IP Library Granted Patent US 8,883,822
Granted Patent B2
US 8,883,822 · App. 13/887,177 · Granted Nov 11, 2014

1H-pyrazolo[3,4-B]pyridines and therapeutic uses thereof

Inventors: John Hood (San Diego, CA); Sunil Kumar KC (San Diego, CA); David Mark Wallace (San Diego, CA)
Assignee: Samumed, LLC
C07D401/14A61K31/437
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Quick Facts
Patent No.
US 8,883,822
App. No.
13/887,177
Granted
Nov 11, 2014
Kind
B2
Abstract

Provided herein are compounds according to Formulas (I) or (II) and pharmaceutically acceptable salts thereof, and compositions comprising the same, for use in various methods, including treating cancer, abnormal cellular proliferation, angiogenesis, Alzheimer's disease, lung disease, osteoarthritis, idiopathic pulmonary fibrosis and neurological conditions/disorders/diseases.

Claims (64)

1. A compound, or pharmaceutically acceptable salt thereof, of Formula I:

wherein:

R 1 and R 2 are independently selected from the group consisting of H, lower alkyl, halide, —(C 1-9 alkyl) n aryl(R 6 ) q , —(C 1-9 alkyl) n heteroaryl(R 7 ) q , —(C 1-9 alkyl) n heterocyclyl(R 8 ) q , —(C 1-9 alkyl) n N(R 9 ) 2 , —OR 10 and —NHC(═O)R 11 ;

R 3 is selected from the group consisting of H, halide and lower alkyl;

with the proviso that at least two of R 1 , R 2 and R 3 are H;

R 4 and R 5 are independently selected from the group consisting of H, —C(═O)N(R 12 ) 2 , -aryl(R 13 ) q , -heterocyclyl(R 14 ) q , and -heteroaryl(R 15 ) q ;

with the proviso that at least one of R 4 and R 5 is H;

each R 6 is a substituent attached to the aryl ring and independently selected from the group consisting of H, —C 1-9 alkyl, halide, CF 3 and CN;

each R 7 is a substituent attached to the heteroaryl ring and independently selected from the group consisting of H, —C 1-9 alkyl, halide, CF 3 and CN;

each R 8 is a substituent attached to the heterocyclyl ring and independently selected from the group consisting of H, halide, —(C 1-3 alkyl) n aryl(R 6 ) q , and —C 1-4 alkyl;

each R 9 is independently selected from the group consisting of H, —C 1-9 alkyl, —(C 1-3 alkyl) n aryl(R 6 ) q , —(C 1-3 alkyl) n carbocyclyl and —(C 1-9 alkyl)N(R 16 ) 2 ;

alternatively, two adjacent R 9 or two adjacent R 12 , may be taken together with the atoms to which they are attached to form a heterocyclyl(R 17 ) q ;

R 10 is selected from the group consisting of H, —CF 3 , —(C 1-3 alkyl) n aryl(R 6 ) q , and —C 1-9 alkyl;

R 11 is selected from the group consisting of —(C 1-3 alkyl) n aryl(R 6 ) q , —(C 1-3 alkyl) n carbocyclyl, —C 1-9 alkyl and —CF 3 ;

each R 12 is independently selected from the group consisting of H, —(C 1-9 alkyl) n aryl(R 6 ) q and —C 1-9 alkyl;

each R 13 is a substituent attached to the aryl ring and independently selected from the group consisting of H, halide, —CF 3 , CN, —(C 1-3 alkyl) n heterocyclyl(R 8 ) q , —(C 1-9 alkyl) n N(R 9 ) 2 and —(C 1-9 alkyl) n NHSO 2 R 18 ;

each R 14 is a substituent attached to the heterocyclyl ring and independently selected from the group consisting of H, lower alkyl, halide, —CF 3 and CN;

each R 15 is a substituent attached to the heteroaryl ring and independently selected from the group consisting of H, lower alkyl, halide, —CF 3 , CN, —C(═O)(C 1-3 alkyl), —(C 1-9 alkyl) n N(R 9 ) 2 and —(C 1-9 alkyl) n NHSO 2 R 18 ;

each R 16 is independently selected from the group consisting of H and lower alkyl;

each R 17 is a substituent attached to the heterocyclyl ring and independently selected from the group consisting of H, —(C 1-9 alkyl) n aryl(R 6 ) q , and —C 1-9 alkyl;

each R 18 is a lower alkyl;

