IP Library Granted Patent US 8,795,430
Granted Patent B2
US 8,795,430 · App. 12/716,176 · Granted Aug 5, 2014

Method of improving surface morphology of (Ga,Al,In,B)N thin films and devices grown on nonpolar or semipolar (Ga,Al,In,B)N substrates

Inventors: Robert M. Farrell (Goleta, CA); Michael Iza (Santa Barbara, CA); James S. Speck (Goleta, CA); Steven P. DenBaars (Goleta, CA); Shuji Nakamura (Santa Barbara, CA)
Assignee: The Regents of the University of California
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Quick Facts
Patent No.
US 8,795,430
App. No.
12/716,176
Granted
Aug 5, 2014
Kind
B2
Abstract

A method for improving the growth morphology of (Ga,Al,In,B)N thin films on nonpolar or semipolar (Ga,Al,In,B)N substrates, wherein a (Ga,Al,In,B)N thin film is grown directly on a nonpolar or semipolar (Ga,Al,In,B)N substrate or template and a portion of the carrier gas used during growth is comprised of an inert gas. Nonpolar or semipolar nitride LEDs and diode lasers may be grown on the smooth (Ga,Al,In,B)N thin films grown by the present invention.

Claims (27)

1. A method for fabricating III-nitride film, comprising:

growing a III-nitride film having a planar top surface, wherein the planar top surface:

is a nonpolar or semipolar plan, and

has a root mean square surface roughness, as-grown, of less than 0.5 nanometers over an area of at least 100 micrometers squared.

2. The method of claim 1 , further comprising growing the film on a III-nitride substrate or template with a miscut away from a low index crystal orientation.

3. The method of claim 2 , wherein the substrate or template is an m-plane substrate or template, the miscut has a miscut angle toward a [000-1] direction between 0.75° and 1.50°, and the III-nitride film is grown on a surface of the miscut.

4. The method of claim 1 , further comprising growing the film using a carrier gas, wherein at least a portion of the carrier gas is comprised of an inert gas and the inert gas is comprised of one or more of the following: N 2 , He, Ne, Ar, Kr, or Xe.

5. The method of claim 1 , wherein one or more device layers are deposited on the top surface of the film, and the device layers are grown with at least a portion of the carrier gas being comprised of H 2 .

6. The method of claim 5 , wherein the device layers include one or more p-type doped layers of the device and the p-type doped layers are grown with at least a portion of the carrier gas being comprised of H 2 .

7. A nonpolar or semipolar III-nitride film, comprising:

a planar top surface, wherein the planar top surface:

is a nonpolar or semipolar plane, and

has a root mean square surface roughness, as-grown, of less than 0.5 nanometers over an area of at least 100 micrometers squared.

8. The film of claim 7 , wherein the area has an absence of striations.

9. The film of claim 7 , wherein the top surface is atomically smooth with a surface roughness on the order of a diameter of Ga,Al,In,B, and N atoms.

10. The film of claim 7 , wherein the root mean square surface roughness is less than 0.25 nanometers over the area.

11. The film of claim 7 , wherein the film is deposited on a surface of an m-plane substrate, and the surface of the m-plane substrate is a miscut with a miscut angle between 0.75° and 1.50° toward a [000-1] direction.

12. The film of claim 11 , wherein the substrate is a Gallium Nitride substrate.

13. The film of claim 7 , wherein the area of the top surface is smoother than a surface characterized pyramidal hillocks having a density of 8.4×10 2 cm −2 , a size of 10 micrometers and a slope angle of 0.1°.

14. The film of claim 7 , wherein the area of the top surface is smoother than a surface characterized pyramidal hillocks having a density of 1.1×10 6 cm −2 .

15. The film of claim 7 , wherein the film is an m-plane GaN film and the top surface is an m-plane of the m-plane GaN film.

16. The film of claim 7 , wherein device layers grown on the film have a top surface that is at least as smooth as the top surface of the film.

17. The film of claim 7 , wherein the area is optically smooth and has an absence of identifiable non-planar surface undulations or features as measured using an optical microscope and with light wavelengths between 400 nanometers and 600 nanometers, the film is a substrate for epitaxial deposition of one or more device layers that emit light having an output power of at least 2 milliwatts at 20 milliamps drive current, and the drive current is direct current.

18. The film of claim 7 , wherein the plane is a nonpolar plane and the film is a nonpolar film.

19. The film of claim 7 , wherein the plane is a semipolar plane and the film is a semipolar film.

20. The film of claim 7 , wherein the film is Gallium Nitride.

21. The film of claim 7 , wherein the film is grown on a Gallium Nitride substrate.

Assignments (1)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Apr 23, 2010
From: FARRELL, ROBERT M.; IZA, MICHAEL; SPECK, JAMES S.; DENBAARS, STEVEN P.; NAKAMURA, SHUJI
To: THE REGENTS OF THE UNIVERSITY OF CALIFORNIA
Reel/Frame 024281/0918 →
Continuity (3)
Provisional Application 61156710 · Mar 2, 2009
Provisional Application 61184535 · Jun 5, 2009
Related Publication 20100219416A1 · Sep 2, 2010