IP Library Granted Patent US 8,900,787
Granted Patent B2
US 8,900,787 · App. 13/896,245 · Granted Dec 2, 2014

Toner compositions

Inventors: Robert D. Bayley (Fairport, NY); Grazyna E. Kmiecik-Lawrynowicz (Fairport, NY); Maura A. Sweeney (Irondequoit, NY); Susan J. LaFica (Fairport, NY)
Assignee: Xerox Corporation
G03G9/093C08J3/02G03G9/087G03G9/0804C08K5/098G03G9/097C09D125/14G03G9/08
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Quick Facts
Patent No.
US 8,900,787
App. No.
13/896,245
Granted
Dec 2, 2014
Kind
B2
Abstract

A process includes forming particles in a latex by emulsion polymerization of a mixture including one or more monomers in an emulsion, and about 4 percent or less by weight of the mixture of a non-surfactant-based charge control agent, the non-surfactant-based charge control agent is distributed within a matrix of the particles, and forming toner particles from the particles in the latex, the toner particles supporting a sufficient triboelectric charge for use under A-zone environmental conditions in a single-component development system.

Claims (27)

1. A process comprising:

forming particles in a latex by emulsion polymerization of a mixture comprising:

one or more monomers in an emulsion; and

less than about 4 percent by weight of the mixture of a non-surfactant-based charge control agent, wherein the non-surfactant-based charge control agent is distributed within a matrix of the particles; and

forming toner particles from the particles in the latex, wherein the particles in the latex are used to form a shell of the toner particles and further wherein the toner particles support a sufficient triboelectric charge for use under A-zone environmental conditions in a single-component development system.

2. The process of claim 1 , wherein the non-surfactant-based charge control agent is present at a concentration of less than about 3 percent by weight of the mixture.

3. The process of claim 1 , wherein the non-surfactant-based charge control agent is present at a concentration of less than about 2 percent by weight of the mixture.

4. The process of claim 1 , wherein the non-surfactant-based charge control agent is present at a concentration of less than about 1 percent by weight of the mixture.

5. The process of claim 1 , wherein the toner particles support a sufficient charge for use under C-zone environmental conditions in a single-component development system.

6. The process of claim 1 , wherein the toner particles are negatively charged.

7. The process of claim 1 , wherein the sufficient triboelectric charge for use under A-zone environmental conditions is in a range from about −20 microcoulombs/gram to −100 microcoulombs/gram.

8. The process of claim 1 , wherein the non-surfactant-based charge control agent is a metal salicylate.

9. The process of claim 6 , wherein the metal salicylate comprises zinc or aluminum.

10. The process of claim 1 , wherein the non-surfactant-based charge control agent is hydrophobic.

11. The process of claim 1 , comprising forming a core of the toner particles from the particles in the latex.

12. The process of claim 1 , comprising forming a core and shell from the particles in the latex.

13. The process of claim 1 , wherein the one or more monomers comprises a styrene, an acrylate, a methacrylate, a butadiene, an isoprene, an acrylic acid, a methacrylic acid, an acrylonitrile, and combinations thereof.

14. A process comprising

polymerizing by emulsion polymerization a mixture comprising:

one or more monomers in an emulsion;

about 1 percent or less by weight of the mixture of a negatively charged charge control agent;

wherein the polymerizing step provides a latex with the non-surfactant-based charge control agent distributed within a matrix of the latex; and

forming by emulsion aggregation/coalescence a plurality of toner particles, wherein the latex is used to form a shell of the toner particles and further

wherein the plurality of toner particles support a sufficient triboelectric charge for use under A-zone environmental conditions in a single-component development system.

15. The process of claim 14 , wherein the plurality of toner particles support a sufficient charge for use under C-zone environmental conditions in a single-component development system.

16. The process of claim 14 , wherein the negatively charged charge control agent is a metal salicylate.

17. The process of claim 12 , wherein the sufficient triboelectric charge for use under A-zone environmental conditions is in a range from about −20 microcoulombs/gram to −100 microcoulombs/gram.

Assignments (9)
SECOND LIEN NOTES PATENT SECURITY AGREEMENT Recorded Jul 2, 2025
From: XEROX CORPORATION
To: U.S. BANK TRUST COMPANY, NATIONAL ASSOCIATION, AS COLLATERAL AGENT
Reel/Frame 071785/0550 →
FIRST LIEN NOTES PATENT SECURITY AGREEMENT Recorded Apr 11, 2025
From: XEROX CORPORATION
To: U.S. BANK TRUST COMPANY, NATIONAL ASSOCIATION, AS COLLATERAL AGENT
Reel/Frame 070824/0001 →
TERMINATION AND RELEASE OF SECURITY INTEREST IN PATENTS RECORDED AT RF 064760/0389 Recorded Feb 13, 2024
From: CITIBANK, N.A., AS COLLATERAL AGENT
To: XEROX CORPORATION
Reel/Frame 068261/0001 →
SECURITY INTEREST Recorded Feb 13, 2024
From: XEROX CORPORATION
To: CITIBANK, N.A., AS COLLATERAL AGENT
Reel/Frame 066741/0001 →
SECURITY INTEREST Recorded Nov 20, 2023
From: XEROX CORPORATION
To: JEFFERIES FINANCE LLC, AS COLLATERAL AGENT
Reel/Frame 065628/0019 →
SECURITY INTEREST Recorded Jun 22, 2023
From: XEROX CORPORATION
To: CITIBANK, N.A., AS COLLATERAL AGENT
Reel/Frame 064760/0389 →
RELEASE OF SECURITY INTEREST IN PATENTS AT R/F 062740/0214 Recorded May 18, 2023
From: CITIBANK, N.A., AS AGENT
To: XEROX CORPORATION
Reel/Frame 063694/0122 →
SECURITY INTEREST Recorded Nov 10, 2022
From: XEROX CORPORATION
To: CITIBANK, N.A., AS AGENT
Reel/Frame 062740/0214 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded May 16, 2013
From: BAYLEY, ROBERT D.; KMIECIK-LAWRYNOWICZ, GRAZYNA E.; SWEENEY, MAURA A.; LAFICA, SUSAN J.
To: XEROX CORPORATION
Reel/Frame 030439/0579 →
Continuity (2)
Continuation In Part 12575736 · Oct 8, 2009
Related Publication 20130252162A1 · Sep 26, 2013