A is C;

each q is an integer of 1 to 5;

each n is an integer of 0 or 1; and

with the proviso that Formula I is not a structure selected from the group consisting of:

2. The compound of claim 1 wherein heteroaryl is pyridinyl.

3. The compound of claim 1 wherein heterocyclyl is selected from the group consisting of azetidinyl, pyrrolidinyl, morpholinyl, piperazinyl and piperidinyl.

4. The compound of claim 1 wherein R 2 is selected from the group consisting of H, —(C 1-9 alkyl) n heterocyclyl(R 8 ) q , and —NHC(═O)R 11 and R 1 and R 3 are both H.

5. The compound of claim 4 wherein R 2 is —NHC(═O)R 11 .

6. The compound of claim 5 wherein R 11 is selected from the group consisting of —C 1-5 alkyl, carbocyclyl, phenyl(R 6 ) q , and —CH 2 phenyl(R 6 ) q .

7. The compound as in any one of claims 5 - 6 , in which R 4 is -heterocyclyl(R 14 ) q .

8. The compound of claim 7 wherein the heterocyclyl is selected from the group consisting of piperazinyl and piperidinyl; and the R 14 is H or Me.

9. A pharmaceutical composition comprising a therapeutically effective amount of a compound, or pharmaceutically acceptable salt thereof, of Formula I:

wherein:

R 1 and R 2 are independently selected from the group consisting of H, lower alkyl, halide, —(C 1-9 alkyl) n aryl(R 6 ) q , —(C 1-9 alkyl) n heteroaryl(R 7 ) q , —(C 1-9 alkyl) n heterocyclyl(R 8 ) q , —(C 1-9 alkyl) n N(R 9 ) 2 , —OR 10 and —NHC(═O)R 11 ;

R 3 is selected from the group consisting of H, halide and lower alkyl;

with the proviso that at least two of R 1 , R 2 and R 3 are H;

R 4 and R 5 are independently selected from the group consisting of H, —C(═O)N(R 12 ) 2 , -aryl(R 13 ) q , -heterocyclyl(R 14 ) q , and -heteroaryl(R 15 ) q ;

with the proviso that at least one of R 4 and R 5 is H;

each R 6 is a substituent attached to the aryl ring and independently selected from the group consisting of H, —C 1-9 alkyl, halide, CF 3 and CN;

each R 7 is a substituent attached to the heteroaryl ring and independently selected from the group consisting of H, —C 1-9 alkyl, halide, CF 3 and CN;

each R 8 is a substituent attached to the heterocyclyl ring and independently selected from the group consisting of H, halide, —(C 1-3 alkyl) n aryl(R 6 ) q , and —C 1-4 alkyl;

each R 9 is independently selected from the group consisting of H, —C 1-9 alkyl, —(C 1-3 alkyl) n aryl(R 6 ) q , —(C 1-3 alkyl) n carbocyclyl and —(C 1-9 alkyl)N(R 16 ) 2 ;

alternatively, two adjacent R 9 or two adjacent R 12 , may be taken together with the atoms to which they are attached to form a heterocyclyl(R 17 ) q ;

R 10 is selected from the group consisting of H, —CF 3 , —(C 1-3 alkyl) n aryl(R 6 ) q , and —C 1-9 alkyl;

