mean rate Vr during an interval between when said product exits said furnace and when said product reaches 400° C., of at least 30° C./s so as to obtain a hot stamped coated steel sheet product with a coating having a plurality of layers;

the plurality of layers including, from the steel strip or sheet outwards, an interdiffusion layer, an intermediate layer, an intermetallic layer and a superficial layer,

the intermetallic layer having a hardness HV50 g from 522 to 710.

12. The process according to claim 11 , wherein the coating has, in surfacic fraction, less than 10% of porosities.

13. The process according to claim 11 , wherein a composition of the steel includes by weight:

0.10%<carbon<0.5%;

0.5%<manganese<3%;

0.1%<silicon<1%;

0.01%<chromium<1%;

nickel<0.1%;

copper<0.1%;

titanium<0.2%;

aluminum<0.1%;

phosphorus<0.1%;

sulfur<0.05%; and

0.0005%<boron<0.010%.

14. The process according to claim 11 , wherein a composition of the intermetallic layer includes by weight: 62 to 67% Fe, 30 to 34% Al and 2 to 6% Si.

15. A process for making a hot stamped coated steel sheet product, comprising:

pre-coating a steel strip or sheet with aluminum or aluminum alloy by hot dipping said steel strip or sheet having a first side and a second side in an aluminum or aluminum alloy bath to provide a pre-coating having a thickness t p of from 20 to 33 micrometers;

cutting said pre-coated steel strip or sheet to obtain a pre-coated steel blank; heating said aluminum or aluminum alloy pre-coated steel blank in a furnace;

transferring said heated blank to a die;

hot stamping said heated blank in said die, to thereby obtain a hot stamped steel product, and

cooling said hot stamped steel sheet product at a mean rate Vr during an interval between when said product exits said furnace and when said product reaches 400° C., of at least 30° C./s so as to obtain a hot stamped coated steel sheet product with a coating having a plurality of layers;

the plurality of layers including, from the steel strip or sheet outwards, an interdiffusion layer, an intermediate layer, an intermetallic layer and a superficial layer,

the interdiffusion layer having a hardness HV50 g from 290 to 410.

16. The process according to claim 15 , wherein the coating has, in surfacic fraction, less than 10% of porosities.

17. The process according to claim 15 , wherein a composition of the steel includes by weight:

0.10%<carbon<0.5%;

0.5%<manganese<3%;

0.1%<silicon<1%;

0.01%<chromium<1%;

nickel<0.1%;

copper<0.1%;

titanium<0.2%;

aluminum<0.1%;

phosphorus<0.1%;

sulfur<0.05%; and

0.0005%<boron<0.010%.

18. The process according to claim 15 , wherein a composition of the interdiffusion layer includes by weight: 86 to 95% Fe, 4 to 10% Al and 0 to 5% Si.

Assignments (2)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Mar 22, 2019
From: ARCELORMITTAL FRANCE
To: ARCELORMITTAL
Reel/Frame 048673/0772 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Sep 28, 2010
From: SPEHNER, DOMINIQUE; KEFFERSTEIN, RONALD; DRILLET, PASCAL
To: ARCELORMITTAL FRANCE
Reel/Frame 025049/0213 →
Continuity (2)
Continuation PCTIB2008000079 · Jan 15, 2008
Related Publication 20110006491A1 · Jan 13, 2011