IP Library Granted Patent US 8,871,747
Granted Patent B2
US 8,871,747 · App. 13/060,789 · Granted Oct 28, 2014

Urea and thiourea derivatives

Inventors: Mette Knak Christensen (Holte, DK); Fredrik Bjorkling (Helsingborg, SE)
Assignee: Topotarget A/S
C07D213/75C07D253/07C07D213/40C07D231/40C07D413/12C07D239/42
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Quick Facts
Patent No.
US 8,871,747
App. No.
13/060,789
Granted
Oct 28, 2014
Kind
B2
Abstract

The present application discloses compounds of formula (I) wherein X is ═O, ═S, ═NH, ═NOH and ═NO-Me; A is —C(═O)—, —S(═O) 2 —, —C(═S)— and P(═O)(R 5 )—; B is, —O—, —(CH 2 ) 3-6 —, and O—(CH 2 ) 2-5 —; D is, —O—, —CR 7 R 8 — and —NR 9 ; m is 0-12, n is 0-12, m+n is 1-20; p is 0-4; R 1 is opt. sub. heteroaryl; and pharmaceutically acceptable salts thereof, and prodrugs thereof. The application also discloses the compound for use as a medicament for the treatment of a disease or a condition caused by an elevated level of nicotinamide phosphoribosyltransferase (NAMPRT), e.g. inflammatory and tissue repair disorders; dermatosis; autoimmune diseases, Alzheimer's disease, stroke, athersclerosis, restenosis, diabetes, glomerulonephritis, cancer, cachexia, inflammation associated with infection and certain viral infections, including Acquired Immune Deficiency Syndrome (AIDS), adult respiratory distress syndrome, ataxia telengiectasia.

Claims (127)

1. A compound of the formula (I)

wherein

X is selected from ═O and ═S;

A is selected from —C(═O)— and —S(═O) 2 —;

B is selected from —(CH 2 ) 3-6 —, —O—, and —O—(CH 2 ) 2-5 —;

D is selected from a single bond —O—, and —NR 9 , wherein R 9 is selected from hydrogen, optionally substituted C 1-12 -alkyl, optionally substituted C 1-12 -alkenyl, optionally substituted aryl, optionally substituted heterocyclyl, and optionally substituted heteroaryl;

m is an integer of 2-8 and n is 0;

p is an integer of 0-2;

R 1 is selected from optionally substituted heteroaryl;

R 2 is selected from hydrogen, optionally substituted C 3-12 -cycloalkyl, —[CH 2 CH 2 O] 1-10 -(optionally substituted C 1-6 -alkyl), CH 2 ) 0-2 -(optionally substituted aryl), —(CH 2 ) 0-2 -(optionally substituted heteroaryl) and —(CH 2 ) 0-2 -(optionally substituted heterocyclyl); and

R 3 is selected from optionally substituted C 3-12 -cycloalkyl, —[CH 2 CH 2 O] 1-10 -(optionally substituted C 1-6 -alkyl), optionally substituted C 1-12 -alkenyl, optionally substituted aryl, optionally substituted heterocyclyl, and optionally substituted heteroaryl;

R 4 is independently selected from hydrogen, optionally substituted C 3-12 -cycloalkyl, —(CH 2 ) 0-2 -(optionally substituted aryl), —(CH 2 ) 0-2 -(optionally substituted heteroaryl) and —(CH 2 ) 0-2 -(optionally substituted heterocyclyl); and

R 4* is hydrogen;

with the provisos that R 1 is not optionally substituted thiazol-2-yl when p is 0;

and with the proviso that the compound is not phenyl-NH—C(═O)—(CH 2 ) 5 —NH—C(═S)—NH-(4-pyridyl);

and pharmaceutically acceptable salts thereof, and prodrugs thereof.

2. The compound according to claim 1 , wherein B is —O—.

3. The compound according to claim 1 , wherein D is a single bond.

4. The compound according to claim 1 , wherein B is selected from —(CH 2 ) 3-6 — and —O—(CH 2 ) 2-5 —.

5. The compound according to claim 4 , wherein A is —S(═O) 2 —.

6. The compound according to claim 1 , wherein R 1 is selected from optionally substituted pyridin-4-yl, optionally substituted pyrimidin-4-yl, optionally substituted 1,2,4-triazin-3-yl, optionally substituted isoxazol-4-yl, optionally substituted pyrazin-2-yl, and optionally substituted picolyl.

7. The compound according to claim 1 , wherein p is 0 and R 1 is pyridine-4-yl.

8. The compound according to claim 1 , which is selected from compounds 1001-1101:

Com-

pound

Structure

1001.

1002.

1003.

1004.

1005.

1006.

1007.

1008.

1009.

1010.

1011.

1012.

1013.

1014.

1015.

1016.

1017.

1018.

1019.

1020.

1021.

1022.

1023.

1024.

1025.

1026.

1027.

1028.

1029.

1030.

1031.

1032.

1033.

1034.

1035.

1036.

1037.

1038.

1039.

1040.

1041.

1042.

1043.

1044.

1045.

1046.

1047.

1048.

1049.

1050.

1051.

1052.

1053.

1054.

1055.

1056.

1057.

1058.

1059.

1060.

1061.

1062.

1063.

1064.

1065.

1066.

1067.

1068.

1069.

1070.

1071.

1072.

1073.

1074.

1075.

1076.

1077.

1078.

1079.

1080.

1081.

1082.

1083.

1084.

1085.

1086.

1087.

1088.

1089.

1090.

1091.

1092.

1093.

1094.

1095.

1096.

1097.

1098.

1099.

1100.

1101.

Assignments (3)
CHANGE OF NAME Recorded Oct 16, 2015
From: ONXEO DK
To: ONXEO DK, BRANCH OF ONXEO S.A., FRANCE
Reel/Frame 036807/0920 →
CHANGE OF NAME Recorded Jul 9, 2015
From: TOPOTARGET S.A.
To: ONXEO DK
Reel/Frame 036053/0148 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Sep 27, 2011
From: CHRISTENSEN, METTE KNAK; BJORKLING, FREDRICK
To: TOPOTARGET A/S
Reel/Frame 026977/0148 →
Continuity (2)
Provisional Application 61092838 · Aug 29, 2008
Related Publication 20120010172A1 · Jan 12, 2012