R 11 is selected from the group consisting of —(C 1-3 alkyl) n aryl(R 6 ) q , —(C 1-3 alkyl) n carbocyclyl, —C 1-9 alkyl and —CF 3 ;

each R 12 is independently selected from the group consisting of H, —(C 1-9 alkyl) n aryl(R 6 ) q and —C 1-9 alkyl;

each R 13 is a substituent attached to the aryl ring and independently selected from the group consisting of H, halide, —CF 3 , CN, —(C 1-3 alkyl) n heterocyclyl(R 8 ) q , —(C 1-9 alkyl) n N(R 9 ) 2 and —(C 1-9 alkyl) n NHSO 2 R 18 ;

each R 14 is a substituent attached to the heterocyclyl ring and independently selected from the group consisting of H, lower alkyl, halide, —CF 3 and CN;

each R 15 is a substituent attached to the heteroaryl ring and independently selected from the group consisting of H, lower alkyl, halide, —CF 3 , CN, —C(═O)(C 1-3 alkyl), —(C 1-9 alkyl) n N(R 9 ) 2 and —(C 1-9 alkyl) n NHSO 2 R 18 ;

each R 16 is independently selected from the group consisting of H and lower alkyl;

each R 17 is a substituent attached to the heterocyclyl ring and independently selected from the group consisting of H, —(C 1-9 alkyl) n aryl(R 6 ) q , and —C 1-9 alkyl;

each R 18 is a lower alkyl;

A is C;

each q is an integer of 1 to 5;

each n is an integer of 0 or 1; and

with the proviso that Formula I is not a structure selected from the group consisting of:

10. The pharmaceutical composition of claim 9 , wherein heteroaryl is pyridinyl.

11. The pharmaceutical composition of claim 9 , wherein heterocyclyl is selected from the group consisting of azetidinyl, pyrrolidinyl, morpholinyl, piperazinyl and piperidinyl.

12. The pharmaceutical composition of claim 9 , wherein R 2 is selected from the group consisting of H, —(C 1-9 alkyl) n heterocyclyl(R 8 ) q , and —NHC(═O)R 11 and R 1 and R 3 are both H.

13. The pharmaceutical composition of claim 12 , wherein R 2 is —NHC(═O)R 11 .

14. The pharmaceutical composition of claim 13 , wherein R 11 is selected from the group consisting of —C 1-5 alkyl, carbocyclyl, phenyl(R 6 ) q , and —CH 2 phenyl(R 6 ) q .

15. The pharmaceutical composition as in any one of claims 13 - 14 , in which R 4 is -heterocyclyl(R 14 ) q .

16. The pharmaceutical composition of claim 15 , wherein the heterocyclyl is selected from the group consisting of piperazinyl and piperidinyl; and the R 14 is H or Me.

Assignments (4)
RELEASE OF SECURITY INTEREST Recorded Mar 12, 2026
From: TMF GROUP NEW YORK, LLC, NOT INDIVIDUALLY BUT SOLELY AS COLLATERAL AGENT
To: BIOSPLICE THERAPEUTICS, INC.
Reel/Frame 075109/0434 →
SECURITY INTEREST Recorded Sep 14, 2022
From: BIOSPLICE THERAPEUTICS, INC.
To: VICKERS VENTURE FUND VI PTE. LTD.; VICKERS VENTURE FUND VI (PLAN) PTE. LTD.; VICKERS-SPLICE CO-INVESTMENT LLC; MED-PATHWAYS II LIMITED
Reel/Frame 061433/0786 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Mar 23, 2021
From: SAMUMED, LLC
To: BIOSPLICE THERAPEUTICS, INC.
Reel/Frame 055693/0882 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jun 21, 2013
From: HOOD, JOHN; KC, SUNIL KUMAR; WALLACE, DAVID MARK
To: SAMUMED, LLC
Reel/Frame 030662/0508 →
Continuity (2)
Provisional Application 61642915 · May 4, 2012
Related Publication 20130296302A1 · Nov 7, 2013