IP Library Granted Patent US 8,876,937
Granted Patent B2
US 8,876,937 · App. 14/248,061 · Granted Nov 4, 2014

Production of nanostructures

Inventors: Sheng Peng (San Francisco, CA); Arjun Srinivas (San Francisco, CA); Tom Credelle (San Francisco, CA); Andrew Loxley (San Francisco, CA); Gayatri Keskar (San Francisco, CA)
Assignee: Innova Dynamics, Inc.
B22F9/24B22F2009/245Y10S977/896B82Y40/00Y10S977/762
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Quick Facts
Patent No.
US 8,876,937
App. No.
14/248,061
Granted
Nov 4, 2014
Kind
B2
Abstract

Methods of producing nanowires and resulting nanowires are described. In one implementation, a method of producing nanowires includes energizing (i) a metal-containing reagent; (ii) a templating agent; (iii) a reducing agent; and (iv) a seed-promoting agent (SPA) in a reaction medium and under conditions of a first temperature for at least a portion of a first duration, followed by a second temperature for at least a portion of a second duration, and the second temperature is different from the first temperature.

Claims (21)

1. A method of producing nanowires, comprising:

energizing

(i) a metal-containing reagent;

(ii) a templating agent;

(iii) a reducing agent; and

(iv) a seed-promoting agent (SPA)

in a reaction medium and under conditions of a first temperature for at least a portion of a first duration, followed by a second temperature for at least a portion of a second duration, and the second temperature is different from the first temperature, wherein:

the reaction medium includes an alcohol including at least three hydroxyl groups per molecule,

the first temperature is less than 85° C.,

the second temperature is less than 105° C. and is greater than the first temperature,

the metal-containing reagent is silver nitrate,

the templating agent is poly(vinylpyrrolidone),

the reducing agent is an oxidized derivative of the alcohol,

the SPA is sodium chloride, and

an overall concentration of silver in the reaction medium, including ionic and elemental metal forms, is less than 0.1 molar.

2. The method of claim 1 , wherein the alcohol is glycerol.

3. The method of claim 1 , wherein the templating agent is in a solid or semi-solid form when combined with the metal-containing reagent.

4. The method of claim 1 , wherein:

the SPA is a first SPA, and

the energizing further includes energizing a second SPA that is a source of nitrate anions different from silver nitrate.

5. The method of claim 1 , wherein the first temperature is at least 40° C., and the second duration is longer than the first duration.

Assignments (3)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Dec 30, 2019
From: NUOVO FILM INC.
To: NUOVO FILM SUZHOU CHINA INC.
Reel/Frame 051448/0865 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jun 13, 2016
From: INNOVA DYNAMICS, INC.
To: NUOVO FILM INC.
Reel/Frame 038900/0451 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Apr 9, 2014
From: PENG, SHENG; SRINIVAS, ARJUN; CREDELLE, TOM; LOXLEY, ANDREW; KESKAR, GAYATRI
To: INNOVA DYNAMICS, INC.
Reel/Frame 032637/0577 →
Continuity (5)
Continuation 14203482 · Mar 10, 2014
Provisional Application 61774917 · Mar 8, 2013
Provisional Application 61793192 · Mar 15, 2013
Provisional Application 61920429 · Dec 23, 2013
Related Publication 20140251086A1 · Sep 11, 2014