IP Library Granted Patent US 8,940,391
Granted Patent B2
US 8,940,391 · App. 12/901,309 · Granted Jan 27, 2015

Silicon carbide fibers and articles including same

Inventors: John E. Garnier (Idaho Falls, ID); George W. Griffith (Idaho Falls, ID)
Assignee: Advanced Ceramic Fibers, LLC
C04B35/62281B82Y30/00C01B31/36C04B35/565C04B35/571C04B35/573C04B35/806C04B2235/428C04B2235/46C04B2235/48C04B2235/5244C04B2235/5248C04B2235/526C04B2235/5264C04B2235/5284C04B2235/5445C04B2235/616C04B2235/72C04B2235/767
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Quick Facts
Patent No.
US 8,940,391
App. No.
12/901,309
Granted
Jan 27, 2015
Kind
B2
Abstract

Methods of producing silicon carbide fibers. The method comprises reacting a continuous carbon fiber material and a silicon-containing gas in a reaction chamber at a temperature ranging from approximately 1500° C. to approximately 2000° C. A partial pressure of oxygen in the reaction chamber is maintained at less than approximately 1.01×10 2 Pascal to produce continuous alpha silicon carbide fibers. Continuous alpha silicon carbide fibers and articles formed from the continuous alpha silicon carbide fibers are also disclosed.

Claims (21)

1. A silicon carbide fiber comprising filaments comprising alpha silicon carbide surrounding a hollow core.

2. The silicon carbide fiber of claim 1 , wherein the alpha silicon carbide is substantially free of beta silicon carbide.

3. The silicon carbide fiber of claim 1 , wherein the filaments have a diameter of from approximately 1 μm to approximately 100 μm.

4. The silicon carbide fiber of claim 1 , wherein the filaments have a diameter of from approximately 2 μm to approximately 20 μm.

5. The silicon carbide fiber of claim 1 , wherein the filaments have a diameter of from approximately 8 μm to approximately 10 μm.

6. The silicon carbide fiber of claim 1 , wherein the silicon carbide fiber comprises between approximately 300 filaments and approximately 3000 filaments.

7. The silicon carbide fiber of claim 1 , wherein the silicon carbide fiber has a length of at least approximately 5 cm.

8. An article comprising a plurality of silicone carbide fibers as recited in claim 1 , the silicon carbide fibers being dispersed in a matrix.

9. The article of claim 8 , wherein the matrix comprises silicon carbide.

10. The article of claim 8 , wherein the matrix comprises alpha silicon carbide.

11. The article of claim 8 , wherein the article is configured as at least a portion of a heat exchanger filter nuclear fuel containment fusion reactor component hot gas engine, turbine engine, hypersonic missile leading edge, or rocket component.

12. The silicon carbide fiber of claim 1 , wherein greater than approximately 99.8% of carbon atoms in the alpha silicon carbide are bonded to a silicon atom.

13. The silicon carbide fiber of claim 1 , wherein the silicon carbide fiber has a density of approximately 3.21 g/cc.

14. A partially converted fiver comprising a layer of alpha silicon carbide formed over a core of unreacted carbon fiber, the layer of alpha silicon carbide including filaments of alpha silicone carbide.

15. The partially converted fiber of claim 14 , wherein the layer formed over the core of unreacted carbon fiber is substantially free of beta silicon carbide.

16. The partially converted fiber of claim 14 , wherein the core of unreacted carbon fiber is continuous pitch-based resin or a continuous polyacrylonitrile-based carbon fiber.

17. The partially converted fiber of claim 14 , wherein the layer formed over the core of unreacted carbon fiber consists essentially of alpha silicon carbide.

18. An article comprising a plurality of partially converted fibers as recited in claim 14 , the partially converted fibers being dispersed in a matrix.

19. The article of claim 18 , wherein the matrix comprises silicone carbide.

20. The article of claim 18 , wherein the matrix comprises alpha silicon carbide.

21. The article of claim 18 , wherein the article is configured as at least a portion of a heat exchanger, filter, nuclear fuel containment, fusion reactor component, hot gas engine, turbine engine, hypersonic missile leading edge, or rocket component.

Assignments (4)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Sep 9, 2013
From: BATTELLE ENERGY ALLIANCE, LLC
To: GARNIER, JOHN E.; GRIFFITH, GEORGE W.
Reel/Frame 031168/0222 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Sep 9, 2013
From: GARNIER, JOHN E.; GRIFFITH, GEORGE W.
To: ADVANCED CERAMIC FIBERS, LLC
Reel/Frame 031168/0243 →
CONFIRMATORY LICENSE Recorded Jan 25, 2011
From: BATTLE ENERGY ALLIANCE, LLC
To: ENERGY, UNITED STATES DEPARTMENT OF
Reel/Frame 025710/0062 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Oct 15, 2010
From: GARNIER, JOHN E.; GRIFFITH, GEORGE W.
To: BATTELLE ENERGY ALLIANCE, LLC
Reel/Frame 025144/0676 →
Continuity (1)
Related Publication 20120088088A1 · Apr 12, 2012