IP Library Granted Patent US 8,987,162
Granted Patent B2
US 8,987,162 · App. 13/404,071 · Granted Mar 24, 2015

Hydrothermally stable, low-temperature NO

Inventors: Chaitanya K. Narula (Knoxville, TN); Xiaofan Yang (Knoxville, TN)
Assignee: UT-Battelle, LLC
B01J29/783B01D53/9418B01D2255/20738B01D2255/20761B01D2255/50B01D2258/012B01J29/7065B01J29/763B01J2229/186C01B39/026C01B39/06
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Quick Facts
Patent No.
US 8,987,162
App. No.
13/404,071
Granted
Mar 24, 2015
Kind
B2
Abstract

A catalyst composition includes a heterobimetallic zeolite characterized by a chabazite structure loaded with copper ions and at least one trivalent metal ion other than Al 3+ . The catalyst composition decreases NO x emissions in diesel exhaust and is suitable for operation in a catalytic converter.

Claims (15)

1. A catalyst composition comprising a heterobimetallic zeolite characterized by a chabazite structure loaded with copper ions and iron(III) ions, wherein said copper ions are present in said catalyst in a loading amount of above 1 wt % and said iron(III) ions are present in said catalyst in a loading amount of less than 1 wt %, and said copper and iron loading amounts are effective to achieve a NO x conversion at 150° C. of at least 50% in the presence of an ammonia reductant.

2. A catalyst in accordance with claim 1 , wherein said iron(III) ions are in combination with at least one other trivalent metal ion.

3. A catalyst in accordance with claim 2 , wherein said at least one other trivalent metal ion is a trivalent transition metal ion.

4. A catalyst in accordance with claim 2 , wherein said at least one other trivalent metal ion is a trivalent lanthanide metal ion.

5. A catalyst in accordance with claim 2 , wherein said at least one other trivalent metal ion is a trivalent main group metal ion.

6. A catalyst in accordance with claim 1 , wherein said zeolite comprises CuFe-SSZ-13.

7. A catalytic converter comprising a catalyst loaded onto a refractory substrate, said catalyst comprising a heterobimetallic zeolite characterized by a chabazite structure loaded with copper ions and iron(III) ions, wherein said copper ions are present in said catalyst in a loading amount of above 1 wt % and said iron(III) ions are present in said catalyst in a loading amount of less than 1 wt %, and said copper and iron loading amounts are effective to achieve a NO x conversion at 150° C. of at least 50% in the presence of an ammonia reductant.

8. A catalytic converter in accordance with claim 7 , wherein said iron(III) ions are in combination with at least one other trivalent metal ion.

9. A catalytic converter in accordance with claim 8 , wherein said at least one other trivalent metal ion is a trivalent transition metal ion.

10. A catalytic converter in accordance with claim 8 , wherein said at least one other trivalent metal ion is a trivalent lanthanide metal ion.

11. A catalytic converter in accordance with claim 8 , wherein said at least one other trivalent metal ion is a trivalent main group metal ion.

12. A catalytic converter in accordance with claim 7 , wherein said zeolite comprises CuFe-SSZ-13.

13. A catalytic converter in accordance with claim 7 , wherein said refractory substrate is characterized by a structure selected from the group consisting of a rod structure, a honeycomb structure, and a pinwheel structure.

14. The catalyst of claim 1 , wherein said copper ions are present in said catalyst in a loading amount of at least 1.5 wt % and said iron(III) ions are present in said catalyst in a loading amount of less than 1 wt %.

15. The catalyst of claim 1 , wherein said copper ions are present in said catalyst in a loading amount of at least 2 wt % and said iron(III) ions are present in said catalyst in a loading amount of less than 1 wt %.

Assignments (4)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Oct 24, 2012
From: OAK RIDGE ASSOCIATED UNIVERSITIES
To: UT-BATTELLE, LLC
Reel/Frame 029179/0180 →
CONFIRMATORY LICENSE Recorded Apr 11, 2012
From: UT-BATTELLE, LLC
To: U.S. DEPARTMENT OF ENERGY
Reel/Frame 028024/0793 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Feb 27, 2012
From: YANG, XIAOFAN
To: OAK RIDGE ASSOCIATED UNIVERSITIES
Reel/Frame 027764/0422 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Feb 27, 2012
From: NARULA, CHAITANYA K.
To: UT-BATTELLE, LLC
Reel/Frame 027764/0451 →
Continuity (1)
Related Publication 20130224082A1 · Aug 29, 2013